JP2010513598A - ゲル状接着剤剥離組成物および使用方法 - Google Patents
ゲル状接着剤剥離組成物および使用方法 Download PDFInfo
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- JP2010513598A JP2010513598A JP2009541466A JP2009541466A JP2010513598A JP 2010513598 A JP2010513598 A JP 2010513598A JP 2009541466 A JP2009541466 A JP 2009541466A JP 2009541466 A JP2009541466 A JP 2009541466A JP 2010513598 A JP2010513598 A JP 2010513598A
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Classifications
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- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
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Abstract
Description
本開示は、硬い基材、特に、自動車、トラック、バス、飛行機を含む航空宇宙乗物などといった乗物から接着剤残留物を除去するための環境に優しい材料を用いる処理を含む。この処理は、1つ以上の非ハロゲン系有機溶媒、非研磨増粘剤、界面活性剤、蒸気圧調節剤を含む新規な接着剤剥離組成物を用いる。非ハロゲン系有機溶媒の各々についての25℃での合計ハンセン溶解度パラメータ(「δt」または「HSP」)は、約14MPa1/2から約24MPa1/2である。この開示は、たとえば、航空機の複合およびアルミニウム表面の広い領域ならびにその他の領域から感圧性接着剤の残留物を除去するために具体的に配合されたコスト効率がよく、安全で、環境に優しい接着剤剥離組成物を提供する。
たとえば、自動車、トラック、バス、列車、船、および航空機の本体などといった硬い表面からビニール製のシールを取除くことに関連する、接着剤残留物を取除くための従来の方法はしばしば、多大な時間を要し、高価であり、非能率であるとともに、環境に有害な材料を用いる必要がある。たとえば、当該技術で認識される技術を用いると、ビニール製のシールはしばしば、ヒートガンを通じて熱を慎重に加え、シールと接着剤のほとんどを取除くよう擦ることにより取除かれる。残っている接着剤残留物を取除く典型的な方法は、溶媒が染み込んだ布切れで拭き取り去ることである。この方法は、小さい領域を清浄する場合には許容可能であり得るが、飛行機の翼のような大きい領域を清浄する場合には実用的でない。
。従来のアルミニウムの航空機表面上に用いられる、クリーナ、ストリッパ、および他の材料のほとんどは、複合材料と適合しない。
本開示の発明は、硬い基材、特に、自動車、トラック、バス、および飛行機を含む航空宇宙乗物などといった乗物から接着剤残留物を取除くための環境に優しい材料を用いた処理を含む。この処理は、1つ以上の非ハロゲン系有機溶媒と、非研磨増粘剤、界面活性剤、蒸気圧調節剤を含む新規な接着剤剥離組成物を用いる。非ハロゲン系有機溶媒の各々についての25℃での合計のハンセン溶解度パラメータ(「δt」または「HSP」)は、約14MPa1/2から約24MPa1/2である。この発明は、たとえば、感圧性接着剤の残留物を航空機の複合およびアルミニウム表面の広い領域ならびにその他の領域から取除くために具体的に配合された、コスト効率がよく、安全で、環境に優しい接着剤剥離組成物を提供する。
する問題が最小限で、接着剤残留物を効果的に取除く。ある実施の形態では、接着剤剥離組成物の中の吸収性の指示(追跡用)染料により処理の有効性の高速な視覚評価が可能になる。この発明の他の特徴は、引火性、爆発、および健康特性が向上した接着剤剥離組成物を含む。別の局面では、この発明の接着剤剥離組成物は、一般的な廃棄物処理および破棄方法と適合し得る。
