JP2014208636A - 付け睫接着剤 - Google Patents
付け睫接着剤 Download PDFInfo
- Publication number
- JP2014208636A JP2014208636A JP2014066179A JP2014066179A JP2014208636A JP 2014208636 A JP2014208636 A JP 2014208636A JP 2014066179 A JP2014066179 A JP 2014066179A JP 2014066179 A JP2014066179 A JP 2014066179A JP 2014208636 A JP2014208636 A JP 2014208636A
- Authority
- JP
- Japan
- Prior art keywords
- adhesive
- component
- eyeliner
- film
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
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- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- 239000000391 magnesium silicate Substances 0.000 description 1
- 229910052919 magnesium silicate Inorganic materials 0.000 description 1
- 235000019792 magnesium silicate Nutrition 0.000 description 1
- 235000019359 magnesium stearate Nutrition 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 229940049920 malate Drugs 0.000 description 1
- 150000004701 malic acid derivatives Chemical class 0.000 description 1
- 239000000845 maltitol Substances 0.000 description 1
- 235000010449 maltitol Nutrition 0.000 description 1
- VQHSOMBJVWLPSR-WUJBLJFYSA-N maltitol Chemical compound OC[C@H](O)[C@@H](O)[C@@H]([C@H](O)CO)O[C@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O VQHSOMBJVWLPSR-WUJBLJFYSA-N 0.000 description 1
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- 239000001923 methylcellulose Substances 0.000 description 1
- 229960002900 methylcellulose Drugs 0.000 description 1
- 235000010981 methylcellulose Nutrition 0.000 description 1
- 239000004200 microcrystalline wax Substances 0.000 description 1
- 235000019808 microcrystalline wax Nutrition 0.000 description 1
- 230000003020 moisturizing effect Effects 0.000 description 1
- 235000013379 molasses Nutrition 0.000 description 1
- 239000001788 mono and diglycerides of fatty acids Substances 0.000 description 1
- RZRNAYUHWVFMIP-UHFFFAOYSA-N monoelaidin Natural products CCCCCCCCC=CCCCCCCCC(=O)OCC(O)CO RZRNAYUHWVFMIP-UHFFFAOYSA-N 0.000 description 1
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- 239000003345 natural gas Substances 0.000 description 1
- SLCVBVWXLSEKPL-UHFFFAOYSA-N neopentyl glycol Chemical compound OCC(C)(C)CO SLCVBVWXLSEKPL-UHFFFAOYSA-N 0.000 description 1
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- 229920001778 nylon Polymers 0.000 description 1
