JP4543504B2 - Dry methane fermentation method for organic waste - Google Patents
Dry methane fermentation method for organic waste Download PDFInfo
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- JP4543504B2 JP4543504B2 JP2000170827A JP2000170827A JP4543504B2 JP 4543504 B2 JP4543504 B2 JP 4543504B2 JP 2000170827 A JP2000170827 A JP 2000170827A JP 2000170827 A JP2000170827 A JP 2000170827A JP 4543504 B2 JP4543504 B2 JP 4543504B2
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- methane fermentation
- organic waste
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- dry methane
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/30—Fuel from waste, e.g. synthetic alcohol or diesel
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W10/00—Technologies for wastewater treatment
- Y02W10/20—Sludge processing
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W30/00—Technologies for solid waste management
- Y02W30/20—Waste processing or separation
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- Processing Of Solid Wastes (AREA)
- Treatment Of Sludge (AREA)
Description
【0001】
【発明の属する技術分野】
本発明は、畜産業、食品産業、製紙業等より発生する有機性廃棄物の乾式メタン発酵方法に係り、特に、これらの有機性廃棄物を高負荷で効率的に乾式メタン発酵処理してメタンガスとして再資源化すると共に、古紙や雑草等の乾式メタン発酵をも行える有機性廃棄物の乾式メタン発酵方法に関する。
【0002】
【従来の技術】
古紙、生ごみ、家畜糞尿などの有機性廃棄物をメタン発酵菌の作用で嫌気性分解するメタン発酵処理は、廃棄物を大幅に減容化すると共に、分解により得られるメタンガスを含むバイオガスを電気又は熱の形でエネルギー回収することができるという優れた利点を有する処理方法である。
【0003】
このメタン発酵法には、TS(全固形物)濃度3〜5%程度でメタン発酵する湿式メタン発酵法と、TS濃度15〜40%程度でメタン発酵する乾式メタン発酵法とがある。
【0004】
このうち、湿式メタン発酵法では、TS濃度が低いため、高負荷処理が困難であり、また、生ゴミや糞尿、古紙、下水汚泥等のTS濃度の高い有機物を処理するためには前処理工程として可溶化処理や希釈によってTS濃度を10%以下にする必要があった。
【0005】
これに対して、乾式メタン発酵法であれば、TS濃度の高い有機性廃棄物を複雑な前処理工程なしに高負荷で処理してバイオガスを得ることができる。
【0006】
【発明が解決しようとする課題】
しかしながら、乾式メタン発酵法では、TS濃度の高い有機性廃棄物を高負荷で処理するため、被処理物によっては窒素含有濃度が高くアンモニアが高濃度に発生して、メタン発酵菌の生育が阻害され、メタン発酵効率が低下したり、炭素源が少なく、メタン発酵の基質が不足してメタン発酵が進行せず、メタンガスを安定かつ効率的に回収することができないという不具合があった。
【0007】
本発明は上記従来の問題点を解決し、古紙、生ごみ、家畜糞尿、し尿、汚泥等の有機性廃棄物を乾式メタン発酵により高いメタン発酵効率にて高負荷処理することにより、メタンガスを安定かつ効率的に回収することができる有機性廃棄物の乾式メタン発酵方法を提供することを目的とする。
【0008】
【課題を解決するための手段】
本発明の有機性廃棄物の乾式メタン発酵方法は、有機性廃棄物をTS(全固形物)濃度20〜40%で乾式メタン発酵処理する方法において、該有機性廃棄物のC/N比が25〜250となるように該有機性廃棄物を調整することを特徴とする。
【0009】
C/N比が25〜250となるように有機性廃棄物を調整することにより、効率的な乾式メタン発酵処理を行うことができる。
【0010】
上記C/N比に調整するためには、繊維含有有機物を有機性廃棄物に添加するのが好ましく、特に、繊維含有有機物として紙(古紙)及び/又は草(雑草)を添加することにより、従来のメタン発酵では前処理が必要とされたこれらの廃棄物を前処理なしでメタン発酵処理することが可能となる。
【0011】