添付の図面を参照して、図1では、接着剤残留物が接着しているサンプル基材が、テープ(18)によって作業台(10)に固定され、接着剤剥離組成物(16)の薄いコーティング(約1cmの厚さ)が、適用ツール(14)を用いて手(12)によって塗布される。たとえば、この基材は、アルミニウムまたはグラファイトエポキシ複合材料であってもよく、以前にはシールが存在していた場合がある。当該シールは、細長い片にされ、ヒートガンで加熱され、基材から細長い片を剥き取ることにより取除かれた。
能な状態にしてしまう。
24MPa1/2である。この発明の別の実施の形態では、1つ以上の非ハロゲン系有機溶媒の各々についての25℃での合計のハンセン溶解度パラメータは、約18MPa1/2から約20MPa1/2である。この発明の別の実施の形態では、1つ以上の非ハロゲン系有機溶媒の各々についての25℃での合計のハンセン溶解度パラメータは、約14MPa1/2から約19MPa1/2である。別の実施の形態では、この発明は、2つ以上の非ハロゲン系有機溶媒を含む接着剤剥離組成物を含む。いくつかの場合、二成分溶媒系が好ましい場合がある。すなわち、接着剤剥離組成物は、同一でないHSP値を有し得る2つの非ハロゲン系有機溶媒を含む場合である。二成分溶媒系が用いられる場合、溶媒のHSPにおける差は以下の範囲内であり得る。すなわち、他のものの中で、0<(HSPsolvent1−HSPsolvent2)≦6である。いくつかのより狭いサブレンジは、0<(HSPsolvent1−HSPsolvent2)≦2および4<(HSPsolvent1−HSPsolvent2)≦6を含む。このような接着剤剥離組成物が、溶媒のないまたは濃縮された形態で与えられる場合、使用の前に非ハロゲン系有機溶媒で再構成されてもよい。
、安息香酸(21.8)、キノリン(22.0)、ジエチレングリコールモノメチルエーテル(22.0)、ニトロベンゼン(22.2)、2−ブタノール(22.2)、ジエチレングリコールモノエチルエーテル(22.3)、シクロヘキサノール(22.4)、アニリン(22.6)、ニトロエタン(22.7)、イソブタノール(22.7)、m−クレゾール(22.7)、硫酸ジエチル(22.8)、N−メチル−2−ピロリドン(22.9)、1−ブタノール(23.1)、2−プロパノール(23.5)、エチレングリコールモノエチルエーテル(23.5)、およびベンジルアルコール(23.8)。
8アルキル、特にアルキル基に12−16の炭素原子を含むスルホ酢酸である)と;エーテル基もしくはアミド基により分断されるアルキルまたはアルケニル基を含むN−モノ−C8−C22アルキルまたはアルケニルと;ジソジウムN−モノ−C8−C18アシルイソプロパノールアミドスルホサクシネート、ジソジウムラウリルスルホサクシネート、およびN−モノオレイルイソプロパノールアミドスルホサクシネートを含むスルホサクシネートと;N−C8−C18アシルタウリン、特にアシル基において12−14の炭素原子を含むタウレートと;O−C8−C18アシルイセチオネート、特にアシル基において12−14の炭素原子を含むイセチオネートとである。
がって、この方法が繰返されるべきである。
Drug Administration)リスト、食品添加物状態リスト(the Food Additive Status List)、および着色添加物状態リスト(the Color Additive Status List)において発見され得る。
中の接着剤剥離組成物の5重量%の懸濁液は、水道水のpHと本質的に同じpHを有する。
実施例1−塗布物接着剤残留物
ハンセンプロファイルが、各種溶媒について「軟化率」(Softening Index;S.I.)を判断することにより生成される。S.I.は、合計のハンセン溶解度パラメータ(δt)の範囲を示すよう選択される標準的な溶媒の組に対する接着剤残留物の反応の相対的な計測値である。ある塩素系テスト溶媒をこの分析において用いたが、この発明の接着剤剥離組成物における利用には好ましくない。なぜならば、塩素系テスト溶媒は廃棄物処理および安全上の望ましくない問題を与えるからである。塗布物系からの残留物を軟化することについての軟化率を判断するために、ASTM標準テスト方法D4752−03を適応したものを用いた。
ト燃料炭化水素成分の範囲内にある約14から15のHSP数を有する溶媒に対して非常に抵抗があることを示す。
