JP2005343859A - 毛髪化粧料 - Google Patents
毛髪化粧料 Download PDFInfo
- Publication number
- JP2005343859A JP2005343859A JP2004168248A JP2004168248A JP2005343859A JP 2005343859 A JP2005343859 A JP 2005343859A JP 2004168248 A JP2004168248 A JP 2004168248A JP 2004168248 A JP2004168248 A JP 2004168248A JP 2005343859 A JP2005343859 A JP 2005343859A
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- Prior art keywords
- carbon atoms
- hair
- fatty acid
- weight
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- Prior art date
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- 239000002537 cosmetic Substances 0.000 title claims abstract description 34
- -1 amide amine Chemical class 0.000 claims abstract description 25
- 150000004665 fatty acids Chemical group 0.000 claims abstract description 23
- 125000002091 cationic group Chemical group 0.000 claims abstract description 11
- 235000014113 dietary fatty acids Nutrition 0.000 claims abstract description 7
- 229930195729 fatty acid Natural products 0.000 claims abstract description 7
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- 150000007524 organic acids Chemical class 0.000 claims abstract description 6
- 125000004432 carbon atom Chemical group C* 0.000 claims description 29
- 239000000203 mixture Substances 0.000 claims description 29
- 125000000217 alkyl group Chemical group 0.000 claims description 12
- 239000003242 anti bacterial agent Substances 0.000 claims description 10
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- 125000003342 alkenyl group Chemical group 0.000 claims description 6
- BTSZTGGZJQFALU-UHFFFAOYSA-N piroctone olamine Chemical compound NCCO.CC(C)(C)CC(C)CC1=CC(C)=CC(=O)N1O BTSZTGGZJQFALU-UHFFFAOYSA-N 0.000 claims description 5
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Landscapes
- Cosmetics (AREA)
Abstract
【解決手段】 (a)一般式(1)で表されるアミドアミン、(b)抗菌剤及びカチオン性殺菌剤から選ばれる少なくとも1種、(c)炭素数8〜30の脂肪族アルコール及び(d)有機酸を含有する毛髪化粧料。
【化1】
[式中、R1COは全脂肪酸残基中、炭素数20以上の脂肪酸残基の割合が60重量%以上、炭素数20の脂肪酸残基の割合が3重量%以上、炭素数22の脂肪酸残基の割合が50〜95重量%である脂肪酸残基を示す。]
【選択図】 なし
Description
(a)一般式(1)で表されるアミドアミン(以下アミドアミン(1)という)
(b)抗菌剤及びカチオン性殺菌剤から選ばれる少なくとも1種
(c)炭素数8〜30の脂肪族アルコール
(d)有機酸
一般式(2)、(3)及び(5)の中のZ1としては、ハロゲン原子が好ましい。
(B)高重合ジメチルポリシロキサン
高重合ジメチルポリシロキサンを本発明の毛髪化粧料中に配合する場合、液状油に溶解して配合するか、予めアミドアミン(1)の酸塩等の陽イオン性界面活性剤やポリオキシエチレンアルキルエーテルなどの非イオン性界面活性剤水溶液中で調製した分散液を配合することが好ましい。液状油としては先に記載した(A)のジメチルポリシロキサンオイルや、下記(E)の環状シリコーン又はイソパラフィン系炭化水素等を挙げることができる。
アミノ変性シリコーンを水性乳濁液として用いる場合、該水性乳濁液中に含まれるアミノ変性シリコーンの量は20〜60重量%が好ましく、30〜50重量%が更に好ましい。
(E)環状シリコーン
(F)フッ素変性シリコーン
(G)アルキル変性シリコーン
(H)一般式(8)で表されるアミノ変性シロキサン−ポリオキシアルキレンブロック共重合体
これらシリコーン成分の中では、(A)ジメチルポリシロキサンオイル、(B)高重合ジメチルポリシロキサン、(E)環状シリコーン、或いはそれらの混合物、(C)アミノ変性シリコーン、(H)アミノ変性シロキサン−ポリオキシアルキレンブロック共重合体が好ましく、その中でも(C)アミノ変性シリコーン、(H)アミノ変性シロキサン−ポリオキシアルキレンブロック共重合体が特に好ましい。