【発明の実施の形態】
以下に本発明の有機性廃棄物の乾式メタン発酵方法の実施の形態を図面を参照しながら詳細に説明する。
【0012】
図1は本発明の有機性廃棄物の乾式メタン発酵方法の実施の形態を示す系統図である。
【0013】
生ゴミ、家畜糞尿、下水処理場等から発生する汚泥などの有機性廃棄物を、要すれば破砕機等を用い直径5〜4cm或いはそれ以下に破砕した投入原料1を混合装置2に投入し、必要に応じて水や繊維含有有機物3を添加混合し、混合発酵原料を得、これを乾式メタン発酵槽6からの返送汚泥9と混合した混合物5を乾式メタン発酵槽6に送給する。
【0014】
本発明においては、この混合発酵原料のC/N比が25〜250、好ましくは25〜60となるように調整する。また、混合発酵原料のTS濃度は20〜40%、好ましくは20〜35%とする。
【0015】
C/N比が20未満ではメタン発酵の基質である炭素源が不足し、250を超えるような炭素過剰のものでは、別途窒素やリンを添加しなければ微生物による分解が困難である。特に、C/N比が60を超えると有機態炭素を資化する増殖速度の大きい酸生成菌がメタン発酵菌に優先してメタン発酵菌の生育が阻害されるため、C/N比は60以下、特に25〜60とするのが好ましい。
【0016】
また、TS濃度が20%未満では乾式メタン発酵による高負荷処理ができず、40%を超えると水分量が不足していずれの場合もメタン発酵効率が低下する場合がある。
【0017】
投入原料1は通常、下水汚泥や糞尿のように窒素過多なものであるため、混合装置2においてC/N比を調整する。C/N比の調整手段としては、投入原料1を加熱脱水し、脱アンモニア処理してC/N比を高くすることにより混合発酵原料のC/N比及びTS濃度を調整することができる。しかし、このような投入原料の前処理を行うと処理操作が複雑化し、また脱水濾液の処理も必要になるので好ましくなく、混合装置2に紙や藁、雑草などC/N比、TS濃度の両方が高い繊維含有有機物3もあわせて投入し、投入原料1と混合することにより混合発酵原料のC/N比を上記範囲に調整することができると共に、TS濃度も調整できる。
【0018】
一般に、汚泥や家畜糞尿等の有機性廃棄物は、上記TS濃度に対して若干固形物量が不足し、またC/Nが低い。これに対して紙(古紙)や草(雑草)は繊維を多く含む有機物であり、しかもC/N比が高い。紙はNを殆ど含まず従って、C/Nは著しく高く、草はC/Nが60〜100程度である。従って、TS濃度やC/N比の調整剤として適している。しかも、紙や草はセルロースなどの生物分解性の炭素源とリグニン、ヘミセルロース、灰分などの難分解性物質も含むため、これらを添加することにより、生物分解性物質が微生物の基質となり、また、難分解性物質が微生物担体として作用することで良好な乾式メタン発酵処理を行える。
【0019】
混合装置2には蒸気4の吹き込みを行って混合発酵原料と返送汚泥9との混合物5を50〜60℃に加温し、これを乾式メタン発酵槽6に投入し、嫌気条件下で乾式メタンを発酵させる。混合発酵原料はメタン生成菌を含む返送汚泥9と混合され、加温されているため、発酵槽6内の加温、攪拌操作は不要である。このため、発酵槽6内にはTS濃度15〜40%の高濃度の汚泥が保持され、10〜20kg−CODCCr/m3/dayの高負荷で乾式メタン発酵が行われる。
【0020】
発酵槽6に投入された混合発酵原料は発酵槽6内で嫌気性微生物により分解されて徐々にTS濃度が低下し、発酵槽6の下部へ移動し、引抜き汚泥7として引き抜かれる。1日当りの汚泥7の引き抜き量は槽内に保有される汚泥の1/4〜1倍、好ましくは1/3〜1/2倍で、このうち混合発酵原料からガス化した部分を除いた量(通常は混合発酵原料の90%程度)を余剰汚泥8として排出し、残りは返送汚泥9として混合装置2に供給し、混合発酵原料と混合する。
【0021】
このような本発明の方法によれば、畜産業、食品産業、製紙業等から排出される有機性廃棄物や、生ごみ等を効率的に処理してメタンガスとして再資源化することが可能となる。
【0022】
【実施例】
以下に実施例及び比較例を挙げて本発明をより具体的に説明する。
【0023】
試験1(実施例1)
図1に示す装置を用いてTS濃度20%、C/N比13の豚糞と生ゴミの混合物(生ゴミは直径5cmに破砕)の処理を行った。混合装置2において豚糞と生ゴミの混合物及び繊維含有有機物3として幅5mm程度に裁断した古紙を表1に示す割合で混合し、混合発酵原料のTS濃度及びC/N比を表1に示す値に調整した。これを31kg−混合発酵原料/t−返送汚泥となるように返送汚泥9と混合し、蒸気の吹き込みにより55℃に加温し、乾式メタン発酵槽6に投入し、下記条件で32日間連続して乾式メタン発酵槽処理し、このときのメタンガス発生量を調べた。表1に試験期間中のメタンガス発生量の平均値を示す。なお、発酵槽6内の温度は試験期間中、52〜55℃であった。
[処理条件]
発酵槽内汚泥量;約21t
投入原料 ;約600kg/day
余剰汚泥量 ;約550kg/day
返送汚泥量 ;約21t/day
【0024】
試験2(実施例2〜4、比較例1)
投入原料1をTS濃度26%、C/N比12の豚糞とし、試験1で用いた装置より規模が小さい試験装置を用い、下記に示す条件で30日間の連続処理を行った。投入原料と実験装置の大きさ及び試験期間以外は実施例1と同様とした。このときの古紙の添加量、混合発酵原料のTS濃度、C/N比、メタンガス発生量の平均値を表1に示す。