- HMMGMWAXVFQUOA-UHFFFAOYSA-N octamethylcyclotetrasiloxane Chemical compound C[Si]1(C)O[Si](C)(C)O[Si](C)(C)O[Si](C)(C)O1 HMMGMWAXVFQUOA-UHFFFAOYSA-N 0.000 description 1
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- 235000014593 oils and fats Nutrition 0.000 description 1
- ZQPPMHVWECSIRJ-KTKRTIGZSA-N oleic acid Chemical compound CCCCCCCC\C=C/CCCCCCCC(O)=O ZQPPMHVWECSIRJ-KTKRTIGZSA-N 0.000 description 1
- 229940055577 oleyl alcohol Drugs 0.000 description 1
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- 239000008385 outer phase Substances 0.000 description 1
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- DXGLGDHPHMLXJC-UHFFFAOYSA-N oxybenzone Chemical compound OC1=CC(OC)=CC=C1C(=O)C1=CC=CC=C1 DXGLGDHPHMLXJC-UHFFFAOYSA-N 0.000 description 1
- 229960001173 oxybenzone Drugs 0.000 description 1
- 125000006353 oxyethylene group Chemical group 0.000 description 1
- RVTZCBVAJQQJTK-UHFFFAOYSA-N oxygen(2-);zirconium(4+) Chemical compound [O-2].[O-2].[Zr+4] RVTZCBVAJQQJTK-UHFFFAOYSA-N 0.000 description 1
- FJKROLUGYXJWQN-UHFFFAOYSA-N papa-hydroxy-benzoic acid Natural products OC(=O)C1=CC=C(O)C=C1 FJKROLUGYXJWQN-UHFFFAOYSA-N 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- BPHQIXJDBIHMLT-UHFFFAOYSA-N perfluorodecane Chemical compound FC(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F BPHQIXJDBIHMLT-UHFFFAOYSA-N 0.000 description 1
- YVBBRRALBYAZBM-UHFFFAOYSA-N perfluorooctane Chemical compound FC(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F YVBBRRALBYAZBM-UHFFFAOYSA-N 0.000 description 1
- 239000010702 perfluoropolyether Substances 0.000 description 1
- 229940066842 petrolatum Drugs 0.000 description 1
- 229960005323 phenoxyethanol Drugs 0.000 description 1
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 description 1
- 239000000419 plant extract Substances 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
- 229920001495 poly(sodium acrylate) polymer Polymers 0.000 description 1
- 229920000768 polyamine Polymers 0.000 description 1
- 229920001083 polybutene Polymers 0.000 description 1
- 230000000379 polymerizing effect Effects 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 238000010526 radical polymerization reaction Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 229960004889 salicylic acid Drugs 0.000 description 1
- 210000002374 sebum Anatomy 0.000 description 1
- HBMJWWWQQXIZIP-UHFFFAOYSA-N silicon carbide Chemical compound [Si+]#[C-] HBMJWWWQQXIZIP-UHFFFAOYSA-N 0.000 description 1
