JP2012193288A - Discharge treatment method for resin film - Google Patents
Discharge treatment method for resin film Download PDFInfo
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- JP2012193288A JP2012193288A JP2011058798A JP2011058798A JP2012193288A JP 2012193288 A JP2012193288 A JP 2012193288A JP 2011058798 A JP2011058798 A JP 2011058798A JP 2011058798 A JP2011058798 A JP 2011058798A JP 2012193288 A JP2012193288 A JP 2012193288A
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- discharge treatment
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- resin film
- corona discharge
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- 238000000034 method Methods 0.000 title claims abstract description 53
- 239000011347 resin Substances 0.000 title claims abstract description 49
- 229920005989 resin Polymers 0.000 title claims abstract description 49
- 208000028659 discharge Diseases 0.000 title claims abstract description 36
- 230000001681 protective effect Effects 0.000 claims abstract description 13
- 239000002313 adhesive film Substances 0.000 claims description 9
- 238000012545 processing Methods 0.000 claims description 4
- 238000003672 processing method Methods 0.000 claims 2
- 239000010408 film Substances 0.000 abstract description 87
- MUBZPKHOEPUJKR-UHFFFAOYSA-N Oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 abstract description 15
- 235000006408 oxalic acid Nutrition 0.000 abstract description 5
- 239000012788 optical film Substances 0.000 abstract description 4
- 230000003287 optical effect Effects 0.000 abstract description 3
- 150000001735 carboxylic acids Chemical class 0.000 abstract 1
- 238000013518 transcription Methods 0.000 abstract 1
- 230000035897 transcription Effects 0.000 abstract 1
- 238000003851 corona treatment Methods 0.000 description 26
- -1 polyethylene Polymers 0.000 description 5
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 4
- 239000000853 adhesive Substances 0.000 description 3
- 230000001070 adhesive effect Effects 0.000 description 2
- 239000012790 adhesive layer Substances 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 229920000139 polyethylene terephthalate Polymers 0.000 description 2
- 239000005020 polyethylene terephthalate Substances 0.000 description 2
- 238000004804 winding Methods 0.000 description 2
- 229920002284 Cellulose triacetate Polymers 0.000 description 1
- 239000004698 Polyethylene Substances 0.000 description 1
- 239000004743 Polypropylene Substances 0.000 description 1
- NNLVGZFZQQXQNW-ADJNRHBOSA-N [(2r,3r,4s,5r,6s)-4,5-diacetyloxy-3-[(2s,3r,4s,5r,6r)-3,4,5-triacetyloxy-6-(acetyloxymethyl)oxan-2-yl]oxy-6-[(2r,3r,4s,5r,6s)-4,5,6-triacetyloxy-2-(acetyloxymethyl)oxan-3-yl]oxyoxan-2-yl]methyl acetate Chemical compound O([C@@H]1O[C@@H]([C@H]([C@H](OC(C)=O)[C@H]1OC(C)=O)O[C@H]1[C@@H]([C@@H](OC(C)=O)[C@H](OC(C)=O)[C@@H](COC(C)=O)O1)OC(C)=O)COC(=O)C)[C@@H]1[C@@H](COC(C)=O)O[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]1OC(C)=O NNLVGZFZQQXQNW-ADJNRHBOSA-N 0.000 description 1
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- 238000001125 extrusion Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 230000000873 masking effect Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- JFNLZVQOOSMTJK-KNVOCYPGSA-N norbornene Chemical compound C1[C@@H]2CC[C@H]1C=C2 JFNLZVQOOSMTJK-KNVOCYPGSA-N 0.000 description 1
- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 238000009832 plasma treatment Methods 0.000 description 1
- 229920003229 poly(methyl methacrylate) Polymers 0.000 description 1
- 229920001707 polybutylene terephthalate Polymers 0.000 description 1
- 229920006289 polycarbonate film Polymers 0.000 description 1
- 229920006267 polyester film Polymers 0.000 description 1
- 229920000573 polyethylene Polymers 0.000 description 1
- 239000004926 polymethyl methacrylate Substances 0.000 description 1
- 229920000098 polyolefin Polymers 0.000 description 1
- 229920001155 polypropylene Polymers 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000012360 testing method Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
Abstract
Description
本発明は、樹脂フィルムの放電処理方法に関するものである。 The present invention relates to a method for discharging a resin film.