テープ残留物を取除くための接着剤剥離組成物をこの発明の原理に従って調製した。ここで上述した方法を用いて、ゴリラテープ(GORILLA TAPE)(登録商標)についての軟化率を判断した。上記の表の「テープ」の欄を参照のこと。ゴリラテープ(登録商標)は、シンシナティ(Cincinnati)、オハイオ(Ohio)のゴリラグルーカンパニー(Gorilla Glue Company)の商標であり、ポリオレフィンならびに天然ゴムおよび合成ゴムを含む感圧性接着剤を有するテープである。
ンを当該混合物の中に混合し、合計の蒸気圧を低減することにより一次溶媒の蒸発を遅らせ、混合物が長期の間にわたって完全に乾燥してしまうことを防ぎ、これにより材料の寿命が延長する。水/エタノール中のメチレンブルー溶液が、ライトブルーの色を与えるよう加えられた。染料は、接着剤により優先的に吸収され、さらにこれにより残っている接着剤残留物を検出するための検査の助けとなるように機能する。界面活性剤/液体石鹸パッケージを包含する商業的な洗剤を加え、混合し、これにより平滑なゲル状の稠度が与えられた。pHが7の緩衝溶液が1容量%(リン酸2水素カリウムおよびリン酸ナトリウム)、敏感な被覆アルミニウム表面の腐食を遅らせるよう加えられた。混合物は、垂直およびオーバーヘッド表面に対する接着についてテストされた。粘性がシリカおよびナフサで必要に応じて調節された。接着剤剥離組成物は、アルミニウム上の経年および硬化したゴリラテープ(登録商標)上でテストされた。接着剤剥離組成物は、テープ残留物を取込むと示された。
Claims (22)
- 1つ以上の非ハロゲン系有機溶媒と、非研磨増粘剤と、界面活性剤と、蒸気圧調節剤とを含み、非ハロゲン系有機溶媒の各々についての25℃での合計のハンセン溶解度パラメータは約14MPa1/2から約24MPa1/2である、接着剤剥離組成物。
- 2つ以上の非ハロゲン系有機溶媒を含む、請求項1に記載の接着剤剥離組成物。
- 2つの非ハロゲン系有機溶媒を含み、ハンセン溶解度パラメータの差が0より大きく、かつ約6MPa1/2未満である、請求項1に記載の接着剤剥離組成物。
- 1つ以上の非ハロゲン系有機溶媒の各々についての25℃での合計のハンセン溶解度パラメータは約18MPa1/2から約20MPa1/2である、請求項1に記載の接着剤剥離組成物。
- 1つ以上の非ハロゲン系有機溶媒の各々についての25℃での合計のハンセン溶解度パラメータは約14MPa1/2から約l9MPa1/2である、請求項1に記載の接着剤剥離組成物。
- 前記非研磨増粘剤はシリカ、セルロース、セルロース誘導体、またはそれらの組み合わせである、請求項1に記載の接着剤剥離組成物。
- 前記界面活性剤は、アニオン系および非イオン系界面活性剤の組み合わせである、請求項1に記載の接着剤剥離組成物。
- 前記蒸気圧調節剤は前記1つ以上の非ハロゲン系有機溶媒に溶解可能であり、前記接着剤剥離組成物は前記1つ以上の非ハロゲン系有機溶媒の蒸気圧を低減するのに十分な量の前記蒸気圧調節剤を含む、請求項1に記載の接着剤剥離組成物。
- 前記蒸気圧調節剤は、20torrで約100℃より大きい沸点を有する非イオン系の液体である、請求項8に記載の接着剤剥離組成物。
- 前記蒸気圧調節剤はグリセリンである、請求項9に記載の接着剤剥離組成物。
- 吸収性指示染料をさらに含み、前記吸収性指示染料は接着剤残留物の中または上へと吸収可能であり、前記吸収性指示染料は前記1つ以上の非ハロゲン系有機溶媒に溶解可能である、請求項1に記載の接着剤剥離組成物。
- 前記吸収性指示染料はメチレンブルーまたは食品着色料である、請求項11に記載の接着剤剥離組成物。
- 水における前記接着剤剥離組成物の5重量%の懸濁液は約6から約8のpHを有する、請求項1に記載の接着剤剥離組成物。
- 緩衝剤、金属錯化剤、乳化剤、香料、およびそれらの組み合わせからなる群から選択される添加物をさらに含む、請求項1に記載の接着剤剥離組成物。
- 前記接着剤剥離組成物にはハロゲン系有機溶媒が本質的に存在しない、請求項1に記載の接着剤剥離組成物。
- 粘度が約500から約1000ポイズである、請求項1に記載の接着剤剥離組成物。
- 基材から接着剤残留物を取除く方法であって、
