JP5361709B2 - ヒュームドシリカ分散液 - Google Patents
ヒュームドシリカ分散液 Download PDFInfo
- Publication number
- JP5361709B2 JP5361709B2 JP2009508286A JP2009508286A JP5361709B2 JP 5361709 B2 JP5361709 B2 JP 5361709B2 JP 2009508286 A JP2009508286 A JP 2009508286A JP 2009508286 A JP2009508286 A JP 2009508286A JP 5361709 B2 JP5361709 B2 JP 5361709B2
- Authority
- JP
- Japan
- Prior art keywords
- fumed silica
- silica
- present
- dispersion
- silanized
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D17/00—Pigment pastes, e.g. for mixing in paints
- C09D17/004—Pigment pastes, e.g. for mixing in paints containing an inorganic pigment
- C09D17/007—Metal oxide
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y30/00—Nanotechnology for materials or surface science, e.g. nanocomposites
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09C—TREATMENT OF INORGANIC MATERIALS, OTHER THAN FIBROUS FILLERS, TO ENHANCE THEIR PIGMENTING OR FILLING PROPERTIES ; PREPARATION OF CARBON BLACK ; PREPARATION OF INORGANIC MATERIALS WHICH ARE NO SINGLE CHEMICAL COMPOUNDS AND WHICH ARE MAINLY USED AS PIGMENTS OR FILLERS
- C09C1/00—Treatment of specific inorganic materials other than fibrous fillers; Preparation of carbon black
- C09C1/28—Compounds of silicon
- C09C1/30—Silicic acid
- C09C1/3081—Treatment with organo-silicon compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/66—Additives characterised by particle size
- C09D7/67—Particle size smaller than 100 nm
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/66—Additives characterised by particle size
- C09D7/68—Particle size between 100-1000 nm
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/66—Additives characterised by particle size
- C09D7/69—Particle size larger than 1000 nm
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/64—Nanometer sized, i.e. from 1-100 nanometer
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/12—Surface area
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/19—Oil-absorption capacity, e.g. DBP values
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/36—Silica
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/04—Ingredients treated with organic substances
- C08K9/06—Ingredients treated with organic substances with silicon-containing compounds
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2991—Coated
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T428/00—Stock material or miscellaneous articles
- Y10T428/29—Coated or structually defined flake, particle, cell, strand, strand portion, rod, filament, macroscopic fiber or mass thereof
- Y10T428/2982—Particulate matter [e.g., sphere, flake, etc.]
- Y10T428/2991—Coated
- Y10T428/2993—Silicic or refractory material containing [e.g., tungsten oxide, glass, cement, etc.]
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Nanotechnology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Inorganic Chemistry (AREA)
- Composite Materials (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Physics & Mathematics (AREA)
- Paints Or Removers (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Silicon Compounds (AREA)
Description
BET表面積 m2/g: 25〜400
平均一次粒子サイズ nm: 5〜50
pH: 3〜10
炭素含有率 質量%: 0.1〜10
DBP価 %: <200
0.01μm〜1.5μmの範囲内の20質量%〜80質量%
1.5μm〜4.0μmの範囲内の2質量%〜80質量%。
0.2μm〜1.5μmの範囲内の60質量%〜95質量%
1.5μm〜3.5μmの範囲内の5質量%〜40質量%。
実施例1〜3において、シラン化された、構造的に改質されたヒュームドシリカのAerosil(登録商標)R9200を、公知の方法によって、クリアコート系中に取り込む。実施例4によって、シラン化された、構造的に改質されたヒュームドシリカを、本発明の分散液によって取り込む。
