JP6106598B2 - タバコ由来シロップ組成物 - Google Patents
タバコ由来シロップ組成物 Download PDFInfo
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- JP6106598B2 JP6106598B2 JP2013544812A JP2013544812A JP6106598B2 JP 6106598 B2 JP6106598 B2 JP 6106598B2 JP 2013544812 A JP2013544812 A JP 2013544812A JP 2013544812 A JP2013544812 A JP 2013544812A JP 6106598 B2 JP6106598 B2 JP 6106598B2
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- Prior art keywords
- tobacco
- sugar
- syrup
- stem
- composition
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Images
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/302—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by natural substances obtained from animals or plants
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Botany (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Manufacture Of Tobacco Products (AREA)
Description
熱風乾燥したタバコ茎(〜4000ポンド)を収穫する。茎は下葉収穫後約5週間野外にあった。テンサイ茎から液体を圧搾するよう設計された圧搾機に茎を手作業で送り込む(茎が通過できるように若干調整する)。約70ガロン(560ポンド)の液体を回収する。液体はキルンに移される。液体に懸濁する細粒はキルンの底部に沈降する。液体はキルンで加熱し、約30分で沸騰し始める。緑色の泡層を頂部に形成し、掬い取り、廃棄する。沸騰の30分後、液体の密度はほぼ水の密度である。色は緑から茶/黄に変化した。
3つの125 mL分液漏斗に実施例1の20 gのタバコ茎シロップを添加する。1つの漏斗に50 mLの塩化メチレンを添加し、1つの漏斗に50 mLのヘキサンを添加し、1つの漏斗には50 mLのメチルt-ブチルエーテルを添加する。3つの全フラスコは激しく振とうし、一晩静置する。溶媒を除去し、無水硫酸ナトリウムで脱水し、約2 mLまで回転式蒸発器を用いて濃縮する。得られる試料はガスクロマトグラフィー(例えばAgilent 6890 GC)により分析する。
下葉収穫後約5週間野外にあり熱風乾燥したタバコ茎を収穫する。茎は熱風乾燥タバコの葉の乾燥で用いた条件と同様の条件を用いて5〜7日間熱風乾燥小屋で乾燥する。乾燥茎は約12重量%の水を含む。乾燥茎はチップ化し、粒状形態の材料を提供し、温水(60°C)を水:乾燥茎が約8:1の重量比で添加し、スラリーを生じる。スラリーは2時間保持した後、水性溶液を濾過し、2部に分配し、各部を個別に濃縮する。
Claims (26)
- ニコチアナ種植物の茎に由来する糖化合物を含む糖含有シロップの形態でたばこ製品に用いる風味タバコ組成物であって、前記シロップが少なくとも20のブリックスレベルを有する組成物。
- 糖含有シロップがタバコ原料への適用に適合するケーシング製剤または最上層製剤に含まれる、請求項1記載のタバコ組成物。
- 糖含有シロップがスクロース、フルクトース、およびグルコースを含む、請求項1記載のタバコ組成物。
- 糖含有シロップが少なくとも50重量%の水と糖化合物を含む、請求項1記載のタバコ組成物。
- 糖含有シロップが少なくとも15重量%の糖化合物を含む、請求項1記載のタバコ組成物。
- 糖含有シロップが少なくとも20重量%の糖化合物を含む、請求項1記載のタバコ組成物。
- 糖含有シロップがシロップ組成物の総重量に基づいて20重量%から60重量%の水および15重量%から40重量%の糖化合物を含む、請求項1記載のタバコ組成物。
- 糖含有シロップが20から50g/cm3の範囲の比重を有する、請求項1記載のタバコ組成物。
- 請求項1から請求項8のいずれか一項に記載の風味タバコ組成物を含むたばこ製品。
- さらにタバコ原料または非タバコ植物原料を糖含有シロップ用の担体として含む、請求項9記載のたばこ製品。
- たばこ製品が無煙タバコ組成物、喫煙具、または植物原料の不燃焼用に設定されたエアロゾル生成装置の形態である、請求項9記載のたばこ製品。
- 無煙タバコ組成物の形態が、湿性嗅ぎたばこ、乾燥嗅ぎたばこ、噛みたばこ、タバコ含有ガム、および溶解または融解するたばこ製品から成る群から選択される、請求項11記載のたばこ製品。
