JP2010521567A - 透明なピグメントバイオレット23の製造方法 - Google Patents
透明なピグメントバイオレット23の製造方法 Download PDFInfo
- Publication number
- JP2010521567A JP2010521567A JP2009553941A JP2009553941A JP2010521567A JP 2010521567 A JP2010521567 A JP 2010521567A JP 2009553941 A JP2009553941 A JP 2009553941A JP 2009553941 A JP2009553941 A JP 2009553941A JP 2010521567 A JP2010521567 A JP 2010521567A
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- JP
- Japan
- Prior art keywords
- salt
- pigment
- propylene carbonate
- kneading
- weight
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0002—Grinding; Milling with solid grinding or milling assistants
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0014—Influencing the physical properties by treatment with a liquid, e.g. solvents
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0022—Wet grinding of pigments
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/30—Inkjet printing inks
- C09D11/32—Inkjet printing inks characterised by colouring agents
- C09D11/322—Pigment inks
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Paints Or Removers (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Testing Relating To Insulation (AREA)
- Tests Of Circuit Breakers, Generators, And Electric Motors (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
15gの商業的に入手可能なピグメントバイオレット23クルード(Wuxi Xinguang Chemical Industry社製)を90gの塩化ナトリウム(<30μm)と2×30秒間、IKAミル中で混合する。それから、混合物を実験室規模のニーダー(Werner&Pfleiderer製)中で30gのプロピレンカーボネイトと共に80℃、100回転/分で8時間混錬する。その後、混錬物を800mlの5重量%濃度塩酸と混し、吸引濾過し、そして脱イオン水で洗浄する。その後、濾過ケーキを乾燥棚中80℃で乾燥させる。そして14.6gの顔料を得る。
15gの商業的に入手可能なピグメントバイオレット23クルード(Wuxi Xinguang Chemical Industry社製)を90gの塩化ナトリウム(<30μm)と2×30秒間、IKAミル中で混合する。それから、混合物を実験室規模のニーダー(Werner & Pfleiderer製)中で30gのジエチレングリコールと共に80℃、100回転/分で8時間混錬する。その後、混錬物を800mlの5重量%濃度塩酸と混合し、吸引濾過し、そして脱イオン水で洗浄する。その後、濾過ケーキを乾燥棚中80℃で乾燥させる。そして14.5gの顔料を得る。
Claims (10)
- 結晶性の塩と有機液体の存在下でピグメントバイオレット23クルードをソルトニーディングすることによって透明なC.I.ピグメントバイオレット23を製造する方法であって、有機液体がプロピレンカーボネイトであることを特徴とする上記方法。
- 一価、二価又は三価の金属カチオンと無機酸基との結晶性の塩、又はこれらの塩の混合物が使用されることを特徴とする請求項1に記載の方法。
- 結晶性の塩として塩化ナトリウムが使用されることを特徴とする請求項1又は2に記載の方法。
- 結晶性の塩が微細化されていることを特徴とする請求項1〜3の何れか一項に記載の方法。
- ソルトニーディングが50〜150℃の温度で実施されることを特徴とする請求項1〜4の何れか一項に記載の方法。
- プロピレンカーボネイトの使用量が顔料と塩の混合物の重量に対して0.05〜0.8倍量であることを特徴とする請求項1〜5の何れか一項に記載の方法。
- プロピレンカーボネイトの使用量が顔料と塩の混合物の重量に対して0.12〜0.35倍量であることを特徴とする請求項6に記載の方法。
- 顔料の重量に対して1〜10倍量の結晶性の塩が使用されることを特徴とする請求項1〜7の何れか一項に記載の方法。
- ニーディング終了後、塩とプロピレンカーボネイトを酸性のpHで水抽出により除去することを特徴とする請求項1〜8の何れか一項に記載の方法。
- 界面活性剤、非顔料系分散剤、顔料系分散剤、フィラー、希釈剤、樹脂、ワックス、消泡剤、帯電防止剤、防塵剤、エクステンダー、陰影を付加するための着色剤、防腐剤、乾燥遅延剤、レオロジー制御剤、湿潤剤、酸化防止剤、紫外線吸収剤、光安定剤、及び殺生物剤の群からの助剤がさらに添加されることを特徴とする請求項1〜9の何れか一項に記載の方法。
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE102007013962A DE102007013962A1 (de) | 2007-03-23 | 2007-03-23 | Verfahren zur Herstellung von transparentem Pigment Violett 23 |
DE102007013962.6 | 2007-03-23 | ||
PCT/EP2008/001590 WO2008116541A2 (de) | 2007-03-23 | 2008-02-28 | Verfahren zur herstellung von transparentem pigment violett 23 |
Publications (2)
Publication Number | Publication Date |
---|---|
JP2010521567A true JP2010521567A (ja) | 2010-06-24 |
JP5156764B2 JP5156764B2 (ja) | 2013-03-06 |
Family
ID=39592794
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
JP2009553941A Active JP5156764B2 (ja) | 2007-03-23 | 2008-02-28 | 透明なピグメントバイオレット23の製造方法 |
Country Status (8)
Country | Link |
---|---|
US (1) | US7892345B2 (ja) |
EP (1) | EP2129726B1 (ja) |
JP (1) | JP5156764B2 (ja) |
CN (1) | CN101641414B (ja) |
DE (2) | DE102007013962A1 (ja) |
DK (1) | DK2129726T3 (ja) |
ES (1) | ES2355285T3 (ja) |
WO (1) | WO2008116541A2 (ja) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE102004010282A1 (de) * | 2004-03-03 | 2005-09-22 | Clariant Gmbh | Violettes Farbmittel für Color Filter, Ink Jet Tinten, elektrophotographische Toner und Entwickler und e-inks |
CN102863818B (zh) * | 2012-09-18 | 2014-05-14 | 杭州红妍颜料化工有限公司 | 一种颜料紫3的制备方法 |