[処理条件]
発酵槽内汚泥量;約3.5kg
投入原料 ;約110g/day
余剰汚泥量 ;約100g/day
返送汚泥量 ;約3.5kg/day
【0025】
試験3(実施例5、比較例2)
投入原料1として2種類の古紙を用い、混合装置2において、TS濃度を調整したものを混合発酵原料とした他は試験2と同様の処理を行った。このときの混合発酵原料のTS濃度、C/N比、メタンガス発生量の平均値を表1に示す。
【0026】
【表1】
【0027】
表1より、被処理物のC/N比を25〜250、好ましくは25〜60とすることにより、効率的なメタン発酵処理を行えることがわかる。
【0028】
【発明の効果】
以上詳述した通り、本発明の有機性廃棄物の乾式メタン発酵方法によれば、生ごみ、家畜糞尿等の有機性廃棄物、更には古紙、雑草等を乾式メタン発酵により高いメタン発酵効率にて高負荷処理することにより、メタンガスを安定かつ効率的に回収することが可能とされる。
【図面の簡単な説明】
【図1】本発明の実施の形態を示す系統図である。
【符号の説明】
1 投入原料
2 混合装置
3 繊維含有有機物
4 蒸気
6 乾式メタン発酵槽
7 引抜汚泥
8 余剰汚泥
9 返送汚泥[0001]
BACKGROUND OF THE INVENTION
The present invention relates to a dry methane fermentation method for organic waste generated from the livestock industry, food industry, paper industry, etc., and in particular, these organic wastes are efficiently subjected to dry methane fermentation treatment with high load to produce methane gas. It is related with the dry methane fermentation method of the organic waste which can also carry out dry methane fermentation of waste paper, weeds, etc.
[0002]
[Prior art]
The methane fermentation process that anaerobically decomposes organic waste such as waste paper, food waste, and livestock manure by the action of methane fermentation bacteria greatly reduces the volume of waste, and biogas containing methane gas obtained by the decomposition. It is a processing method having an excellent advantage that energy can be recovered in the form of electricity or heat.
[0003]
This methane fermentation method includes a wet methane fermentation method in which methane fermentation is performed at a TS (total solids) concentration of about 3 to 5%, and a dry methane fermentation method in which methane fermentation is performed at a TS concentration of about 15 to 40%.
[0004]
Among these, the wet methane fermentation method has a low TS concentration, so it is difficult to carry out a high load treatment, and a pretreatment step is required to treat organic matter with a high TS concentration such as raw garbage, manure, waste paper, and sewage sludge. As a result, it was necessary to reduce the TS concentration to 10% or less by solubilization or dilution.
[0005]
On the other hand, if it is a dry-type methane fermentation method, a biogas can be obtained by processing an organic waste with a high TS concentration at a high load without a complicated pretreatment process.