1つ以上の非ハロゲン系有機溶媒と、非研磨増粘剤と、界面活性剤と、蒸気圧調節剤と、吸収性指示染料とを含む接着剤剥離組成物を与えるステップを含み、非ハロゲン系有機溶媒の各々についての25℃での合計のハンセン溶解度パラメータは、約14MPa1/2から約24MPa1/2であり、前記方法はさらに、
接着剤残留物が引っ付いている基材に前記接着剤剥離組成物を適用するステップと、
前記吸収性指示染料が前記接着剤残留物の中または上へと吸収されるのに十分な時間を経過させるステップと、
清浄された基材が得られるよう前記接着剤剥離組成物を取除くステップと、
前記吸収性指示染料の存在について前記清浄された基材を検査するステップとを含む、方法。 - 前記清浄された基材を水溶液で洗浄するステップをさらに含む、請求項18に記載の方法。
- 前記清浄された基材を非水溶液で洗浄するステップをさらに含む、請求項18に記載の方法。
- 前記基材はエポキシグラファイトの複合材料である、請求項18に記載の方法。
- 前記基材は航空宇宙乗物の外面である、請求項18に記載の方法。
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US11/610,622 US7977294B2 (en) | 2006-12-14 | 2006-12-14 | Gelled adhesive remover composition and method of use |
PCT/US2007/085846 WO2008076603A1 (en) | 2006-12-14 | 2007-11-29 | Gelled adhesive remover composition and method of use |
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JP2016090750A (ja) * | 2014-10-31 | 2016-05-23 | キヤノン株式会社 | トナーの製造方法 |
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Cited By (6)
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JP2013133636A (ja) * | 2011-12-26 | 2013-07-08 | Shimizu Corp | 有機系材料の仕上げ材の撤去方法 |
JP2015124268A (ja) * | 2013-12-26 | 2015-07-06 | 古河電気工業株式会社 | 蓄熱材組成物及び蓄熱装置 |
JP2016090750A (ja) * | 2014-10-31 | 2016-05-23 | キヤノン株式会社 | トナーの製造方法 |
JPWO2019017133A1 (ja) * | 2017-07-20 | 2019-08-08 | Dic株式会社 | 反応性ホットメルト樹脂用剥離剤 |
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KR102317626B1 (ko) * | 2017-07-20 | 2021-10-26 | 디아이씨 가부시끼가이샤 | 반응성 핫멜트 수지용 박리제 |
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JP5840347B2 (ja) | 2016-01-06 |
WO2008076603A1 (en) | 2008-06-26 |
US20080146480A1 (en) | 2008-06-19 |
CN101553560A (zh) | 2009-10-07 |
CN101553560B (zh) | 2012-07-04 |
US8728245B2 (en) | 2014-05-20 |
US7977294B2 (en) | 2011-07-12 |
US20110226283A1 (en) | 2011-09-22 |
EP2115115B1 (en) | 2013-03-20 |
EP2115115A1 (en) | 2009-11-11 |
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