- 糖含有シロップをニコチアナ種植物の茎から調製する方法であって、
i)糖化合物を含む水性液体成分をニコチアナ種植物の茎またはその一部から採取する工程;および
ii)水性液体成分を濃縮して水性液体成分の比重を増し、たばこ製品における風味タバコ組成物としての使用に適した糖含有シロップを形成する工程を含み、前記糖含有シロップが少なくとも20のブリックスレベルを有する方法。 - さらにニコチアナ植物種の茎またはその一部を採取段階前に乾燥させる工程を含む、請求項13記載の方法。
- 乾燥段階が茎を14重量パーセント未満の水分量まで乾燥させる工程を含む、請求項14記載の方法。
- 採取段階が水性液体成分を茎から圧搾する工程;植物の茎またはその一部を液体と接触させ前記水性液体成分を取り出す工程;および前記茎を水性液体で抽出する工程の少なくとも1つを含む、請求項13記載の方法。
- 濃縮段階が水性液体成分を大気圧または真空下で加熱する工程を含む、請求項13記載の方法。
- 濃縮段階が水性液体成分を20から50g/cm3の比重に濃縮する工程を含む、請求項13記載の方法。
- さらに水性液体成分を濾過して固体成分を除去する工程を含む、請求項13記載の方法。
- 濾過段階が水性液体成分を限外濾過膜に曝す工程を含む、請求項19記載の方法。
- 水性液体成分が濃縮段階中に固体成分を表面からすくい取ることにより濾過される、請求項19記載の方法。
- さらに1以上の清澄剤を水性液体成分に添加することにより水性液体成分を浄化する工程を含む、請求項13記載の方法。
- さらに糖含有シロップを糖含有シロップ用の担体としてのタバコ原料または非タバコ植物原料に添加する工程を含む、請求項13記載の方法。
- さらにタバコ原料または非タバコ植物原料をたばこ製品に組み込む工程を含む、請求項23記載の方法。
- たばこ製品が無煙タバコ組成物または喫煙具の形態である、請求項24記載の方法。
- 無煙タバコ組成物の形態が、湿性嗅ぎたばこ、乾燥嗅ぎたばこ、噛みたばこ、タバコ含有ガム、および溶解または融解するたばこ製品から成る群から選択される、請求項25記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US12/971,746 US20120152265A1 (en) | 2010-12-17 | 2010-12-17 | Tobacco-Derived Syrup Composition |
US12/971,746 | 2010-12-17 | ||
PCT/US2011/065398 WO2012083127A1 (en) | 2010-12-17 | 2011-12-16 | Tobacco-derived syrup composition |
Publications (3)
Publication Number | Publication Date |
---|---|
JP2014501104A JP2014501104A (ja) | 2014-01-20 |
JP2014501104A5 JP2014501104A5 (ja) | 2015-01-22 |
JP6106598B2 true JP6106598B2 (ja) | 2017-04-05 |
Family
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Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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JP2013544812A Active JP6106598B2 (ja) | 2010-12-17 | 2011-12-16 | タバコ由来シロップ組成物 |
Country Status (6)
Country | Link |
---|---|
US (2) | US20120152265A1 (ja) |
EP (1) | EP2651253B1 (ja) |
JP (1) | JP6106598B2 (ja) |
CN (1) | CN103338661B (ja) |
ES (1) | ES2616791T3 (ja) |
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WO2012083127A1 (en) | 2012-06-21 |
US20190313690A1 (en) | 2019-10-17 |
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EP2651253A1 (en) | 2013-10-23 |
CN103338661B (zh) | 2016-07-13 |
EP2651253B1 (en) | 2016-11-30 |
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