[0006]
[Problems to be solved by the invention]
However, in the dry methane fermentation method, organic waste with a high TS concentration is treated with a high load, so depending on the material to be treated, the nitrogen content is high and ammonia is generated at a high concentration, which inhibits the growth of methane fermentation bacteria. However, the methane fermentation efficiency is reduced, the carbon source is low, the substrate for methane fermentation is insufficient, methane fermentation does not proceed, and methane gas cannot be recovered stably and efficiently.
[0007]
The present invention solves the above-mentioned conventional problems and stabilizes methane gas by treating organic waste such as waste paper, garbage, livestock manure, human waste, sludge, etc. with high methane fermentation efficiency by dry methane fermentation. An object of the present invention is to provide a method for dry methane fermentation of organic waste that can be recovered efficiently.
[0008]
[Means for Solving the Problems]
The method of dry methane fermentation of organic waste according to the present invention is a method of subjecting organic waste to dry methane fermentation at a TS (total solids) concentration of 20 to 40%, wherein the C / N ratio of the organic waste is The organic waste is adjusted to be 25 to 250.
[0009]
By adjusting the organic waste so that the C / N ratio is 25 to 250, an efficient dry methane fermentation treatment can be performed.
[0010]
In order to adjust to the C / N ratio, it is preferable to add fiber-containing organic matter to organic waste, and in particular, by adding paper (waste paper) and / or grass (weed) as fiber-containing organic matter, It becomes possible to perform methane fermentation treatment of these wastes, which require pretreatment in conventional methane fermentation, without pretreatment.
[0011]
DETAILED DESCRIPTION OF THE INVENTION
Embodiments of the organic waste dry methane fermentation method of the present invention will be described below in detail with reference to the drawings.
[0012]
FIG. 1 is a system diagram showing an embodiment of the organic waste dry methane fermentation method of the present invention.
[0013]
Feeding raw material 1 that has been crushed into organic waste such as raw garbage, livestock manure, sludge, etc. from sewage treatment plant, if necessary, using a crusher etc. If necessary, water and fiber-containing organic matter 3 are added and mixed to obtain a mixed fermentation raw material, and the mixture 5 mixed with the return sludge 9 from the dry methane fermentation tank 6 is fed to the dry methane fermentation tank 6.
[0014]
In the present invention, C / N ratio of the mixed fermentation material is 25 to 250, preferably adjusted to be 25 to 60. Also, TS concentration in the mixed fermentation material 20-40% preferably you 20 to 35%.
[0015]
When the C / N ratio is less than 20, the carbon source that is a substrate for methane fermentation is insufficient, and when the carbon excess exceeds 250, decomposition by microorganisms is difficult unless nitrogen or phosphorus is added separately. In particular, when the C / N ratio exceeds 60, acid-producing bacteria having a high growth rate that assimilate organic carbon are preferentially inhibited from growth of methane-fermenting bacteria. Therefore, the C / N ratio is 60 Hereinafter, it is particularly preferably 25 to 60.
[0016]
Moreover, if the TS concentration is less than 20%, high-load treatment by dry methane fermentation cannot be performed, and if it exceeds 40%, the amount of water is insufficient and the methane fermentation efficiency may be reduced in any case.
[0017]
Since the input raw material 1 is usually rich in nitrogen such as sewage sludge and manure, the
[0018]
In general, organic wastes such as sludge and livestock manure are slightly deficient in solids and have a low C / N ratio with respect to the TS concentration. On the other hand, paper (waste paper) and grass (weeds) are organic substances containing a lot of fibers and have a high C / N ratio. The paper contains almost no N, so the C / N is remarkably high and the grass has a C / N of about 60-100. Therefore, it is suitable as a regulator of TS concentration and C / N ratio. Moreover, since paper and grass also contain biodegradable carbon sources such as cellulose and refractory substances such as lignin, hemicellulose, and ash, by adding these, the biodegradable substance becomes a microbial substrate, A good dry methane fermentation process can be performed because a hardly decomposable substance acts as a microorganism carrier.
