JP2018507093A - 容器の内面上にコーティングされたコーティング層を作製するための方法及びそのような方法を用いて得られる容器 - Google Patents
容器の内面上にコーティングされたコーティング層を作製するための方法及びそのような方法を用いて得られる容器 Download PDFInfo
- Publication number
- JP2018507093A JP2018507093A JP2017527854A JP2017527854A JP2018507093A JP 2018507093 A JP2018507093 A JP 2018507093A JP 2017527854 A JP2017527854 A JP 2017527854A JP 2017527854 A JP2017527854 A JP 2017527854A JP 2018507093 A JP2018507093 A JP 2018507093A
- Authority
- JP
- Japan
- Prior art keywords
- container
- acid
- solution
- solvent
- mol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/001—General methods for coating; Devices therefor
- C03C17/003—General methods for coating; Devices therefor for hollow ware, e.g. containers
- C03C17/004—Coating the inside
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C17/00—Surface treatment of glass, not in the form of fibres or filaments, by coating
- C03C17/22—Surface treatment of glass, not in the form of fibres or filaments, by coating with other inorganic material
- C03C17/23—Oxides
- C03C17/25—Oxides by deposition from the liquid phase
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/16—Antifouling paints; Underwater paints
- C09D5/1656—Antifouling paints; Underwater paints characterised by the film-forming substance
- C09D5/1662—Synthetic film-forming substance
- C09D5/1675—Polyorganosiloxane-containing compositions
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1204—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material inorganic material, e.g. non-oxide and non-metallic such as sulfides, nitrides based compounds
- C23C18/122—Inorganic polymers, e.g. silanes, polysilazanes, polysiloxanes
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1225—Deposition of multilayers of inorganic material
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1229—Composition of the substrate
- C23C18/1233—Organic substrates
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1229—Composition of the substrate
- C23C18/1241—Metallic substrates
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/1229—Composition of the substrate
- C23C18/1245—Inorganic substrates other than metallic
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/125—Process of deposition of the inorganic material
- C23C18/1254—Sol or sol-gel processing
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/125—Process of deposition of the inorganic material
- C23C18/1262—Process of deposition of the inorganic material involving particles, e.g. carbon nanotubes [CNT], flakes
- C23C18/127—Preformed particles
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