Dispers 652:Tego社製の分散剤
Macrynal SM 565:USBのSurface Specialties社製のアクリルコポリマー
Solvesso 100:Imperial Oil社製の芳香族混合物
BM:Getzmann社製のDispermat SL 5
*)粒ゲージ30μmは、使用できない塗料材料を意味する
**)Degussa AGの技術情報第1284号
***)Coulter LS230 Micro Volumeモジュールにおけるレーザー回折によって、試料を測定した。純粋なワニス系又は溶剤を測定媒体として導入し、かつ試料を数滴添加することによって行った。
****)Degussa AGの技術情報第1204号
Claims (4)
- シラン化された、構造的に改質されたシリカ、及び溶剤としてメトキシプロピルアセテートのみを含有することを特徴とする、クリアコート材料用のヒュームドシリカの分散液。
- さらに添加剤を含有することを特徴とする、請求項1に記載のヒュームドシリカの分散液。
- 請求項1に記載の分散液を、少なくとも1つのバインダーと混合することを特徴とする、溶剤系の塗料材料の製造方法。
- 少なくとも1つの硬化剤を添加することを特徴とする、請求項3に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102006020987.7 | 2006-05-04 | ||
DE102006020987A DE102006020987A1 (de) | 2006-05-04 | 2006-05-04 | Dispersion von pyrogen hergestelltem Siliciumdioxid |
PCT/EP2007/053370 WO2007128636A2 (en) | 2006-05-04 | 2007-04-05 | Fumed silica dispersion |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2009535469A JP2009535469A (ja) | 2009-10-01 |
JP5361709B2 true JP5361709B2 (ja) | 2013-12-04 |
Family
ID=38269028
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2009508286A Expired - Fee Related JP5361709B2 (ja) | 2006-05-04 | 2007-04-05 | ヒュームドシリカ分散液 |
Country Status (6)
Country | Link |
---|---|
US (1) | US7722714B2 (ja) |
EP (1) | EP2013292A2 (ja) |
JP (1) | JP5361709B2 (ja) |
CN (1) | CN101405351A (ja) |
DE (1) | DE102006020987A1 (ja) |
WO (1) | WO2007128636A2 (ja) |
Families Citing this family (23)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US8258206B2 (en) | 2006-01-30 | 2012-09-04 | Ashland Licensing And Intellectual Property, Llc | Hydrophobic coating compositions for drag reduction |
US20080221263A1 (en) | 2006-08-31 | 2008-09-11 | Subbareddy Kanagasabapathy | Coating compositions for producing transparent super-hydrophobic surfaces |
DE102007024095A1 (de) * | 2007-05-22 | 2008-11-27 | Evonik Degussa Gmbh | Hydrophobe pyrogen hergestellte Kieselsäure und Silikonkautschukmassen, enthaltend die pyrogene Kieselsäure |
EP2070992A1 (de) * | 2007-12-11 | 2009-06-17 | Evonik Degussa GmbH | Lacksysteme |
ATE556121T1 (de) * | 2008-04-02 | 2012-05-15 | Evonik Degussa Gmbh | Dispersion enthaltend hydrophobierte siliciumdioxidpartikel |
EP2145928B1 (de) * | 2008-07-18 | 2017-09-13 | Evonik Degussa GmbH | Dispersion von hydrophobierten Siliciumdioxidpartikeln und Granulat hiervon |
DE102008057524A1 (de) * | 2008-11-15 | 2010-05-20 | Basf Coatings Ag | Kratzfestbeschichtete Polycarbonate mit hoher Transparenz, Verfahren zu deren Herstellung und deren Verwendung |
US8147607B2 (en) | 2009-10-26 | 2012-04-03 | Ashland Licensing And Intellectual Property Llc | Hydrophobic self-cleaning coating compositions |
WO2011109302A2 (en) * | 2010-03-01 | 2011-09-09 | Cabot Corporation | Coating comprising multipopulation fumed silica particles |
ES2653617T3 (es) * | 2011-02-02 | 2018-02-08 | Ashland Licensing And Intellectual Property, Llc | Recubrimiento de gel resistente al rayado |
DE102011088787A1 (de) | 2011-12-16 | 2013-06-20 | Evonik Industries Ag | Siloxannitrone und deren Anwendung |
WO2017205636A1 (en) * | 2016-05-25 | 2017-11-30 | University Of Florida Research Foundation, Inc. | Texturized insecticidal formulation |
FR3055630B1 (fr) | 2016-09-08 | 2020-07-10 | Total Marketing Services | Composition bitumineuse pour enrobes a module eleve |
FR3055631B1 (fr) | 2016-09-08 | 2018-09-28 | Total Marketing Services | Bitume solide a temperature ambiante |
FR3055633B1 (fr) | 2016-09-08 | 2020-06-12 | Total Marketing Services | Granules de brai solides a temperature ambiante |