[0019]
Steam 4 is blown into the
[0020]
The mixed fermented raw material charged into the fermenter 6 is decomposed by anaerobic microorganisms in the fermenter 6 and gradually decreases in TS concentration, moves to the lower part of the fermenter 6, and is extracted as drawn sludge 7. The extraction amount of sludge 7 per day is 1/4 to 1 times, preferably 1/3 to 1/2 times the sludge retained in the tank, and the amount excluding the gasified portion from the mixed fermentation raw material (Normally, about 90% of the mixed fermentation raw material) is discharged as surplus sludge 8, and the remainder is supplied as return sludge 9 to the
[0021]
According to such a method of the present invention, it is possible to efficiently treat organic waste discharged from the livestock industry, food industry, paper industry, etc., garbage, etc., and recycle it as methane gas. Become.
[0022]
【Example】
Hereinafter, the present invention will be described more specifically with reference to Examples and Comparative Examples.
[0023]
Test 1 (Example 1)
Using the apparatus shown in FIG. 1, a mixture of pig feces and garbage having a TS concentration of 20% and a C / N ratio of 13 (food garbage was crushed to a diameter of 5 cm) was performed. In the
[Processing conditions]
Amount of sludge in the fermenter; approx. 21t
Input material: approx. 600 kg / day
Excess sludge amount: about 550kg / day
Return sludge volume: approx. 21t / day
[0024]
Test 2 (Examples 2 to 4, Comparative Example 1)
The input raw material 1 was pig feces having a TS concentration of 26% and a C / N ratio of 12, and a test apparatus having a smaller scale than the apparatus used in the test 1 was used, and continuous treatment was performed for 30 days under the following conditions. Example 1 was the same as in Example 1 except for the input materials, the size of the experimental apparatus, and the test period. Table 1 shows the amount of waste paper added, the TS concentration of the mixed fermentation material, the C / N ratio, and the average value of the amount of methane gas generated.
[Processing conditions]
Amount of sludge in the fermenter; about 3.5 kg
Input material: about 110 g / day
Excess sludge amount: approx. 100 g / day
Return sludge amount: about 3.5kg / day
[0025]
Test 3 (Example 5, Comparative Example 2)
The same treatment as in
[0026]
[Table 1]
[0027]
From Table 1, it is understood that an efficient methane fermentation treatment can be performed by setting the C / N ratio of the object to be treated to 25 to 250, preferably 25 to 60.
[0028]
【The invention's effect】
As described in detail above, according to the dry methane fermentation method for organic waste of the present invention, organic waste such as garbage, livestock manure, etc., as well as waste paper, weeds, etc., have high methane fermentation efficiency by dry methane fermentation. By carrying out high load processing, methane gas can be recovered stably and efficiently.
[Brief description of the drawings]
FIG. 1 is a system diagram showing an embodiment of the present invention.
[Explanation of symbols]
DESCRIPTION OF SYMBOLS 1 Input
Claims (3)
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CN110252763A (en) * | 2019-05-13 | 2019-09-20 | 江苏天楹环保能源成套设备有限公司 | A kind of rubbish from cooking dry type anaerobic fermentation system |
JP2022101095A (en) * | 2020-12-24 | 2022-07-06 | 株式会社サムズ | Methane fermentation system of organic waste |
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JP2005279411A (en) * | 2004-03-29 | 2005-10-13 | Kurita Water Ind Ltd | High-speed methane fermentation process of glycerol |
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JP4665693B2 (en) * | 2005-09-30 | 2011-04-06 | 栗田工業株式会社 | Method and apparatus for treating organic waste |
JP5564309B2 (en) * | 2010-03-31 | 2014-07-30 | 日立造船株式会社 | Method for preparing waste-derived biomass material |
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JP2019177333A (en) * | 2018-03-30 | 2019-10-17 | Jfeエンジニアリング株式会社 | Method for methane fermentation of organic waste |
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CN110252763A (en) * | 2019-05-13 | 2019-09-20 | 江苏天楹环保能源成套设备有限公司 | A kind of rubbish from cooking dry type anaerobic fermentation system |
JP2022101095A (en) * | 2020-12-24 | 2022-07-06 | 株式会社サムズ | Methane fermentation system of organic waste |
JP7209975B2 (en) | 2020-12-24 | 2023-01-23 | 株式会社サムズ | Organic waste methane fermentation system |
JP7468873B2 (en) | 2020-12-24 | 2024-04-16 | 株式会社サムズ | Methane fermentation system for organic waste |
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