JP5758412B2 - 消費者製品組成物で使用するジアミドゲル化剤 - Google Patents
消費者製品組成物で使用するジアミドゲル化剤 Download PDFInfo
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- JP5758412B2 JP5758412B2 JP2012557268A JP2012557268A JP5758412B2 JP 5758412 B2 JP5758412 B2 JP 5758412B2 JP 2012557268 A JP2012557268 A JP 2012557268A JP 2012557268 A JP2012557268 A JP 2012557268A JP 5758412 B2 JP5758412 B2 JP 5758412B2
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/32—Amides; Substituted amides
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- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C237/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups
- C07C237/02—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton
- C07C237/22—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups having the carbon atoms of the carboxamide groups bound to acyclic carbon atoms of the carbon skeleton having nitrogen atoms of amino groups bound to the carbon skeleton of the acid part, further acylated
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- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C271/00—Derivatives of carbamic acids, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
- C07C271/06—Esters of carbamic acids
- C07C271/08—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms
- C07C271/10—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atoms of the carbamate groups bound to hydrogen atoms or to acyclic carbon atoms
- C07C271/22—Esters of carbamic acids having oxygen atoms of carbamate groups bound to acyclic carbon atoms with the nitrogen atoms of the carbamate groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of hydrocarbon radicals substituted by carboxyl groups
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C271/00—Derivatives of carbamic acids, i.e. compounds containing any of the groups, the nitrogen atom not being part of nitro or nitroso groups
- C07C271/06—Esters of carbamic acids
- C07C271/32—Esters of carbamic acids having oxygen atoms of carbamate groups bound to carbon atoms of rings other than six-membered aromatic rings
- C07C271/34—Esters of carbamic acids having oxygen atoms of carbamate groups bound to carbon atoms of rings other than six-membered aromatic rings with the nitrogen atoms of the carbamate groups bound to hydrogen atoms or to acyclic carbon atoms
-
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- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/32—Amides; Substituted amides
- C11D3/323—Amides; Substituted amides urea or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3263—Amides or imides
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3272—Urea, guanidine or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2603/00—Systems containing at least three condensed rings
- C07C2603/02—Ortho- or ortho- and peri-condensed systems
- C07C2603/04—Ortho- or ortho- and peri-condensed systems containing three rings
- C07C2603/06—Ortho- or ortho- and peri-condensed systems containing three rings containing at least one ring with less than six ring members
- C07C2603/10—Ortho- or ortho- and peri-condensed systems containing three rings containing at least one ring with less than six ring members containing five-membered rings