FR3055623B1 (fr) | 2016-09-08 | 2020-04-17 | Total Marketing Services | Liant clair solide a froid |
FR3055568B1 (fr) | 2016-09-08 | 2020-01-31 | Total Marketing Services | Procede de fabrication de materiau sous forme de granules utilisable comme liant routier ou liant d’etancheite et dispositif pour sa fabrication |
FR3059674B1 (fr) | 2016-12-07 | 2018-11-23 | Total Marketing Services | Bitume solide a temperature ambiante |
FR3059673B1 (fr) | 2016-12-07 | 2018-11-23 | Total Marketing Services | Liants solides |
FR3061190B1 (fr) | 2016-12-22 | 2022-05-27 | Total Marketing Services | Liant solide a temperature ambiante |
FR3061191B1 (fr) | 2016-12-22 | 2019-05-24 | Total Marketing Services | Composition d’asphalte coule pour la realisation de revetements |
EP3467052B1 (de) | 2017-10-06 | 2022-04-13 | Evonik Operations GmbH | Wässrige dispersion enthaltend siliziumdioxid und trimethyl 1,6-hexamethylendiamin |
IT201900025168A1 (it) * | 2019-12-20 | 2021-06-20 | Carcano Antonio S P A | Composizione, in particolare utilizzabile quale vernice di copertura di superfici di lastre o componenti |
Family Cites Families (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL246681A (ja) * | 1958-12-24 | |||
JPH06220326A (ja) * | 1993-01-25 | 1994-08-09 | Matsushita Electric Works Ltd | コーティング用組成物 |
JP2004285361A (ja) * | 1993-08-27 | 2004-10-14 | Asahi Glass Co Ltd | 含フッ素溶媒に分散されてなるオルガノゾルおよびその用途 |
JP3465810B2 (ja) * | 1996-10-01 | 2003-11-10 | 日本油脂Basfコーティングス株式会社 | 塗料組成物 |
JPH11343396A (ja) * | 1998-04-03 | 1999-12-14 | Kansai Paint Co Ltd | エポキシ基含有コロイド粒子有機溶剤液、エポキシ基含有コロイド粒子、このコロイド粒子を含む活性エネルギー線硬化型組成物及びそれを使用した被膜形成方法 |
JP4716621B2 (ja) * | 2001-08-09 | 2011-07-06 | 電気化学工業株式会社 | 高濃度シリカスラリー及びシリカスラリーの製造方法 |
DE10239425A1 (de) * | 2002-08-28 | 2004-03-11 | Degussa Ag | Lackformulierungen |
DE10239423A1 (de) * | 2002-08-28 | 2004-03-11 | Degussa Ag | Kieselsäure |
JP4044813B2 (ja) * | 2002-09-18 | 2008-02-06 | 電気化学工業株式会社 | 超微粉シリカ分散スラリーの製造方法 |
US7544726B2 (en) * | 2002-10-14 | 2009-06-09 | Akzo Nobel N.V. | Colloidal silica composition |
US7553888B2 (en) * | 2002-10-14 | 2009-06-30 | Akzo Nobel N.V. | Aqueous dispersion |
DE10330020A1 (de) * | 2003-07-03 | 2005-01-20 | Degussa Ag | Hochgefüllte Silan-Zubereitung |
DE10362060B4 (de) * | 2003-10-21 | 2009-07-09 | Altana Coatings & Sealants Gmbh | Verpackungsmaterial mit einer Barriereschicht für Gase |
EP1922154A4 (en) * | 2005-07-07 | 2013-07-31 | Arkema Inc | METHOD FOR REINFORCING A SPROUTS OXIDE SUBSTRATE WITH A WEATHERPROOF COATING |
-
2006
- 2006-05-04 DE DE102006020987A patent/DE102006020987A1/de not_active Withdrawn
-
2007
- 2007-04-05 CN CNA200780009726XA patent/CN101405351A/zh active Pending
- 2007-04-05 JP JP2009508286A patent/JP5361709B2/ja not_active Expired - Fee Related
- 2007-04-05 WO PCT/EP2007/053370 patent/WO2007128636A2/en active Application Filing
- 2007-04-05 US US12/299,081 patent/US7722714B2/en not_active Expired - Fee Related
- 2007-04-05 EP EP07727838A patent/EP2013292A2/en not_active Withdrawn
Also Published As
Publication number | Publication date |
---|---|
JP2009535469A (ja) | 2009-10-01 |
WO2007128636A2 (en) | 2007-11-15 |
EP2013292A2 (en) | 2009-01-14 |
DE102006020987A1 (de) | 2007-11-08 |
US20090120328A1 (en) | 2009-05-14 |
WO2007128636A3 (en) | 2008-01-31 |
CN101405351A (zh) | 2009-04-08 |
US7722714B2 (en) | 2010-05-25 |
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