- C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
- C23C18/125—Process of deposition of the inorganic material
- C23C18/1283—Control of temperature, e.g. gradual temperature increase, modulation of temperature
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B15/00—Layered products comprising a layer of metal
- B32B15/04—Layered products comprising a layer of metal comprising metal as the main or only constituent of a layer, which is next to another layer of the same or of a different material
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2217/00—Coatings on glass
- C03C2217/20—Materials for coating a single layer on glass
- C03C2217/21—Oxides
- C03C2217/213—SiO2
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C2218/00—Methods for coating glass
- C03C2218/10—Deposition methods
- C03C2218/11—Deposition methods from solutions or suspensions
- C03C2218/113—Deposition methods from solutions or suspensions by sol-gel processes
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Inorganic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Dispersion Chemistry (AREA)
- Nanotechnology (AREA)
- Wood Science & Technology (AREA)
- Surface Treatment Of Glass (AREA)
- Details Of Rigid Or Semi-Rigid Containers (AREA)
- Application Of Or Painting With Fluid Materials (AREA)
- Paints Or Removers (AREA)
Abstract
Description
−溶媒、水、アルコキシル基を含む分子前駆体及び触媒としての酸を含有する溶液が形成され、
−そのようにして得られた溶液が容器の内面の少なくとも一部に適用され(該溶液は、ゲル化の過程にある)、
−次いで、そのようにして適用された溶液が、焼成の前に、所定の温度及び所定の時間で乾燥させられ、
酸が硝酸又はクエン酸であることを特徴とする、方法を提供する。
−溶媒、水、アルコキシル基を含む分子前駆体及び触媒としての酸を含有する溶液が形成され、
−この溶液が、加水分解及び凝縮を開始するために混合され、
−そのようにして得られた溶液が容器の内面の少なくとも一部に適用され(該溶液は、加水分解及び凝縮の過程にある)、
−そのようにして適用された溶液が、所定の温度及び所定の時間で乾燥させられ、
酸が6mol/l以下の濃度のクエン酸であること、及び、前記濃度の酸の1単位体積に対して、溶液が1単位以上の体積の前駆体を含むことを特徴とする、方法をさらに提供する。
−乾燥が適用と同時に実施される;
−乾燥の後により高い所定の温度範囲内での焼成工程が続く;
−適用の前に、溶液に界面活性剤が添加される;
有利には、界面活性剤は、以下の構成要素の1つ及び/又はその他から抜粋される:ポリエチレングリコール、臭化セトリモニウム、陰イオン性界面活性剤、ポリエチレングリコールp−(1,1,3,3−テトラメチルブチル)フェニルエーテル;
−乾燥が、容器の内部を換気しながら、溶媒及び酸の沸点より高い温度で20分より長い時間実施される。
−硝酸の大気圧での沸点が121℃であり、クエン酸の大気圧での沸点が175℃であること;
−溶液が、2mol/l〜3mol/lの間、有利には2.5mol/lの硝酸濃度、又は0.02mol/l〜0.8mol/lの間、有利には0.189mol/lのクエン酸濃度を有すること;
−内面への溶液の適用の前に、抽出可能な材料が、R若しくはR1品質の水及び/又は0.5%〜1.2%の濃度に従ってNaClが添加された水と共にオートクレーブ内の少なくとも3つの通路によって、前記内面からあらかじめ抽出されること;
−内面への溶液の適用の前に、抽出可能な材料が、該当する分子の完全な溶解を可能にするのに十分な割合で水に溶解された塩化ナトリウム及び/又はグルコン酸カルシウムを含有する多湿雰囲気状態のオーブン内での処理によって、前記内面からあらかじめ抽出されること;
−容器がガラス製である場合、容器が、酸が硝酸である場合は450℃〜550℃の温度で、酸がクエン酸である場合は530℃〜600℃の温度で、20〜40分間焼成されること;
−容器がプラスチック製である場合、容器が、90℃〜150℃の温度で40〜60分間焼成されること;
−3−グリシドキシプロピルトリメトキシシラン又はオルトケイ酸テトラエチルが前駆体として使用されること;
−2−ブトキシエタノールが溶媒として使用されること(大気圧でのその沸点は172℃である);