- C07C2603/12—Ortho- or ortho- and peri-condensed systems containing three rings containing at least one ring with less than six ring members containing five-membered rings only one five-membered ring
- C07C2603/18—Fluorenes; Hydrogenated fluorenes
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- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Cosmetics (AREA)
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Description
外部構造化剤は、好ましくは、組成物の洗浄性界面活性剤のあらゆる構造化効果とは別個に、つまりは無関係に、消費者製品組成物にずり減粘性プロファイルを付与する。好ましい外部構造化剤には、50cps〜20,000cps、より好ましくは200cps〜10,000cps、最も好ましくは500cps〜7,000cpsの流動粘度(pouring viscosity)をもたらすものが含まれる。消費者製品組成物は、少なくとも1,500cps、好ましくは少なくとも10,000cps、より好ましくは少なくとも50,000cpsの静止粘度(resting viscosity)を有するのが好ましい。この静止(低応力)粘度は、パーッケージ内における軽い振盪下での、及び輸送中の、消費者製品組成物の粘度を表す。あるいは、消費者製品組成物は揺変性ゲルであってもよい。そのような組成物は、10,000cps〜500,000cps、好ましくは100,000cps〜400,000cps、より好ましくは200,000cps〜300,000cpsの静止粘度を有してもよい。消費者製品の好ましいずり減粘特性は、少なくとも2、好ましくは少なくとも10、より好ましくは少なくとも100、最大2000である、低応力粘度と流動粘度との比として定義される。
消費者製品組成物は、ジアミドゲル化剤を外部構造化剤として、0.01重量%〜10重量%、好ましくは0.05重量%〜5重量%、より好ましくは0.1重量%〜2重量%、最も好ましくは0.4重量%〜1重量%の濃度で含む。代替実施形態において、消費者製品組成物は、0.1重量%〜0.5重量%のジアミドゲル化剤(gallant)を含む。
(式中、AAは、
R3及びR4は、独立して、次式[II]:
[II](L’)m−(L”)q−R(式中、(m+q)は1〜10であり、
それにより、R1及びR2はアミノ官能性末端基である)を有する。
[III]Aa−Bb−Cc−Dd(式中、(a+b+c+d)は1〜20である)を有する。
(式中、AAは、
Rは、
消費者製品組成物は、希釈又は濃縮水性液体であってもよい。あるいは、消費者製品組成物は、ほぼ全体的に非水性であってもよく、非アミノ官能性有機溶媒を含んでいてもよい。そのような消費者製品組成物は、例えば、他の原料物質と共に導入され得る水をほとんど含有していなくてもよい。好ましくは、消費者製品組成物は、1重量%〜95重量%の水及び/又は非アミノ官能性有機溶媒を含む。濃縮洗剤に関しては、この組成物は、好ましくは5重量%〜70重量%、より好ましくは10重量%〜50重量%、最も好ましくは15重量%〜45重量%の水及び/又は非アミノ官能性有機溶媒を含む。
材料は、Iris Biotech GmbH,Waldershofer Str.49−51,95615 Marktredwitz,Germany;Bachem Holding AG,Hauptstrasse 144,4416 Bubendorf,Switzerland;Sigma Aldrich NV/SA,Kardinaal Cardijnplein 8,2880 Bornem,Belgiumから購入することができる。
1.濁度(NTU):
製造業者から提供された手順に従って調整されたHach 2100P濁度計を使用して、濁度(NTU:Nephelometric Turbidity Units(比濁度計濁度単位)で測定)を測定した。取扱説明書に従ってサンプルバイアルに15mLの代表サンプルを充填し、蓋をし、洗浄する。必要な場合、真空を適用するか又は超音波浴を使用することによって、サンプルを脱気してあらゆる気泡を除去する(手順に関する説明書を参照のこと)。自動範囲選択により濁度を測定する。
R.G.Weiss,P.Terech;「Molecular Gels:Materials with self−assembled fibrillar structures」2006 springer,p 243に基づいた管反転法(tube inversion method)によって、MGCを計算する。MGCを判定するために、スクリーニングを3回行う。
TA InstrumentsのAR−G2レオメーターをレオロジー的測定に使用する。
2 PEG−PVAグラフトコポリマーは、ポリエチレンオキシド主鎖及び多種のポリ酢酸ビニル側鎖を有するポリ酢酸ビニルグラフト化ポリエチレンオキシドコポリマーである。ポリエチレンオキシド主鎖の分子量は6000であり、ポリエチレンオキシドとポリ酢酸ビニルとの重量比は40対60であり、50個のエチレンオキシド単位当たりのグラフト点は1以下である。
3 −NH当たり20個のエトキシレート基を有する、分子量600g/molのポリエチレンイミンコア。
液体洗濯洗剤組成物を次の通りに調製する。
2 ジアミドゲル化剤プレミックスを介して添加
3 Millikenより供給される高分子色素
4、5 布地色相染料
6 非織物直接染料
7 ジアミドゲル化剤プレミックスを介して添加
8 gNaOH/製品100g
流体洗剤布地ケア組成物は、列挙された成分を記載の比率で混合することにより調製することができる。
2 Novozymes,Denmarkより入手可能。
3 −NH当たり20個のエトキシレート基を有する、分子量600g/molのポリエチレンイミンコア。BASF(Ludwigshafen,Germany)より入手可能。
4 国際公開第01/05874号に記載され、BASF(Ludwigshafen,Germany)より入手可能。
5 −NH当たり24個のエトキシレート基と−NH当たり16個のプロポキシレート基とを有する、分子量600g/molのポリエチレンイミンコア。BASF(Ludwigshafen,Germany)より入手可能。
6 PEG−PVAグラフトコポリマーは、ポリエチレンオキシド主鎖と複数のポリビニルアセテート側鎖とを有する、ポリ酢酸ビニルグラフト化ポリエチレンオキシドコポリマーである。ポリエチレンオキシド主鎖の分子量は約6000であり、ポリエチレンオキシドとポリビニルアセテートとの重量比は約40:60であり、50個のエチレンオキシド単位当たりのグラフト点は1以下である。BASF(Ludwigshafen,Germany)より入手可能。
食器手洗い用液体洗剤組成物は、列挙された成分を記載の比率で混合することにより調製することができる。
Claims (4)