- 229910010271 silicon carbide Inorganic materials 0.000 description 1
- 229920002545 silicone oil Polymers 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000000344 soap Substances 0.000 description 1
- 235000010413 sodium alginate Nutrition 0.000 description 1
- 239000000661 sodium alginate Substances 0.000 description 1
- 229940005550 sodium alginate Drugs 0.000 description 1
- 239000011780 sodium chloride Substances 0.000 description 1
- 229940010747 sodium hyaluronate Drugs 0.000 description 1
- 239000001540 sodium lactate Substances 0.000 description 1
- 229940005581 sodium lactate Drugs 0.000 description 1
- 235000011088 sodium lactate Nutrition 0.000 description 1
- NNMHYFLPFNGQFZ-UHFFFAOYSA-M sodium polyacrylate Chemical compound [Na+].[O-]C(=O)C=C NNMHYFLPFNGQFZ-UHFFFAOYSA-M 0.000 description 1
- YWIVKILSMZOHHF-QJZPQSOGSA-N sodium;(2s,3s,4s,5r,6r)-6-[(2s,3r,4r,5s,6r)-3-acetamido-2-[(2s,3s,4r,5r,6r)-6-[(2r,3r,4r,5s,6r)-3-acetamido-2,5-dihydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-2-carboxy-4,5-dihydroxyoxan-3-yl]oxy-5-hydroxy-6-(hydroxymethyl)oxan-4-yl]oxy-3,4,5-trihydroxyoxane-2- Chemical compound [Na+].CC(=O)N[C@H]1[C@H](O)O[C@H](CO)[C@@H](O)[C@@H]1O[C@H]1[C@H](O)[C@@H](O)[C@H](O[C@H]2[C@@H]([C@@H](O[C@H]3[C@@H]([C@@H](O)[C@H](O)[C@H](O3)C(O)=O)O)[C@H](O)[C@@H](CO)O2)NC(C)=O)[C@@H](C(O)=O)O1 YWIVKILSMZOHHF-QJZPQSOGSA-N 0.000 description 1
- 235000019337 sorbitan trioleate Nutrition 0.000 description 1
- 229960000391 sorbitan trioleate Drugs 0.000 description 1
- 239000000600 sorbitol Substances 0.000 description 1
- 235000013599 spices Nutrition 0.000 description 1
- 229940032094 squalane Drugs 0.000 description 1
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- 239000010935 stainless steel Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 235000000346 sugar Nutrition 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- BDHFUVZGWQCTTF-UHFFFAOYSA-M sulfonate Chemical compound [O-]S(=O)=O BDHFUVZGWQCTTF-UHFFFAOYSA-M 0.000 description 1
- 238000004381 surface treatment Methods 0.000 description 1
- 239000000454 talc Substances 0.000 description 1
- 229910052623 talc Inorganic materials 0.000 description 1
- XOAAWQZATWQOTB-UHFFFAOYSA-N taurine Chemical class NCCS(O)(=O)=O XOAAWQZATWQOTB-UHFFFAOYSA-N 0.000 description 1
- TUNFSRHWOTWDNC-HKGQFRNVSA-N tetradecanoic acid Chemical compound CCCCCCCCCCCCC[14C](O)=O TUNFSRHWOTWDNC-HKGQFRNVSA-N 0.000 description 1