−溶媒及び前駆体が、1測定単位の水と、硝酸については10mol/l〜18mol/lの間、有利には15.55mol/l、そして、クエン酸については0.5mol/l〜4mol/lの間、有利には1mol/lの濃度の2測定単位の酸と2測定単位の前駆体に対して7測定単位の溶媒の重量割合で、混合されること;
−SiO2、着色顔料、酸化セリウム及び/又は銀の組み合わせから抜粋される機能を実施するために好適な添加物が混合物に添加されること;
−成分の添加後、溶液が、15℃〜35℃の間の温度で25〜45分間の時間(t)混合されること。
−前記内面の少なくとも一部へのコーティング溶液の適用の工程、過剰なコーティング生成物の排出の工程及び生成物の焼成工程の連続工程が少なくとも3回繰り返される;
−溶媒、酸触媒、水、次に分子前駆体が、順番に連続的に混合される;
−プラズマ雰囲気での処理があらかじめ実施される。
Claims (22)
- ヒト及び/動物と生体適合性のある製品を含有するのに適したガラス製又はプラスチック製の容器の内面を覆う層の製造のための方法であって、
−溶媒、水、アルコキシル基を含む分子前駆体及び触媒としての酸を含有する溶液を形成し、
−加水分解及び凝縮を開始させるためにその溶液を混ぜ合わせ、
−そのようにして得られた溶液を該容器の内面の少なくとも一部分に適用し、該溶液は加水分解及び凝縮中であり、
−そのようにして適用された該溶液が所定の温度で所定の時間にわたり乾燥される方法であって、
該酸が6mol/L以下の濃度のクエン酸であることと、1単位量の酸に対して該溶液が1単位以上の前駆体量を含むことを特徴とする方法。 - 該乾燥が、該適用と同時に実施されることを特徴とする、請求項1記載の方法。
- 該乾燥の後に、より高い所定の温度範囲内での焼成工程が続くことを特徴とする、先行する請求項のうちの一項記載の方法。
- 適用前に該溶液に界面活性剤を添加することを特徴とする、先行する請求項のうちの一項記載の方法。
- 該界面活性剤が、ポリエチレングリコール及び/又は臭化セチルトリメチルアンモニウム及び/又は陰イオン性界面活性剤及び/又はポリエチレングリコール・p−(1,1,3,3−テトラメチルブチル)−フェニルエーテルから選択されることを特徴とする、請求項4記載の方法。
- 該容器の内部を換気しながら該溶媒及び該酸の沸点より高い温度で20分を超える時間にわたり乾燥することを特徴とする、先行する請求項のうちの一項記載の方法。
- 該選択溶媒が、該酸の沸点に近い沸点を有することを特徴とする、先行する請求項のうちの一項記載の方法。
- 該溶液が0.02mol/L〜0.8mol/Lのクエン酸濃度を有することを特徴とする、先行する請求項のうちの一項記載の方法。
- 該内面へ該溶液を適用する前にあらかじめ、R又はR1水質の水及び/又は0.5%〜1.2%の濃度のNaCl充填水を用いたオートクレーブに少なくとも3回通すことにより、抽出可能な物質を前記内面から抽出することを特徴とする、先行する請求項のうちの一項記載の方法。
- 該内面に該溶液を適用する前にあらかじめ、保湿器内において関連分子の完全な溶解を可能にするのに十分な比率で水に溶解された塩化ナトリウム及び/又はグルコン酸カルシウムを含有する多湿雰囲気で処理することにより、抽出可能な物質を前記内面から抽出することを特徴とする、請求項1〜4のうちの一項記載の方法。
- 該容器がガラス製のものである場合、該酸が硝酸であるときは450°〜550℃で、該酸がクエン酸であるときは530°〜600℃で20〜40分の時間にわたり該容器を焼成することを特徴とする、請求項3記載の方法。
- 該容器がプラスチック製のものである場合、90°〜150℃の温度で40〜60分にわたり該容器を焼成することを特徴とする、請求項3記載の方法。
- 前駆体として3−グリシドキシプロピルトリメトキシシラン又はオルトケイ酸テトラエチルが使用されることを特徴とする、先行する請求項のうちの一項記載の方法。
- 溶媒として2−ブトキシエタノールが使用されることを特徴とする、先行する請求項のうちの一項記載の方法。
- 1測定単位の水に対して7測定単位の溶媒、0.5mol/L〜4mol/L濃度の2測定単位の酸及び2測定単位の前駆体の重量比で該溶媒と該前駆体とを混合することを特徴とする、先行する請求項のうちの一項記載の方法。
- SiO2、着色顔料、酸化セリウム及び/又は銀の組み合わせから選択される機能を実施するのに適合した添加物が該混合物に添加されることを特徴とする、先行する請求項のうちの一項記載の方法。
- 該成分添加後に、25〜45分の時間tにわたり15°〜35℃の温度で混合することを特徴とする、先行する請求項のうちの一項記載の方法。
- 前記内面の少なくとも一部分に該コーティング液体を適用し、過剰な該コーティング生成物を排出し、該生成物を乾燥する連続工程が少なくとも3回繰り返されることを特徴とする、先行する請求項のうちの一項記載の方法。
- 順に該溶媒、該酸性触媒、該水、次に該分子前駆体が連続的に混合されることを特徴とする、先行する請求項のうちの一項記載の方法。
- プラズマ雰囲気での処理があらかじめ実行されることを特徴とする、先行する請求項のうちの一項記載の方法。
- ヒト及び/又は動物と生体適合性のある製品を含有するのに適した空洞の境界を定める壁を含むガラス製又はプラスチック製の容器において、前記壁が前記空洞と向き合う内面を有し、前記内面の少なくとも一部分が、溶媒、水、アルコキシ基を含む分子前駆体及び触媒としての酸を含有する溶液から得られる凝固ゲルにより覆われる容器であって、該酸がクエン酸であることを特徴とする容器。
- 該溶液がSiO2、着色顔料、酸化セリウム及び/又は銀を含むことを特徴とする、請求項20記載の容器。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR1461531A FR3028778B1 (fr) | 2014-11-26 | 2014-11-26 | Procede de fabrication d'une couche de revetement de la face interne d'un recipient et recipient obtenu avec un tel procede |