従来、偏光フィルムや位相差フィルムなどの樹脂フィルムの表面改質の為にコロナ放電処理、プラズマ処理などの放電処理をすることが知られている。これは樹脂フィルムの表面を親水化させ接着性を向上させるために行うものである。
例えば、樹脂フィルムとガラス基板などの部材とを貼合する際には、樹脂フィルムに粘着剤層（粘着フィルム）を貼合する工程を必要とし、粘着フィルムを貼合する前に樹脂フィルムにコロナ放電処理することが一般的である。樹脂フィルムに粘着フィルムを貼合する際には、樹脂フィルムと粘着フィルムのそれぞれ貼合する面をコロナ放電処理し貼合することが知られている。（特許文献１参照）
Conventionally, it is known to perform discharge treatment such as corona discharge treatment or plasma treatment for surface modification of a resin film such as a polarizing film or a retardation film. This is performed in order to make the surface of the resin film hydrophilic and improve adhesiveness.
For example, when bonding a resin film and a member such as a glass substrate, a step of bonding an adhesive layer (adhesive film) to the resin film is required, and the corona is applied to the resin film before the adhesive film is bonded. It is common to perform a discharge treatment. When bonding an adhesive film to a resin film, it is known that the surfaces of the resin film and the adhesive film to be bonded are subjected to corona discharge treatment and bonded. (See Patent Document 1)
ところで、樹脂フィルムを長時間にわたって連続的に放電処理を行なうと樹脂フィルムに輝点が発生してしまい、特に光学フィルムとしては使用できず問題となっていた。
ここにいう輝点とは、偏光フィルム、供試フィルム、偏光フィルム（各偏光フィルムの偏光軸をクロスニコル状態にする）を貼り合わせ、裏側に配置されているバックライト（光源）から光を入射し、表側から見て光漏れとして認識される部分等を言う。
By the way, when the resin film is continuously subjected to a discharge treatment for a long time, bright spots are generated in the resin film, and it cannot be used as an optical film, which has been a problem.
The bright spot here refers to a polarizing film, a test film, and a polarizing film (the polarizing axis of each polarizing film is set in a crossed Nicol state), and light is incident from a backlight (light source) arranged on the back side. The part recognized as light leakage when viewed from the front side.
本発明は、光学フィルムに現れる輝点を解決する為になされたものであって、この輝点は、大きさが５０μｍ以下である目に見えない光学的異物によるものであることが解明され、その原因は、放電処理を連続的に長時間にわたって施した際に、シュウ酸などのカルボン酸誘導体が工程ロールに付着（樹脂フィルムの表面にコロナ放電処理などの放電処理することにより、樹脂の炭素骨格が切れて空気中の酸素などと反応し、その結果シュウ酸などのカルボン酸誘導体が発生すると思われる）し、それがフィルム面に転写され発生するという知見を得た。
本発明は、このような知見に基づき鑑みなされたもので、樹脂フィルムに輝点を生ずることのない放電処理方法を提供するものである。
The present invention was made to solve the bright spot appearing in the optical film, it was elucidated that this bright spot is caused by invisible optical foreign matter having a size of 50 μm or less, The cause is that when the discharge treatment is continuously performed over a long period of time, a carboxylic acid derivative such as oxalic acid adheres to the process roll (the surface of the resin film is subjected to discharge treatment such as corona discharge treatment, thereby The skeleton is cut and reacts with oxygen in the air, and as a result, carboxylic acid derivatives such as oxalic acid are considered to be generated).
The present invention has been made based on such knowledge, and provides a discharge treatment method that does not cause bright spots on a resin film.