- 238000005979 thermal decomposition reaction Methods 0.000 description 1
- AOBORMOPSGHCAX-DGHZZKTQSA-N tocofersolan Chemical compound OCCOC(=O)CCC(=O)OC1=C(C)C(C)=C2O[C@](CCC[C@H](C)CCC[C@H](C)CCCC(C)C)(C)CCC2=C1C AOBORMOPSGHCAX-DGHZZKTQSA-N 0.000 description 1
- 229960000984 tocofersolan Drugs 0.000 description 1
- 125000000647 trehalose group Chemical group 0.000 description 1
- VLPFTAMPNXLGLX-UHFFFAOYSA-N trioctanoin Chemical compound CCCCCCCC(=O)OCC(OC(=O)CCCCCCC)COC(=O)CCCCCCC VLPFTAMPNXLGLX-UHFFFAOYSA-N 0.000 description 1
- UJMBCXLDXJUMFB-UHFFFAOYSA-K trisodium;5-oxo-1-(4-sulfonatophenyl)-4-[(4-sulfonatophenyl)diazenyl]-4h-pyrazole-3-carboxylate Chemical compound [Na+].[Na+].[Na+].[O-]C(=O)C1=NN(C=2C=CC(=CC=2)S([O-])(=O)=O)C(=O)C1N=NC1=CC=C(S([O-])(=O)=O)C=C1 UJMBCXLDXJUMFB-UHFFFAOYSA-K 0.000 description 1
- 235000013799 ultramarine blue Nutrition 0.000 description 1
- 239000006097 ultraviolet radiation absorber Substances 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 229940088594 vitamin Drugs 0.000 description 1
- 239000011782 vitamin Substances 0.000 description 1
- 229930003231 vitamin Natural products 0.000 description 1
- 235000013343 vitamin Nutrition 0.000 description 1
- 239000000341 volatile oil Substances 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 229940118846 witch hazel Drugs 0.000 description 1
- XOOUIPVCVHRTMJ-UHFFFAOYSA-L zinc stearate Chemical compound [Zn+2].CCCCCCCCCCCCCCCCCC([O-])=O.CCCCCCCCCCCCCCCCCC([O-])=O XOOUIPVCVHRTMJ-UHFFFAOYSA-L 0.000 description 1
- UHVMMEOXYDMDKI-JKYCWFKZSA-L zinc;1-(5-cyanopyridin-2-yl)-3-[(1s,2s)-2-(6-fluoro-2-hydroxy-3-propanoylphenyl)cyclopropyl]urea;diacetate Chemical compound [Zn+2].CC([O-])=O.CC([O-])=O.CCC(=O)C1=CC=C(F)C([C@H]2[C@H](C2)NC(=O)NC=2N=CC(=CC=2)C#N)=C1O UHVMMEOXYDMDKI-JKYCWFKZSA-L 0.000 description 1
- 229910001928 zirconium oxide Inorganic materials 0.000 description 1
- 239000004711 α-olefin Substances 0.000 description 1
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/60—Sugars; Derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q1/00—Make-up preparations; Body powders; Preparations for removing make-up
- A61Q1/02—Preparations containing skin colorants, e.g. pigments
- A61Q1/10—Preparations containing skin colorants, e.g. pigments for eyes, e.g. eyeliner, mascara