FR1461531 | 2014-11-26 | ||
PCT/FR2015/053241 WO2016083755A2 (fr) | 2014-11-26 | 2015-11-26 | Procede de fabrication d'une couche de revetement de la face interne d'un recipient et recipient obtenu avec un tel procede |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2018507093A true JP2018507093A (ja) | 2018-03-15 |
JP2018507093A5 JP2018507093A5 (ja) | 2018-12-06 |
Family
ID=52692776
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2017527854A Pending JP2018507093A (ja) | 2014-11-26 | 2015-11-26 | 容器の内面上にコーティングされたコーティング層を作製するための方法及びそのような方法を用いて得られる容器 |
Country Status (6)
Country | Link |
---|---|
US (1) | US20170327414A1 (ja) |
EP (2) | EP3561150A1 (ja) |
JP (1) | JP2018507093A (ja) |
FR (1) | FR3028778B1 (ja) |
PL (1) | PL3224387T3 (ja) |
WO (1) | WO2016083755A2 (ja) |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR3143388A1 (fr) * | 2022-12-15 | 2024-06-21 | Wheaton Pintura E Beneficiamento De Vidros Ltda | Méthode de peinture interne |
Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4385086A (en) * | 1978-12-07 | 1983-05-24 | Tokyo Ohka Kogyo Kabushiki Kaisha | Method for preventing leaching of contaminants from solid surfaces |
JPH08500771A (ja) * | 1993-06-21 | 1996-01-30 | エルフ アトケム ノース アメリカ インコーポレイテッド | 架橋可能なシランにより強化された脆性酸化物支持体 |
JP2006130889A (ja) * | 2004-11-09 | 2006-05-25 | National Institute Of Advanced Industrial & Technology | 透明無機多孔体被膜およびその製造方法 |
JP2008519144A (ja) * | 2004-11-03 | 2008-06-05 | ジョンソンディバーシー・インコーポレーテッド | リサイクル用容器の洗浄方法 |
WO2009116300A1 (ja) * | 2008-03-21 | 2009-09-24 | 大和特殊硝子株式会社 | 低アルカリガラス容器の製造方法 |
US20130019932A1 (en) * | 2011-07-18 | 2013-01-24 | Gwangju Institute Of Science And Technology | Nanostructure Array Substrate, Method for Fabricating the Same and Dye-Sensitized Solar Cell Using the Same |
WO2013065801A1 (ja) * | 2011-11-04 | 2013-05-10 | 旭硝子株式会社 | 低反射膜付き物品の製造方法 |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2886309B1 (fr) * | 2005-05-31 | 2007-08-17 | Airbus France Sas | Sol pour le revetement par voie sol-gel d'une surface et procede de revetement par voie sol-gel le mettant en oeuvre |
DE102007043650A1 (de) * | 2007-09-13 | 2009-04-02 | Siemens Ag | Verfahren zur Verbesserung der Eigenschaften von Beschichtungen |
FR2939615B1 (fr) * | 2008-06-16 | 2015-09-25 | Courval Verreries | Procede de decoration d'un flacon transparent ou translucide |
FR2935594B1 (fr) * | 2008-09-10 | 2012-01-20 | Oreal | Recipients revetus par depot d'un sol-gel sur leur surface interne |
DE102008062881B4 (de) * | 2008-12-16 | 2021-04-08 | Schott Ag | Verfahren zur Herstellung eines hohlen Glasformkörpers |