本発明は、
（１）樹脂フィルムに放電処理を行なうに際し、
表面に放電処理した後、直ちに処理面を保護フィルムで被覆し、
次いで、裏面に放電処理した後、該処理面を非接触状態のまま樹脂フィルムを移送し、後次工程に供することを特徴とする樹脂フィルムの放電処理方法；
（２）空気噴出孔を設けた工程ロールにて前記処理面を非接触状態のまま樹脂フィルムを移送することを特徴とする（１）記載の樹脂フィルムの放電処理方法；
（３）前記保護フィルムは、粘着フィルムを有するものであることを特徴とする（１）、（２）のいずれかに記載の樹脂フィルムの放電処理方法；
（４）前記樹脂フィルムが偏光フィルムまたは位相差フィルムであることを特徴とする（１）乃至（３）のいずれかに記載の樹脂フィルムの放電処理方法；
である。
The present invention
(1) When performing discharge treatment on a resin film,
After the discharge treatment on the surface, immediately cover the treated surface with a protective film,
Next, after the discharge treatment is performed on the back surface, the resin film is transferred while the treated surface is in a non-contact state, and subjected to a subsequent process;
(2) The resin film discharge treatment method according to (1), wherein the resin film is transferred while the treatment surface is in a non-contact state by a process roll provided with air ejection holes;
(3) The method for discharging treatment of a resin film according to any one of (1) and (2), wherein the protective film has an adhesive film;
(4) The resin film discharge treatment method according to any one of (1) to (3), wherein the resin film is a polarizing film or a retardation film;
It is.
本発明の放電処理方法は、樹脂フィルムの放電処理面がガイドロール、移送ロールなどの工程ロール面に直接接することがないので、工程ロール面の状態如何に拘らず（工程ロールに付着したシュウ酸などのカルボン酸誘導体の有無に関係なく）、処理面は清浄に保持され、簡便な方法で、輝点の発生が抑制される。 In the discharge treatment method of the present invention, the discharge treatment surface of the resin film is not in direct contact with the process roll surface such as a guide roll or a transfer roll. Therefore, regardless of the state of the process roll surface (oxalic acid adhering to the process roll) Regardless of the presence or absence of a carboxylic acid derivative, etc.), the treated surface is kept clean, and the generation of bright spots is suppressed by a simple method.
以下、本発明の樹脂フィルムの放電処理方法について詳細に説明する。 Hereinafter, the discharge treatment method for the resin film of the present invention will be described in detail.
図１に基づいて本発明を説明する。
ロール巻きされている樹脂フィルム１０１を繰り出し、コロナ放電処理装置１１１によりフィルムの表面にコロナ放電処理をする。その後直ちにコロナ放電処理面に保護フィルム１０４（セパレーターフィルム、粘着フィルム、セパレーターフィルムを順次積層したノンキャリアフィルム１０２の一方のセパレーターフィルム１０３を剥離した粘着フィルム付きフィルム）を被覆する。次いで、樹脂フィルム１０１の裏面にコロナ放電処理装置１１２によりコロナ放電処理をした後、その処理面を非接触状態（コロナ放電処理装置１１２によりコロナ放電処理をした後、巻き取り工程までの間に工程ロールがない）で樹脂フィルム１０１を移送し、後次工程に供する。
本発明における非接触状態とは、コロナ放電処理面が工程ロールと直接接触しない状態のことをいい、具体的な実施形態としては、樹脂フィルムの裏面にコロナ放電処理装置１１２によりコロナ放電処理した後、後次工程の間全く工程ロールがなく移送する方法（図１）、保護フィルム２０４で被覆している面に工程ロール２２１を抱かせて移送する方法（図２）、樹脂フィルムの裏面にコロナ放電処理装置３１２によりコロナ放電処理した後、空気噴出孔を設けた工程ロール３２２で移送する方法（図３）、裏面にコロナ放電処理した後その面を保護フィルムで被覆して移送する方法（図示せず）などがある。
The present invention will be described with reference to FIG.
The rolled resin film 101 is fed out, and the corona discharge treatment device 111 performs corona discharge treatment on the surface of the film. Immediately thereafter, the protective film 104 (a film with an adhesive film from which one separator film 103 of the non-carrier film 102 in which the separator film, the adhesive film, and the separator film are sequentially laminated) is peeled is coated on the corona discharge treated surface. Next, after the corona discharge treatment device 112 is subjected to corona discharge treatment on the back surface of the resin film 101, the treatment surface is in a non-contact state (the process between the corona discharge treatment by the corona discharge treatment device 112 and the winding process). The resin film 101 is transferred with no roll) and used for the subsequent process.