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/04—Non-macromolecular additives inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09J—ADHESIVES; NON-MECHANICAL ASPECTS OF ADHESIVE PROCESSES IN GENERAL; ADHESIVE PROCESSES NOT PROVIDED FOR ELSEWHERE; USE OF MATERIALS AS ADHESIVES
- C09J11/00—Features of adhesives not provided for in group C09J9/00, e.g. additives
- C09J11/02—Non-macromolecular additives
- C09J11/06—Non-macromolecular additives organic
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Birds (AREA)
- Epidemiology (AREA)
- Inorganic Chemistry (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Adhesives Or Adhesive Processes (AREA)
Abstract
Description
(1)付け睫を接着することができる十分な接着力を有しながら、塗布部分は比較的早く乾き、べたべたしないこと、
(2)まばたきしても、付け睫がゆらゆらしたり、とれないだけの粘着力と追随性を有すること、
(3)洗顔等の簡単な手段で塗布部分が脱着しやすいこと、
の条件を満足させる付け睫接着剤を見出すべく研究を行っていたところ、水不溶性皮膜形成性高分子とグリコシルトレハロースを組み合わせることで、当該条件が満たされた付け睫接着剤が得られることを見出した。
(4)着色料を十分に混和し、塗布部を着色できるものであること、
(5)アイライナーとしても描きやすいこと
の条件を満足させることを念頭に、アイライナーと兼用可能な付け睫接着剤の組成をも検討していたところ、着色料を特定の非イオン性界面活性剤と共に上記付け睫接着剤に配合することで、これら条件を満足するアイライナーと兼用可能な付け睫接着剤が得られることを見出し、本発明を完成した。
(A)水不溶性皮膜形成性高分子
(B)グリコシルトレハロース
を含有することを特徴とする付け睫接着剤である。
(A)水不溶性皮膜形成性高分子
(B)グリコシルトレハロース
(C)着色料
を含有することを特徴とするアイライナー兼用付け睫接着剤である。
付け睫接着剤:
下記表1の組成および下記製法により、本発明品1〜6と、比較品1および2の付け睫接着剤を調製した。これらの付け睫接着剤について、下記4評価項目について、試験を行った。この結果も表1に示す。
固形分45%)
注2:ビニゾール2140L(大同化成工業社製;固形分43%)
注3:ビニブランGV−5651(日信化学工業社製;固形分36%)
注4:TORNALE(林原社製;グリコシルトレハロース含量
47%)
(1)1〜5を混合し、均一に分散する。
(評価項目)
イ.付け睫の付着性
ロ.乾きの早さ
ハ.経時での付け睫の付着性
ニ.化粧膜のべたつきの無さ
各試料について、上記イ〜ニの各項目で専門パネル20名による使用テストを行った。使用テストは、各試料を付け睫に塗布し、睫の根元近くのまぶたの際に付け睫を付着させて行い、付け睫の付着性(項目イ)は付け睫を付着させて30秒後に手を離したときに付け睫が付着しているかどうか、乾きの早さ(項目ロ)は塗布1分後に乾いて膜を形成しているかどうか、経時での付け睫の付着性(項目ハ)は塗布10時間後に付け睫が付着しているかどうか、化粧膜のべたつきの無さ(項目ニ)は塗布3分後に膜がべたついていないかどうかを評価した。
絶対評価基準
(評 点):(評価)
6 : 非常に良い
5 : 良い
4 : やや良い
3 : 普通
2 : やや悪い
1 : 悪い
0 : 非常に悪い
(判 定):(評点の平均点)
AA :5点を超える/非常に良好
A :3.5点を超え5点以下/良好
B :1点を超え3.5点以下/やや不良
C :1点以下/不良
発明品1〜3は全ての項目において、AAの評価となり、良い結果だった。発明品4はグリコシルトレハロースが少ないため付け睫の付着性が若干劣るがA評価であり、良い結果だった。また、発明品5は水不溶性皮膜形成性高分子量が少ないため乾きの早さ、化粧膜のべたつきの無さが若干劣るがA評価であり、良い結果だった。発明品6は全ての項目において、AAの評価となり、良い結果だった。
アイライナー兼用付け睫接着剤:
下記表2の組成および下記製法により、本発明品7〜12と、比較品3および4のアイライナー兼用付け睫接着剤を調製した。これらのアイライナー兼用付け睫接着剤について、実施例1の4項目の評価と新たに追加した3項目について、試験を行った。試験は、各試料をアイライナーを塗布する様に、睫の根元近くのまぶたの際に塗布し、その部分に付け睫を付着させ行った。この結果も表2に示す。
(1)1〜4を分散する。
(2)5〜9を混合し(1)を加え、均一に分散する。
(追加評価項目)
ホ.化粧膜の持続
ヘ.にじみにくさ
ト.アイラインの書きやすさ
化粧膜の持続(項目ホ)は塗布10時間後に化粧膜が持続しているかどうか、にじみにくさ(項目ヘ)は塗布10時間後ににじんでいないかどうか、アイラインの書きやすさ(項目ト)はアイライナーとして描きやすいかどうかを評価した。なお、評価基準および判定は、実施例1と同じである。