- ジベンジル(2S,2’S)−1,1’−(エタン−1,2−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(プロパン−1,3−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(ブタン−1,4−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(ペンタン−1,5−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(ヘキサン−1,6−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(ヘプタン−1,7−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(オクタン−1,8−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(ノナン−1,9−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(デカン−1,10−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(ウンデカン−1,11−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(ドデカン−1,12−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(トリデカン−1,13−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(ヘキサデカン−1,16−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(オクトデカン−1,18−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;ジベンジル(2S,2’S)−1,1’−(テトラデカン−1,14−ジイルビス(アザンジイル))ビス(3−メチル−1−オキソブタン−2,1−ジイル)ジカルバマート;及びこれらの混合物からなる群から選択されるジアミドゲル化剤であって、
前記ジアミドゲル化剤がタンパク質でない、ジアミドゲル化剤。 - 前記ジアミドゲル化剤が、150〜1500g/モルの分子量を有する、請求項1に記載のジアミドゲル化剤。
- 前記ジアミドゲル化剤が、0.1〜100mg/mLの最小ゲル化濃度(MGC)を有する、請求項1に記載のジアミドゲル化剤。
- 消費者製品組成物を構造化するための、請求項1〜3のいずれか一項に記載のジアミドゲル化剤の使用。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
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EP10156371.6 | 2010-03-12 | ||
EP10156371 | 2010-03-12 | ||
PCT/US2011/028021 WO2011112887A1 (en) | 2010-03-12 | 2011-03-11 | Di-amido gellant for use in consumer product compositions |
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JP2013521402A JP2013521402A (ja) | 2013-06-10 |
JP5758412B2 true JP5758412B2 (ja) | 2015-08-05 |
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JP2012557268A Expired - Fee Related JP5758412B2 (ja) | 2010-03-12 | 2011-03-11 | 消費者製品組成物で使用するジアミドゲル化剤 |
JP2012557267A Expired - Fee Related JP5571202B2 (ja) | 2010-03-12 | 2011-03-11 | ジアミドゲル化剤を含む流体洗剤組成物及び製造方法 |
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JP2012557267A Expired - Fee Related JP5571202B2 (ja) | 2010-03-12 | 2011-03-11 | ジアミドゲル化剤を含む流体洗剤組成物及び製造方法 |
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US (3) | US8207107B2 (ja) |
EP (2) | EP2365051B1 (ja) |
JP (2) | JP5758412B2 (ja) |
AR (1) | AR080507A1 (ja) |
BR (2) | BR112012023033A2 (ja) |
CA (2) | CA2791251C (ja) |
MX (2) | MX2012010571A (ja) |
WO (2) | WO2011112887A1 (ja) |
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JP5571202B2 (ja) | 2014-08-13 |
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CA2791252A1 (en) | 2011-09-15 |
CA2791252C (en) | 2014-09-02 |
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CA2791251A1 (en) | 2011-09-15 |
JP2013521402A (ja) | 2013-06-10 |
AR080507A1 (es) | 2012-04-11 |
US8168579B2 (en) | 2012-05-01 |
CA2791251C (en) | 2014-08-12 |
EP2365051B1 (en) | 2015-11-11 |
US8207107B2 (en) | 2012-06-26 |
MX2012010572A (es) | 2012-10-09 |
BR112012023014A2 (pt) | 2016-05-31 |
MX2012010571A (es) | 2012-10-09 |
JP2013521401A (ja) | 2013-06-10 |
EP2365050A1 (en) | 2011-09-14 |
US8309507B2 (en) | 2012-11-13 |
EP2365051A1 (en) | 2011-09-14 |
WO2011112887A1 (en) | 2011-09-15 |
US20110224455A1 (en) | 2011-09-15 |
US20110220536A1 (en) | 2011-09-15 |
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