The non-contact state in the present invention refers to a state in which the corona discharge treatment surface is not in direct contact with the process roll. As a specific embodiment, after the corona discharge treatment device 112 performs corona discharge treatment on the back surface of the resin film. , A method in which there is no process roll during the subsequent process (FIG. 1), a method in which the process roll 221 is held on the surface covered with the protective film 204 (FIG. 2), and a corona on the back surface of the resin film. After the corona discharge treatment by the discharge treatment device 312, a method of transferring with a process roll 322 provided with air ejection holes (FIG. 3), a method of corona discharge treatment on the back surface and coating the surface with a protective film (FIG. 3) Not shown).
また、最初に樹脂フィルムの表面にコロナ放電処理した後、直ちに該処理面を保護フィルム１０４で被覆することが必要である。従来のような樹脂フィルムの両面コロナ放電処理方法（図４）であれば、コロナ放電処理装置４１１を用いてコロナ放電処理をした面が次のコロナ放電処理装置４１２を用いてコロナ放電処理する際に使用されるロールに直接接触するため、長時間にわたって連続的に行うとシュウ酸などのカルボン酸誘導体がロールに付着し、結果としてフィルムに輝点が発生するのであるが、本発明の放電処理方法は、コロナ放電処理装置１１１を用いてコロナ放電処理した後、直ちに処理面を保護フィルム１０４で被覆することにより、最初のコロナ放電処理面についてはその後どのようなパスラインにしようと工程ロールが直接表面処理面に接することがないので、輝点の発生が抑制される。 Further, after the corona discharge treatment is first performed on the surface of the resin film, it is necessary to immediately cover the treated surface with the protective film 104. In the conventional double-sided corona discharge treatment method for resin films (FIG. 4), when the corona discharge treatment surface using the corona discharge treatment device 411 is subjected to corona discharge treatment using the next corona discharge treatment device 412. The carboxylic acid derivative such as oxalic acid adheres to the roll when it is continuously applied over a long period of time because it is in direct contact with the roll used for the film, and as a result, a bright spot is generated on the film. After the corona discharge treatment using the corona discharge treatment apparatus 111, the method immediately coats the treatment surface with the protective film 104, so that the process roll can be changed to any pass line for the first corona discharge treatment surface thereafter. Since there is no direct contact with the surface-treated surface, generation of bright spots is suppressed.
また、裏面の処理面についても非接触状態のまま移送することで、工程ロールに直接接触させずに移送させ、両面加工の樹脂フィルムの輝点の発生を抑制するのである。 Further, by transferring the processing surface on the back surface in a non-contact state, the processing surface is transferred without being brought into direct contact with the process roll, and generation of bright spots on the double-sided resin film is suppressed.
図１の実施形態では、ロール巻きされている樹脂フィルム１０１を繰り出して、コロナ放電処理する方法を記載しているが、樹脂フィルムの供給方法はこれに限らず、例えば溶融押出で成形したフィルムをそのままコロナ放電処理する場合も包含する。 In the embodiment of FIG. 1, a method is described in which the roll-wrapped resin film 101 is fed out and subjected to corona discharge treatment. However, the resin film supply method is not limited to this, for example, a film formed by melt extrusion is used. This includes the case where the corona discharge treatment is performed as it is.
本発明における樹脂フィルムとしては、ポリエチレンフィルム、ポリプロピレンフィルム、ノルボルネン系フィルムなどのポリオレフィン系フィルム、ポリメチルメタクリレートなどのアクリル系フィルム、ポリエチレンテレフタレート、ポリブチレンテレフタレートなどのポリエステル系フィルム、ポリカーボネートフィルム、トリアセチルセルロースフィルム等の透明フィルムが挙げられるが、特にこれらに限定されない。 Examples of the resin film in the present invention include polyethylene films, polypropylene films, polyolefin films such as norbornene films, acrylic films such as polymethyl methacrylate, polyester films such as polyethylene terephthalate and polybutylene terephthalate, polycarbonate films, and triacetyl cellulose. Although transparent films, such as a film, are mentioned, it is not specifically limited to these.