表1に示す組成の毛髪化粧料(ヘアコンディショナー)を以下の方法で調製し、以下の方法で官能評価を行った。結果を表1に示す。
1)100mlのビーカーにイオン交換水、酸以外の成分を最終製造量が300gとなる所要量を入れ65℃に加熱して、均一に溶解させた。
2)500mlのビーカーにイオン交換水、酸を最終製造量が300gとなる所要量を入れ、65℃に加熱し、1)で得た混合物を添加し乳化して、ヘアコンディショナーを調製した。
パネラー10名が、陰イオン性界面活性剤を主体とする市販のシャンプーを用いて洗髪後、各ヘアコンディショナーを使用した。これを1日1回2週間繰り返した。各ヘアコンディショナーの塗布時の滑らかさ、柔らかさ、濯ぎ時の滑らかさ、柔らかさ、及び乾燥後の櫛通りの良さ、仕上がり感について、下記基準で官能評価した。また、乾燥後の抗フケ効果及び抗カユミ効果を下記基準で評価した。
・使用感の評価基準
A:8人以上が効果あると回答
B:6〜7人が効果あると回答
C:4〜5人が効果あると回答
D:3人以下が効果あると回答
・抗フケ効果の評価基準
A:8人以上が、フケが減少した或いはフケがやや減少したと回答
B:6〜7人が、フケが減少した或いはフケがやや減少したと回答
C:4〜5人が、フケが減少した或いはフケがやや減少したと回答
D:フケが減少した或いはフケがやや減少したと回答したのが3人以下
・抗カユミ効果の評価基準
A:8人以上が、カユミが減少した或いはカユミがやや減少したと回答
B:6〜7人が、カユミが減少した或いはカユミがやや減少したと回答
C:4〜5人が、カユミが減少した或いはカユミがやや減少したと回答
D:カユミが減少した或いはカユミがやや減少したと回答したのが3人以下
アミドアミン(1)として、花王(株)製ルナックBAとジメチルアミノプロピルアミンから合成した、下記式(A)で表されるアミドアミン[純度99.6%(その他、未反応脂肪酸、未反応アミン、水分等を含有)、以下アミドアミンAという]を用い、下記組成のコンディショナーを調製した。このコンディショナーは、湿潤時から乾燥後まで滑らかさ、柔らかさに優れ、抗フケ、抗カユミ効果にも優れていた。
<コンディショナー組成>
アミドアミンA 1.5%
ジンクピリチオン 0.5%
ステアリルアルコール*1 4.0%
グリセリン 1.0%
ベンジルオキシエタノール 0.3%
シリコーン*2 2.0%
アミノ変性シリコーン−ポリオキシアルキレンブロック共重合体*3 0.5%
乳酸 0.5%
ジペンタエリスルトール脂肪酸エステル*4 0.2%
ヒドロキシエチルセルロース*5 0.2%
高重合ポリエチレングリコール*6 0.05%
酢酸トコフェロール 0.1%
香料、メチルパラベン 適量
精製水 残量
(pH4.5)
*1 花王(株)製 カルコール8098
*2 東レ・ダウコーニング・シリコーン(株)製 BY00−003
*3 日本ユニカー(株)製 FZ−3789
*4 日清製油(株)製 コスモール168AR
*5 ダイセル化学工業(株)製 SE−850
*6 ユニオンカーバイド(株)製 ポリオックスWSRN−60K。
下記組成のヘアコンディショナーを調製した。このヘアコンディショナーは、塗布時、濯ぎ時のリッチ感とその持続性、柔軟性、平滑性、及び乾燥後の柔らか感、櫛通りが良好で、抗フケ、抗カユミ効果にも優れていた。
アミドアミンA 2.0%
ピロクトンオラミン 0.5%
塩化ベヘニルトリメチルアンモニウム 0.3%
ステアリルアルコール 4.5%
ベヘニルアルコール*1 1.5%
イソノナン酸イソノニル*2 0.5%
シリコーン*3 1.0%
アミノ変性シリコーン*4 0.5%
グリコール酸 0.5%
リンゴ酸 0.1%
ジプロピレングリコール 3.0%
ベンジルアルコール 0.3%
アルギニン 0.2%
パントテニルエチルエーテル 0.1%
香料、メチルパラベン 適量
精製水 残量
(pH4.0)
*1 花王(株)製 カルコール22080
*2 日清製油(株)製 サラコス99
*3 東レ・ダウコーニング・シリコーン(株)製 SH200C―5000cs
*4 東レ・ダウコーニング・シリコーン(株)製 SM8704C
Claims (3)
- (b)成分が、トリクロサン、トリクロカルバン、ピロクトンオラミン、ジンクピリチオン、二硫化セレン及び3−メチル−4−(1−メチルエチル)フェノールから選ばれる抗菌剤、次の一般式(2)で表される第4級アンモニウム塩、一般式(3)で表されるベンザルコニウム塩又はベンゼトニウム塩、一般式(4)で表されるクロルヘキシジン塩、一般式(5)で表されるピリジニウム塩から選ばれるカチオン性殺菌剤の少なくとも1種である請求項1記載の毛髪化粧料。
- 更に、芳香族アルコールを含有する請求項1又は2記載の毛髪化粧料。
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JP2004168248A JP4198641B2 (ja) | 2004-06-07 | 2004-06-07 | 毛髪化粧料 |
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JP2004168248A JP4198641B2 (ja) | 2004-06-07 | 2004-06-07 | 毛髪化粧料 |
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JP2005343859A true JP2005343859A (ja) | 2005-12-15 |
JP4198641B2 JP4198641B2 (ja) | 2008-12-17 |
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Cited By (13)
Publication number | Priority date | Publication date | Assignee | Title |
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JP2007262046A (ja) * | 2006-03-29 | 2007-10-11 | Sanei Kagaku Kk | ロウ類配合毛髪化粧料 |