発明品7〜9は全ての項目において、AAの評価となり、良い結果だった。発明品10はグリコシルトレハロースが少ないため付け睫の付着性が若干劣るがA評価であり、良い結果だった。また、発明品11は水不溶性皮膜形成性高分子量が少ないため乾きの早さ、化粧膜のべたつきの無さ、にじみにくさが若干劣るがA評価であり、良い結果だった。発明品12は全ての項目において、AAの評価となり、良い結果だった。
下記成分および製法により、塗布色が紺のアイライナー兼用付け睫接着剤を調製した。
1.ポリオキシエチレン(20)硬化ひまし油 注6 2
2.1,3-ブチレングリコール 10
3.群青 1
4.コンジョウ 0.5
5.黒酸化鉄 0.8
6.アクリル酸アルキル/酢酸ビニル共重合体エマルション 注1 60
7.グリコシルトレハロース・水添デンプン分解物水溶液 注4 20
8.水 残 量
9.酸化チタン被覆合成金雲母 注7 1
注1:前と同じ
注4:前と同じ
注6:HLB値 10.5
注7:HELIOS R100S(S)(トピー工業社製)
平均粒径105μm
A.成分(1)〜(5)を均一に分散させる。
B.Aと成分(6)〜(9)を均一に混合する。
下記成分および製法により、塗布色が茶のアイライナー兼用付け睫接着剤を調製した。
1.モノステアリン酸ポリエチレングリコール(40) 注8 2
2.1,3-ブチレングリコール 10
3.赤202 0.5
4.黄色4 0.5
5.黄酸化鉄 0.8
6.赤酸化鉄 0.5
7.酢酸ビニル重合体エマルション 注3 40
8.グリコシルトレハロース・水添デンプン分解物水溶液 注4 40
9.水 残 量
10.酸化チタン被覆マイカ 注9 1
注3:前と同じ
注4:前と同じ
注8:HLB値 17.5
注9:FLAMENCO ULTRA SPARKLE 4500(BASF
社製)平均粒径50μm
A.成分(1)〜(6)を均一に分散させる。
B.Aと成分(7)〜(10)を均一に混合する。
下記成分および製法により、塗布後にきらめきを付与できる透明のアイライナー兼用付け睫接着剤を調製した。
1.モノステアリン酸ポリエチレングリコール(55) 注10 2
2.1,3-ブチレングリコール 10
3.アクリル酸アルキル重合体エマルション 注1 20
4.グリコシルトレハロース・水添デンプン分解物水溶液 注4 60
5.水 残 量
6.(PET/AL)ラミネート 注11 2
7.酸化チタン被覆ガラス末 注12 1
注1:前と同じ
注4:前と同じ
注10:HLB値 18
注11:KFSグリッターシルバー 0.15mm(カタニ産業社製)
平均粒径150μm
注12:マイクログラス メタシャインMT1080RS(日本板硝子社製)
平均粒径80μm
A.成分(1)〜(7)を均一に混合する。
下記成分および製法により、塗布色が緑のアイライナー兼用付け睫接着剤を調製した。
1.ポリオキシエチレン(20)モノオレイン酸ソルビタン 注13 1
2.ポリオキシエチレンセチルエーテル 注5 1
3.1,3-ブチレングリコール 10
4.黄酸化鉄 2
5.コンジョウ 1
6.アクリル酸アルキル/酢酸ビニル共重合体エマルション 注1 30
7.グリコシルトレハロース・水添デンプン分解物水溶液 注4 40
8.水 残 量
9.酸化チタン被覆合成金雲母 注7 1
注1:前と同じ
注4:前と同じ
注5:前と同じ
注7:前と同じ
注13:HLB値 15
A.成分(1)〜(5)を均一に分散させる。
B.Aと成分(6)〜(9)を均一に混合する。
Claims (12)
- 次の成分(A)および(B);
(A)水不溶性皮膜形成性高分子
(B)グリコシルトレハロース
を含有することを特徴とする付け睫接着剤。 - 前記成分(A)を、1〜60質量%、前記成分(B)を5〜70質量%含有する請求項1記載の付け睫接着剤。
- 前記成分(A)の水不溶性皮膜形成性高分子が、(メタ)アクリル酸アルキルをモノマー構成単位として含む重合体もしくは共重合体である請求項 1または2記載の付け睫接着剤。
- 前記成分(A)の水不溶性皮膜形成性高分子が、酢酸ビニルをモノマー構成単位として含む重合体もしくは共重合体である請求項1または2記載の付け睫接着剤。
- 次の成分(A)〜(C);
(A)水不溶性皮膜形成性高分子
(B)グリコシルトレハロース
(C)着色料
を含有することを特徴とするアイライナー兼用付け睫接着剤。 - 前記成分(A)を、5〜60質量%、前記成分(B)を20〜70質量%および前記成分(C)を1〜50質量%含有する請求項5記載のアイライナー兼用付け睫接着剤。
- 前記成分(A)の水不溶性皮膜形成性高分子が、(メタ)アクリル酸アルキルをモノマー構成単位として含む重合体もしくは共重合体である請求項5または6記載のアイライナー兼用付け睫接着剤。
- 前記成分(A)の水不溶性皮膜形成性高分子が、酢酸ビニルをモノマー構成単位として含む重合体もしくは共重合体である請求項5または6記載のアイライナー兼用付け睫接着剤。
- 成分(C)の着色料がカーボンブラックを含むものである請求項5ないし8の何れかの項記載のアイライナー兼用付け睫接着剤。
- 更に成分(D)としてHLB10以上の非イオン性界面活性剤を含有する請求項5ないし9の何れかの項記載のアイライナー兼用付け睫接着剤。
- 成分(D)の含有量が0.1〜10質量%である請求項10記載のアイライナー兼用付け睫接着剤。
- 前記成分(D)のHLB10以上の非イオン性界面活性剤が、ポリオキシエチレンアルキルエーテルである請求項10または11記載のアイライナー兼用付け睫接着剤。
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