CN103275517B (zh) * | 2013-05-27 | 2015-06-03 | 南通龙翔化工有限公司 | 一种在颜料化过程中有效回收研磨介质的方法 |
CN105111784B (zh) * | 2015-09-28 | 2017-11-24 | 温州金源新材料科技有限公司 | 高性能颜料蓝60的制备方法 |
CN108795101A (zh) * | 2017-06-02 | 2018-11-13 | 银川百泓新材料科技有限公司 | 一种捏合法制备永固紫的制备工艺及永固紫 |
EP3647374A4 (en) * | 2017-06-28 | 2021-04-14 | DIC Corporation | PIGMENT COMPOSITION AND PRINT INK |
CN113881245B (zh) * | 2020-07-03 | 2023-11-17 | 山东凯瑞尔光电科技有限公司 | 用于光刻胶的改性黄色颜料、其制备方法及应用 |
Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000336293A (ja) * | 1999-03-19 | 2000-12-05 | Seiko Epson Corp | インクジェット記録に好ましく用いられる水性インク組成物 |
JP2003089756A (ja) * | 2001-06-28 | 2003-03-28 | Dainichiseika Color & Chem Mfg Co Ltd | 微細化顔料および着色用組成物 |
EP1411091A1 (en) * | 1999-07-09 | 2004-04-21 | Ciba Specialty Chemicals Holding Inc. | Process for the preparation of pigments having improved colouristic properties |
US20050139127A1 (en) * | 2003-12-31 | 2005-06-30 | Smith Norman W. | Preparation of yellow pigment |
EP1655352A1 (en) * | 2003-08-11 | 2006-05-10 | Dainippon Ink And Chemicals, Inc. | Process for producing water based pigment dispersion for ink jet recording |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS52935A (en) | 1975-06-24 | 1977-01-06 | Pentel Kk | Method for preparation of pigment |
JP3388591B2 (ja) * | 1991-03-22 | 2003-03-24 | クラリアント・ゲゼルシヤフト・ミト・ベシユレンクテル・ハフツング | C.i.ピグメント・バイオレット23を基礎とする顔料調製物の製造方法 |
JP3916786B2 (ja) | 1998-12-18 | 2007-05-23 | 花王株式会社 | 皮膚化粧料 |
US6476222B2 (en) * | 2001-01-05 | 2002-11-05 | Sun Chemical Corporation | Preparation of heat stable pigment violet 23 |
DE102004010282A1 (de) | 2004-03-03 | 2005-09-22 | Clariant Gmbh | Violettes Farbmittel für Color Filter, Ink Jet Tinten, elektrophotographische Toner und Entwickler und e-inks |
JP2006299138A (ja) * | 2005-04-22 | 2006-11-02 | Toyo Ink Mfg Co Ltd | 顔料組成物の製造方法 |
EP1956060B1 (en) * | 2005-10-31 | 2012-01-11 | DIC Corporation | Aqueous pigment dispersion and ink for inkjet recording |
-
2007
- 2007-03-23 DE DE102007013962A patent/DE102007013962A1/de not_active Withdrawn
-
2008
- 2008-02-28 CN CN2008800092754A patent/CN101641414B/zh active Active
- 2008-02-28 US US12/531,797 patent/US7892345B2/en active Active
- 2008-02-28 DK DK08716117.0T patent/DK2129726T3/da active
- 2008-02-28 JP JP2009553941A patent/JP5156764B2/ja active Active
- 2008-02-28 WO PCT/EP2008/001590 patent/WO2008116541A2/de active Search and Examination
- 2008-02-28 DE DE502008002288T patent/DE502008002288D1/de active Active
- 2008-02-28 ES ES08716117T patent/ES2355285T3/es active Active
- 2008-02-28 EP EP08716117A patent/EP2129726B1/de active Active
Patent Citations (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2000336293A (ja) * | 1999-03-19 | 2000-12-05 | Seiko Epson Corp | インクジェット記録に好ましく用いられる水性インク組成物 |
EP1411091A1 (en) * | 1999-07-09 | 2004-04-21 | Ciba Specialty Chemicals Holding Inc. | Process for the preparation of pigments having improved colouristic properties |
JP2003089756A (ja) * | 2001-06-28 | 2003-03-28 | Dainichiseika Color & Chem Mfg Co Ltd | 微細化顔料および着色用組成物 |
EP1655352A1 (en) * | 2003-08-11 | 2006-05-10 | Dainippon Ink And Chemicals, Inc. | Process for producing water based pigment dispersion for ink jet recording |
US20050139127A1 (en) * | 2003-12-31 | 2005-06-30 | Smith Norman W. | Preparation of yellow pigment |
Also Published As
Publication number | Publication date |
---|---|
WO2008116541A3 (de) | 2009-04-02 |
WO2008116541A2 (de) | 2008-10-02 |
DE502008002288D1 (de) | 2011-02-24 |
EP2129726A2 (de) | 2009-12-09 |
CN101641414B (zh) | 2013-04-17 |
EP2129726B1 (de) | 2011-01-12 |
JP5156764B2 (ja) | 2013-03-06 |
DK2129726T3 (da) | 2011-04-11 |
ES2355285T3 (es) | 2011-03-24 |
CN101641414A (zh) | 2010-02-03 |
US20100101456A1 (en) | 2010-04-29 |
US7892345B2 (en) | 2011-02-22 |
DE102007013962A1 (de) | 2008-09-25 |
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