EP1870080A1 (en) * | 2005-04-11 | 2007-12-26 | Kao Corporation | Hair cosmetic |
JP2008297296A (ja) * | 2007-06-04 | 2008-12-11 | Hoyu Co Ltd | 毛髪処理用組成物 |
JP2009120558A (ja) * | 2007-11-16 | 2009-06-04 | Kracie Home Products Kk | ヘアリンス組成物 |
JP2010024169A (ja) * | 2008-07-17 | 2010-02-04 | Kracie Home Products Ltd | ヘアリンス組成物 |
JP2010528101A (ja) * | 2007-06-15 | 2010-08-19 | ザ プロクター アンド ギャンブル カンパニー | アミン型カチオン性界面活性剤及び直接染料を含むヘアコンディショニング組成物 |
JP2011525543A (ja) * | 2008-06-25 | 2011-09-22 | ザ プロクター アンド ギャンブル カンパニー | ステアリルアミドプロピルジメチルアミンとl−グルタミン酸との塩を含有するヘアコンディショニング組成物 |
US8101801B2 (en) | 2009-05-18 | 2012-01-24 | Xerox Corporation | Low molecular weight quaternary ammonium salt dispersants |
US8118922B2 (en) | 2009-05-18 | 2012-02-21 | Xerox Corporation | Pigmented phase change inks containing low molecular weight quaternary ammonium salt dispersants |
JP2012176995A (ja) * | 2012-06-21 | 2012-09-13 | Kao Corp | 毛髪化粧料 |
CN102670422A (zh) * | 2011-03-08 | 2012-09-19 | 花王株式会社 | 毛发化妆品 |
WO2015133382A1 (ja) * | 2014-03-06 | 2015-09-11 | ライオン株式会社 | ヘアコンディショナー組成物 |
WO2022144161A1 (en) * | 2020-12-30 | 2022-07-07 | Unilever Ip Holdings B.V. | Hair care composition |
-
2004
- 2004-06-07 JP JP2004168248A patent/JP4198641B2/ja not_active Expired - Fee Related
Cited By (15)
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EP1870080A1 (en) * | 2005-04-11 | 2007-12-26 | Kao Corporation | Hair cosmetic |
EP1870080A4 (en) * | 2005-04-11 | 2013-05-15 | Kao Corp | hair cosmetic |
JP2007262046A (ja) * | 2006-03-29 | 2007-10-11 | Sanei Kagaku Kk | ロウ類配合毛髪化粧料 |
JP2008297296A (ja) * | 2007-06-04 | 2008-12-11 | Hoyu Co Ltd | 毛髪処理用組成物 |
JP2010528101A (ja) * | 2007-06-15 | 2010-08-19 | ザ プロクター アンド ギャンブル カンパニー | アミン型カチオン性界面活性剤及び直接染料を含むヘアコンディショニング組成物 |
JP2009120558A (ja) * | 2007-11-16 | 2009-06-04 | Kracie Home Products Kk | ヘアリンス組成物 |
JP2011525543A (ja) * | 2008-06-25 | 2011-09-22 | ザ プロクター アンド ギャンブル カンパニー | ステアリルアミドプロピルジメチルアミンとl−グルタミン酸との塩を含有するヘアコンディショニング組成物 |
JP2010024169A (ja) * | 2008-07-17 | 2010-02-04 | Kracie Home Products Ltd | ヘアリンス組成物 |
US8101801B2 (en) | 2009-05-18 | 2012-01-24 | Xerox Corporation | Low molecular weight quaternary ammonium salt dispersants |
US8118922B2 (en) | 2009-05-18 | 2012-02-21 | Xerox Corporation | Pigmented phase change inks containing low molecular weight quaternary ammonium salt dispersants |
CN102670422A (zh) * | 2011-03-08 | 2012-09-19 | 花王株式会社 | 毛发化妆品 |
JP2012176995A (ja) * | 2012-06-21 | 2012-09-13 | Kao Corp | 毛髪化粧料 |
WO2015133382A1 (ja) * | 2014-03-06 | 2015-09-11 | ライオン株式会社 | ヘアコンディショナー組成物 |
JPWO2015133382A1 (ja) * | 2014-03-06 | 2017-04-06 | ライオン株式会社 | ヘアコンディショナー組成物 |
WO2022144161A1 (en) * | 2020-12-30 | 2022-07-07 | Unilever Ip Holdings B.V. | Hair care composition |
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