FR2944007B1 (fr) * | 2009-04-03 | 2012-06-08 | Sgd Sa | Procede de fabrication d'un recipient en verre et recipient correspondant. |
DE102010007147A1 (de) * | 2010-02-05 | 2011-08-11 | Eckart GmbH, 91235 | Mit SiO2 beschichtete Metalleffektpigmente, Verfahren zur Herstellung dieser Metalleffektpigmente und Verwendung |
US8389052B2 (en) * | 2010-03-30 | 2013-03-05 | Toyo Glass Co., Ltd. | Method for treating inside surface of glass container and glass container |
KR101514120B1 (ko) * | 2010-08-18 | 2015-04-21 | 에스디씨 테크놀로지스 인코포레이티드 | 증기서림 방지 오르가노실록산 코팅 조성물 및 코팅 |
-
2014
- 2014-11-26 FR FR1461531A patent/FR3028778B1/fr active Active
-
2015
- 2015-11-26 US US15/529,323 patent/US20170327414A1/en not_active Abandoned
- 2015-11-26 EP EP19172851.8A patent/EP3561150A1/fr not_active Withdrawn
- 2015-11-26 PL PL15808757T patent/PL3224387T3/pl unknown
- 2015-11-26 EP EP15808757.7A patent/EP3224387B1/fr active Active
- 2015-11-26 WO PCT/FR2015/053241 patent/WO2016083755A2/fr active Application Filing
- 2015-11-26 JP JP2017527854A patent/JP2018507093A/ja active Pending
Patent Citations (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4385086A (en) * | 1978-12-07 | 1983-05-24 | Tokyo Ohka Kogyo Kabushiki Kaisha | Method for preventing leaching of contaminants from solid surfaces |
JPH08500771A (ja) * | 1993-06-21 | 1996-01-30 | エルフ アトケム ノース アメリカ インコーポレイテッド | 架橋可能なシランにより強化された脆性酸化物支持体 |
JP2008519144A (ja) * | 2004-11-03 | 2008-06-05 | ジョンソンディバーシー・インコーポレーテッド | リサイクル用容器の洗浄方法 |
JP2006130889A (ja) * | 2004-11-09 | 2006-05-25 | National Institute Of Advanced Industrial & Technology | 透明無機多孔体被膜およびその製造方法 |
WO2009116300A1 (ja) * | 2008-03-21 | 2009-09-24 | 大和特殊硝子株式会社 | 低アルカリガラス容器の製造方法 |
US20130019932A1 (en) * | 2011-07-18 | 2013-01-24 | Gwangju Institute Of Science And Technology | Nanostructure Array Substrate, Method for Fabricating the Same and Dye-Sensitized Solar Cell Using the Same |
WO2013065801A1 (ja) * | 2011-11-04 | 2013-05-10 | 旭硝子株式会社 | 低反射膜付き物品の製造方法 |
Non-Patent Citations (1)
Title |
---|
上部隆男 他3名: "ゾル−ゲル法によるガラスコーティング膜の作製", 東京都立工業技術センター研究報告, vol. 第22号, JPN6020030654, 1 March 1993 (1993-03-01), pages 57 - 60, ISSN: 0004335767 * |
Also Published As
Publication number | Publication date |
---|---|
EP3224387A2 (fr) | 2017-10-04 |
EP3561150A1 (fr) | 2019-10-30 |
WO2016083755A2 (fr) | 2016-06-02 |
US20170327414A1 (en) | 2017-11-16 |
WO2016083755A3 (fr) | 2016-07-21 |
FR3028778A1 (fr) | 2016-05-27 |
PL3224387T3 (pl) | 2019-11-29 |
EP3224387B1 (fr) | 2019-05-08 |
FR3028778B1 (fr) | 2019-04-12 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
