JP5695815B2 - 潤滑油組成物 - Google Patents
潤滑油組成物 Download PDFInfo
- Publication number
- JP5695815B2 JP5695815B2 JP2008201043A JP2008201043A JP5695815B2 JP 5695815 B2 JP5695815 B2 JP 5695815B2 JP 2008201043 A JP2008201043 A JP 2008201043A JP 2008201043 A JP2008201043 A JP 2008201043A JP 5695815 B2 JP5695815 B2 JP 5695815B2
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- Prior art keywords
- oil
- viscosity
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- base oil
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- Prior art date
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- 239000002199 base oil Substances 0.000 claims description 216
- 239000002480 mineral oil Substances 0.000 claims description 80
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- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 74
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- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 description 5
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- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 4
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- Lubricants (AREA)
Description
ノルマルパラフィンを含有する原料油について、水素化処理触媒を用いて水素化処理する第1工程と、
第1工程により得られる被処理物について、水素化脱ロウ触媒を用いて水素化脱ロウする第2工程と、
第2工程により得られる被処理物について、水素化精製触媒を用いて水素化精製する第3工程とを備える。
(ガスクロマトグラフィー条件)
カラム:液相無極性カラム(長さ25mm、内径0.3mmφ、液相膜厚さ0.1μm)昇温条件:50℃〜400℃(昇温速度:10℃/min)
キャリアガス:ヘリウム(線速度:40cm/min)
スプリット比:90/1
試料注入量:0.5μL(二硫化炭素で20倍に希釈した試料の注入量)
(I)100℃における動粘度が1.5mm2/s以上3.5mm2/s未満、より好ましくは2.0〜3.0mm2/sの鉱油系基油
(II)100℃における動粘度が3.0mm2/s以上4.5mm2/s未満、より好ましくは3.5〜4.1mm2/sの鉱油系基油
(III)100℃における動粘度が4.5〜20mm2/s、より好ましくは4.8〜11mm2/s、特に好ましくは5.5〜8.0mm2/sの鉱油系基油。
(IV)40℃における動粘度が6.0mm2/s以上12mm2/s未満、より好ましくは8.0〜12mm2/sの鉱油系基油
(V)40℃における動粘度が12mm2/s以上28mm2/s未満、より好ましくは13〜19mm2/sの鉱油系基油
(VI)40℃における動粘度が28〜50mm2/s、より好ましくは29〜45mm2/s、特に好ましくは30〜40mm2/sの鉱油系基油。
ρ=0.0025×kv100+0.816 (1)
[式中、kv100は鉱油系基油の100℃における動粘度(mm2/s)を示す。]
A=4.3×kv100+100 (2)
[式中、kv100は鉱油系基油の100℃における動粘度(mm2/s)を示す。]
(a)一価アルコールと一塩基酸とのエステル
(b)多価アルコールと一塩基酸とのエステル
(c)一価アルコールと多塩基酸とのエステル
(d)多価アルコールと多塩基酸とのエステル
(e)一価アルコールおよび多価アルコールの混合物と、多塩基酸との混合エステル
(f)多価アルコールと、一塩基酸および多塩基酸の混合物との混合エステル
(g)一価アルコールおよび多価アルコールの混合物と、一塩基酸および多塩基酸の混合物との混合エステル
(h)一価アルコールと不飽和一塩基酸とのエステルの重合物
有機モリブデン化合物としては、モリブデンジチオホスフェート、モリブデンジチオカーバメート等の硫黄を含有する有機モリブデン化合物あるいはモリブデン−アミン錯体、モリブデン−コハク酸イミド錯体、有機酸のモリブデン塩、アルコールのモリブデン塩など構成元素として硫黄を含まない有機モリブデン化合物を用いることができる。
表1に示す性状を有する基油1〜基油4およびエステル系基油(基油5)ならびに添加剤を用いて、表2に示す組成を有する潤滑油組成物を調製した。
(基油)
基油1:水素化分解/水素化異性化基油
基油2:水素化分解/水素化異性化基油
基油3:パラフィン系水素化分解基油
基油4:パラフィン系水素化分解基油
基油5:エステル系基油(アクリル酸エステルの重合物、100℃動粘度:700mm2/s、粘度指数:253)
(添加剤)
PMA−1:非分散型ポリメタクリレート(重量平均分子量:2万、PSSI:0)
PMA−2:非分散型ポリメタクリレート(重量平均分子量:2万、PSSI:0)
PKG−1:性能添加剤パッケージ
[原料ワックス]
溶剤精製基油を精製する工程において減圧蒸留で分離した留分を、フルフラールで溶剤抽出した後で水素化処理し、次いで、メチルエチルケトン−トルエン混合溶剤で溶剤脱ろうした。溶剤脱ろうの際に除去され、スラックワックスとして得られたワックス分(以下、「WAX1」という)の性状を表3に示す。
WAX1を原料油とし、水素化処理触媒を用いて水素化処理を行った。このとき、原料油中のノルマルパラフィンの分解率が10質量%以下となるように、反応温度および液空間速度を調整した。
実施例1〜2、比較例1〜6の各潤滑油組成物を用い、高温転がり試験機(1410rpm、120℃、3.7GPa)で疲労寿命試験を行い、L50(50%破損確率)を求めた。得られた結果を表2に示した。
Claims (3)
- 尿素アダクト値が0.8質量%以上2.5質量%以下であり且つ粘度指数が100以上である鉱油系基油と、
エステル系基油と、
潤滑油組成物全量基準で、1〜30質量%の粘度指数向上剤と、
を含有し、−30℃におけるBF粘度が1500mPa・s以下であることを特徴とする潤滑油組成物。 - 前記鉱油系基油が、ノルマルパラフィンを含有する原料油について、得られる被処理物の尿素アダクト値が0.8質量%以上2.5質量%以下であり且つ粘度指数が100以上となるように、ノルマルパラフィンを含有する原料油について、水素化処理触媒を用いて水素化処理する第1工程と、第1工程により得られる被処理物について、水素化脱ロウ触媒を用いて水素化脱ロウする第2工程と、第2工程により得られる被処理物について、水素化精製触媒を用いて水素化精製する第3工程と、を備える水素化分解/水素化異性化工程により得られた鉱油系基油であることを特徴とする、請求項1に記載の潤滑油組成物。
- 前記原料油が潤滑油基油の溶剤脱ろうによって得られるスラックワックスを50質量%以上含有することを特徴とする、請求項2に記載の潤滑油組成物。
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