IT989178B - Procedimento per eliminare vinil cloruro residuo presente in poli meri - Google Patents

Procedimento per eliminare vinil cloruro residuo presente in poli meri

Info

Publication number
IT989178B
IT989178B IT2538173A IT2538173A IT989178B IT 989178 B IT989178 B IT 989178B IT 2538173 A IT2538173 A IT 2538173A IT 2538173 A IT2538173 A IT 2538173A IT 989178 B IT989178 B IT 989178B
Authority
IT
Italy
Prior art keywords
meri
poli
procedure
vinyl chloride
eliminate residual
Prior art date
Application number
IT2538173A
Other languages
English (en)
Original Assignee
Solvay
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Solvay filed Critical Solvay
Application granted granted Critical
Publication of IT989178B publication Critical patent/IT989178B/it

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24Stationary reactors without moving elements inside
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18Stationary reactors having moving elements inside
    • B01J19/20Stationary reactors having moving elements inside in the form of helices, e.g. screw reactors
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/18Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles
    • B01J8/24Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with fluidised particles according to "fluidised-bed" technique
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08FMACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
    • C08F6/00Post-polymerisation treatments
    • C08F6/001Removal of residual monomers by physical means
    • C08F6/005Removal of residual monomers by physical means from solid polymers
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00026Controlling or regulating the heat exchange system
    • B01J2208/00035Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/00044Temperature measurement
    • B01J2208/00061Temperature measurement of the reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00026Controlling or regulating the heat exchange system
    • B01J2208/00035Controlling or regulating the heat exchange system involving measured parameters
    • B01J2208/0007Pressure measurement
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00017Controlling the temperature
    • B01J2208/00106Controlling the temperature by indirect heat exchange
    • B01J2208/00168Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00256Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles in a heat exchanger for the heat exchange medium separate from the reactor
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00539Pressure
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008Controlling the process
    • B01J2208/00548Flow
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049Controlling or regulating processes
    • B01J2219/00051Controlling the temperature
    • B01J2219/00121Controlling the temperature by direct heating or cooling
    • B01J2219/00128Controlling the temperature by direct heating or cooling by evaporation of reactants
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/182Details relating to the spatial orientation of the reactor horizontal
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/18Details relating to the spatial orientation of the reactor
    • B01J2219/185Details relating to the spatial orientation of the reactor vertical
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/19Details relating to the geometry of the reactor
    • B01J2219/194Details relating to the geometry of the reactor round
    • B01J2219/1941Details relating to the geometry of the reactor round circular or disk-shaped
    • B01J2219/1946Details relating to the geometry of the reactor round circular or disk-shaped conical

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Combustion & Propulsion (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)
IT2538173A 1972-07-19 1973-06-14 Procedimento per eliminare vinil cloruro residuo presente in poli meri IT989178B (it)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
BE120023 1972-07-19
BE125979 1972-12-29

Publications (1)

Publication Number Publication Date
IT989178B true IT989178B (it) 1975-05-20

Family

ID=25647603

Family Applications (1)

Application Number Title Priority Date Filing Date
IT2538173A IT989178B (it) 1972-07-19 1973-06-14 Procedimento per eliminare vinil cloruro residuo presente in poli meri

Country Status (5)

Country Link
DE (1) DE2331895C2 (it)
FI (1) FI57423C (it)
FR (1) FR2193042A1 (it)
IT (1) IT989178B (it)
NL (1) NL172860C (it)