本発明でいう保護フィルムには、前述の保護フィルム１０４の他に基材フィルムに粘着剤層を塗布した粘着タイプ、オレフィン系の自己粘着タイプのプロテクトフィルム・マスキングフィルムや粘着性を有しないいわゆる合紙と呼ばれるポリエチレンテレフタレート系フィルムを使用できる。また、本発明でいう後次工程とは、巻き取り工程（図１、図２、図３）に限定されず、それ以外にカット工程（枚葉加工）や他のフィルムと貼合する工程なども含まれる。さらに、上記の説明においては、放電処理がコロナ放電処理の場合について説明したが、プラズマ放電処理にも本発明が適用できることは言うまでもない。 The protective film referred to in the present invention includes, in addition to the protective film 104 described above, an adhesive type in which an adhesive layer is applied to a base film, an olefin-based self-adhesive type protective film / masking film, and a so-called non-adhesive composite. A polyethylene terephthalate film called paper can be used. In addition, the subsequent process referred to in the present invention is not limited to the winding process (FIGS. 1, 2, and 3), but other than that, a cutting process (sheet processing), a process of bonding with another film, and the like. Is also included. Further, in the above description, the case where the discharge process is the corona discharge process has been described, but it goes without saying that the present invention can also be applied to the plasma discharge process.
本発明は、樹脂フィルムの放電処理方法に関するものであり、特に液晶ディスプレー等の製造に用いられる偏光フィルムや位相差フィルムなどの光学フィルムの処理に好適に用いられる。 The present invention relates to a discharge treatment method for resin films, and is particularly suitable for the treatment of optical films such as polarizing films and retardation films used in the production of liquid crystal displays and the like.
１０１、２０１、３０１、４０１：樹脂フィルム
１０２、２０２、３０２：ノンキャリアフィルム
１０３、２０３、３０３：セパレーターフィルム
１０４、２０４、３０４：保護フィルム（粘着フィルム付きフィルム）
１１１、１１２、２１１、２１２、３１１、３１２、４１１、４１２：コロナ放電処理装置
２２１：工程ロール
３２２：空気噴出孔を設けた工程ロール
101, 201, 301, 401: Resin film 102, 202, 302: Non-carrier film 103, 203, 303: Separator film 104, 204, 304: Protection film (film with adhesive film)
111, 112, 211, 212, 311, 312, 411, 412: Corona discharge treatment device 221: Process roll 322: Process roll provided with air ejection holes
Claims (4)
表面に放電処理した後、直ちに処理面を保護フィルムで被覆し、
次いで、裏面に放電処理した後、該処理面を非接触状態のまま樹脂フィルムを移送し、後次工程に供することを特徴とする樹脂フィルムの放電処理方法。 When performing a discharge treatment on a resin film,
After the discharge treatment on the surface, immediately cover the treated surface with a protective film,
Next, after the discharge treatment is performed on the back surface, the resin film is transferred while the treated surface is in a non-contact state, and is subjected to a subsequent process.
4. The resin film discharge treatment method according to claim 1, wherein the resin film is a polarizing film or a retardation film.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2011058798A JP5600622B2 (en) | 2011-03-17 | 2011-03-17 | Discharge treatment method for resin film |
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|---|---|---|---|
| JP2011058798A JP5600622B2 (en) | 2011-03-17 | 2011-03-17 | Discharge treatment method for resin film |
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| JP2012193288A true JP2012193288A (en) | 2012-10-11 |
| JP5600622B2 JP5600622B2 (en) | 2014-10-01 |
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Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11286561A (en) * | 1998-04-03 | 1999-10-19 | Konica Corp | Surface-treatment of substrate, surface-treating apparatus, coating and coater |
| JP2005213314A (en) * | 2004-01-28 | 2005-08-11 | Sumitomo Chemical Co Ltd | Method for sticking adhesive layer |
| JP2009265624A (en) * | 2008-03-31 | 2009-11-12 | Fujifilm Corp | Optical film, polarizing plate and liquid crystal display |
-
2011
- 2011-03-17 JP JP2011058798A patent/JP5600622B2/en active Active
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11286561A (en) * | 1998-04-03 | 1999-10-19 | Konica Corp | Surface-treatment of substrate, surface-treating apparatus, coating and coater |
| JP2005213314A (en) * | 2004-01-28 | 2005-08-11 | Sumitomo Chemical Co Ltd | Method for sticking adhesive layer |
| JP2009265624A (en) * | 2008-03-31 | 2009-11-12 | Fujifilm Corp | Optical film, polarizing plate and liquid crystal display |
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| JP5600622B2 (en) | 2014-10-01 |
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