EP2753593B1 (en) | Colouring solution for selectively treating the surface of dental ceramic and related methods | |
JP5634676B2 (ja) | 水で希釈可能なゾルゲル組成物 | |
US20190292097A1 (en) | Method For The Production of a Coating For The Inner Surface of a Receptacle, and Receptacle Obtained by a Method of Said Type | |
EP2776381B1 (en) | Method for selectively treating the surface of dental ceramic | |
JP2018507093A (ja) | 容器の内面上にコーティングされたコーティング層を作製するための方法及びそのような方法を用いて得られる容器 | |
JP2017512173A (ja) | ガラスフラスコの内表面を不動態化する方法及び装置、並びにこのような方法によって得られるフラスコ | |
CN105709216B (zh) | 一种类人胶原蛋白口腔粘膜修复液 | |
JPS5950188B2 (ja) | ガラス容器の擦り傷遮蔽用組成物 | |
CN109562984A (zh) | 在容器和相关设备的表面形成阻隔涂层的方法 | |
JPH06240174A (ja) | 膜形成用塗布液および塗料組成物 | |
US20190202732A1 (en) | Method for the production of a layer or a pattern for coating the inner surface of a receptacle, and receptacle obtained by a method of said type | |
US20170326586A1 (en) | Method and device for coating the inner surface of a container and container obtained with such a method | |
CN107406262A (zh) | 甲基甲硅烷基衍生的二氧化硅颗粒、胶体、其制备方法和包含其的套组 | |
TWI774263B (zh) | 次氯酸組合物及其應用 | |
TWI682010B (zh) | 被膜形成用之塗佈液及其製造方法、以及附被膜基材之製造方法 | |
JP6077958B2 (ja) | 歯科用前処理材組成物 | |
US20030205169A1 (en) | Inorganic film-forming coating composition, preparation method thereof and inorganic film-forming method | |
JPS6021936B2 (ja) | ガラス成形品の表面処理方法 | |
US20190118220A1 (en) | Method for the Production of a Layer for Coating the Plastic Inner Surface of a Receptacle, and Receptacle Obtained by a Method of Said Type | |
IE53173B1 (en) | Clear aluminium oxide solutions and glasses | |
JP2018507093A5 (ja) | ||
JPS62227965A (ja) | 素材処理方法 | |
JPH0610094B2 (ja) | ガラス容器の擦り傷遮蔽剤 | |
JP2937358B2 (ja) | ホーロー製品及びその製造方法 | |
JP2000335941A (ja) | ガラス物品 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20181019 |
|
A621 | Written request for application examination |
Free format text: JAPANESE INTERMEDIATE CODE: A621 Effective date: 20181019 |
|
A977 | Report on retrieval |
Free format text: JAPANESE INTERMEDIATE CODE: A971007 Effective date: 20190912 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20190924 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20191211 |
|
A601 | Written request for extension of time |
Free format text: JAPANESE INTERMEDIATE CODE: A601 Effective date: 20200210 |
|
A521 | Request for written amendment filed |
Free format text: JAPANESE INTERMEDIATE CODE: A523 Effective date: 20200323 |
|
A131 | Notification of reasons for refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A131 Effective date: 20200901 |
|
A02 | Decision of refusal |
Free format text: JAPANESE INTERMEDIATE CODE: A02 Effective date: 20210413 |