Families Citing this family (33)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2429776C3 (de) * 1974-06-21 1981-12-24 Hoechst Ag, 6000 Frankfurt Verfahren zur Entfernung von restlichem Vinylchlorid aus wäßrigen Polyvinylchloriddispersionen
DE2439203B2 (de) * 1974-08-16 1981-07-23 Hoechst Ag, 6000 Frankfurt Verfahren zur Entfernung von nicht umgesetztem, restlichen Vinchlorid aus wäßrigen Dispersionen von Vinylchloridpolymerisaten
DE2429777B2 (de) * 1974-06-21 1981-04-02 Hoechst Ag, 6000 Frankfurt Verfahren zur Entfernung von nicht ungesetztem, restlichem Vinylchlorid aus wäßrigen Dispersionen von Vinylchloridpolymerisaten
DE2463047C2 (it) * 1974-06-21 1988-02-04 Hoechst Ag, 6230 Frankfurt, De
US3956249A (en) * 1974-06-24 1976-05-11 Tenneco Chemicals, Inc. Manufacture of polyvinyl chloride of low vinyl chloride monomer content by treatment of wet polyvinyl chloride
IL47420A (en) * 1974-06-24 1978-07-31 Tenneco Chem Process for the removal of vinyl chloride from pvc slurries and latexes and pvc thus obtained
ES438975A1 (es) * 1974-08-14 1977-02-16 Solvay Un procedimiento para la eliminacion del cloruro de vinilo residual procedente de la polimerizacion en los polimeros decloruro de vinilo.
US4104459A (en) * 1974-08-19 1978-08-01 Ethyl Corporation Treating polyvinyl chloride resins
JPS5126988A (ja) * 1974-08-30 1976-03-05 Sumitomo Chemical Co Enkabinirukeijugotaichunizanzonsuru enkabinirutanryotai no jokyohoho
DE2450464A1 (de) * 1974-10-24 1976-04-29 Basf Ag Verfahren zur emissionsarmen entfernung von vinylchlorid aus polymerisaten des vinylchlorids
DE2453909B2 (de) * 1974-11-14 1977-03-17 Hoechst Ag, 6000 Frankfurt Verfahren zur herstellung von verarbeitungsfertigen pulverfoermigen mischungen auf basis von vinylchlorid-polymerisaten
JPS5169587A (en) * 1974-12-13 1976-06-16 Tetsukosha Kk Jugotaichuno zanzonenkabinirutanryotaijokyohoho
DE2500765C3 (de) * 1975-01-10 1983-03-03 Chemische Werke Hüls AG, 4370 Marl Verfahren zur Verringerung des Gehaltes an monomerem Vinylchlorid in durch Massepolymerisation hergestelltem Polyvinylchlorid
JPS6020402B2 (ja) * 1975-02-25 1985-05-22 チッソ株式会社 塩化ビニル樹脂から微量の塩化ビニル単量体を分離する方法
US4031056A (en) * 1975-02-27 1977-06-21 Tenneco Chemicals, Inc. Process for the removal of vinyl chloride from latexes containing polyvinyl chloride
US4217444A (en) * 1975-03-28 1980-08-12 Rhone-Poulenc Industries Method of degassing polymers prepared by mass polymerizing a monomeric composition based on vinyl chloride
FR2305446A1 (fr) * 1975-03-28 1976-10-22 Rhone Poulenc Ind Procede ameliore de degazage des polymeres et copolymeres prepares par polymerisation en masse d'une composition monomere a base de chlorure de vinyle
JPS51127187A (en) * 1975-04-26 1976-11-05 Kureha Chem Ind Co Ltd A process and an apparatus for recovering monomers
JPS51149389A (en) * 1975-05-14 1976-12-22 Sumitomo Chem Co Ltd A method to decrease the vinyl chloride monomer remaining in the polyv inyl chloride resin slurry
US4171427A (en) * 1975-05-16 1979-10-16 Hoechst Aktiengesellschaft Process for continuously removing monomers from an aqueous dispersion of a polymer
JPS51135990A (en) * 1975-05-20 1976-11-25 Shin Etsu Chem Co Ltd Method of removing residual monomers f rom polyvinylchloride slurries
FR2312514A1 (fr) * 1975-05-26 1976-12-24 Solvay Procede pour la polymerisation du chlorure de vinyle en suspension aqueuse
IL50060A (en) * 1975-08-13 1979-09-30 Tenneco Chem Process for the removal of vinyl chloride from polyvinyl chloride latexes and slurries
GB1547614A (en) * 1975-09-15 1979-06-27 Tenneco Chem Removing residual monomer from vinyl chloryde polymers
US4168373A (en) * 1975-11-24 1979-09-18 Borden, Inc. Removal of residual vinyl chloride monomer from polyvinyl chloride latex
JPS5813563B2 (ja) * 1976-04-03 1983-03-14 信越化学工業株式会社 塩化ビニルの水性分散液から未反応モノマ−を除去する方法およびその装置
US4226976A (en) * 1976-09-20 1980-10-07 Tenneco Chemicals, Inc. Process for the removal of vinyl chloride from polyvinyl chloride latexes and slurries with hydrocarbon compounds
DE2653256C2 (de) * 1976-11-24 1983-02-17 Hoechst Ag, 6000 Frankfurt Verfahren zur Senkung des Restmonomerengehaltes von Vinylchlorid-Polymerisaten
US4226974A (en) * 1977-01-21 1980-10-07 Tenneco Chemicals, Inc. Process for the removal of vinyl chloride from polyvinyl chloride latexes and slurries
US4219640A (en) * 1977-09-22 1980-08-26 Tenneco Chemicals, Inc. Polymers of vinyl chloride having low vinyl chloride monomer content, and method of making same
US4229569A (en) * 1979-02-05 1980-10-21 Tenneco Chemicals, Inc. Process for the removal of vinyl chloride from aqueous slurries of vinyl chloride polymers
DE3122614A1 (de) * 1981-06-06 1983-01-05 Hoechst Ag, 6000 Frankfurt "verfahren zur polymerisation von vinylchlorid in der masse"
CN111841453B (zh) * 2020-06-18 2022-08-23 西北大学 一种应用于热重分析的微型流化床反应装置

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE954920C (de) * 1955-02-19 1956-12-27 Hoechst Ag Verfahren zum Aufarbeiten von Emulsionen von Polyvinylverbindungen, insbesondere Polyvinylchlorid
NL126831C (it) * 1963-10-24
NL6501687A (it) * 1964-02-12 1965-08-13
BE686088A (it) * 1966-08-29 1967-02-28
US3622553A (en) * 1967-12-18 1971-11-23 Phillips Petroleum Co Agitated reactor and gas fluidized bed reactor in series for polymerization of vinyl chloride
DE2442931B2 (de) * 1974-09-07 1976-11-04 Chemische Werke Hüls AG, 4370 Mari Verfahren zur entfernung von nicht umgesetztem vinylchlorid aus waessrigen polyvinylchlorid-dispersionen

Also Published As

Publication number Publication date
FI57423B (fi) 1980-04-30
FR2193042B1 (it) 1976-05-28
DE2331895A1 (de) 1974-01-31
FI57423C (fi) 1980-08-11
NL172860C (nl) 1986-02-17
FR2193042A1 (en) 1974-02-15
DE2331895C2 (de) 1989-04-06
NL172860B (nl) 1983-06-01
NL7309808A (it) 1974-01-22

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