HRP20210363T1 - Energetski učinkovit i ekološki prihvatljiv postupak proizvodnje furfurala iz lignoceluloznog materijala - Google Patents
Energetski učinkovit i ekološki prihvatljiv postupak proizvodnje furfurala iz lignoceluloznog materijala Download PDFInfo
- Publication number
- HRP20210363T1 HRP20210363T1 HRP20210363TT HRP20210363T HRP20210363T1 HR P20210363 T1 HRP20210363 T1 HR P20210363T1 HR P20210363T T HRP20210363T T HR P20210363TT HR P20210363 T HRP20210363 T HR P20210363T HR P20210363 T1 HRP20210363 T1 HR P20210363T1
- Authority
- HR
- Croatia
- Prior art keywords
- steam
- furfural
- separation
- lignocellulosic material
- separation device
- Prior art date
Links
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 title claims 26
- 238000000034 method Methods 0.000 title claims 12
- 239000012978 lignocellulosic material Substances 0.000 title claims 10
- 238000004519 manufacturing process Methods 0.000 title claims 4
- 238000000926 separation method Methods 0.000 claims 15
- 239000012071 phase Substances 0.000 claims 5
- 238000001179 sorption measurement Methods 0.000 claims 3
- 230000005494 condensation Effects 0.000 claims 2
- 238000009833 condensation Methods 0.000 claims 2
- 238000010438 heat treatment Methods 0.000 claims 2
- 238000004064 recycling Methods 0.000 claims 2
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 claims 1
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 claims 1
- 239000008346 aqueous phase Substances 0.000 claims 1
- 238000011084 recovery Methods 0.000 claims 1
- 230000009466 transformation Effects 0.000 claims 1
Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0215—Solid material in other stationary receptacles
- B01D11/0223—Moving bed of solid material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D11/00—Solvent extraction
- B01D11/02—Solvent extraction of solids
- B01D11/0292—Treatment of the solvent
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/16—Alumino-silicates
- B01J20/18—Synthetic zeolitic molecular sieves
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/51—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition
- C07C45/55—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by pyrolysis, rearrangement or decomposition of oligo- or polymeric oxo-compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/31—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation of cyclic compounds with ring-splitting
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D307/00—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom
- C07D307/02—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings
- C07D307/34—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D307/38—Heterocyclic compounds containing five-membered rings having one oxygen atom as the only ring hetero atom not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with substituted hydrocarbon radicals attached to ring carbon atoms
- C07D307/40—Radicals substituted by oxygen atoms
- C07D307/46—Doubly bound oxygen atoms, or two oxygen atoms singly bound to the same carbon atom
- C07D307/48—Furfural
- C07D307/50—Preparation from natural products
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08H—DERIVATIVES OF NATURAL MACROMOLECULAR COMPOUNDS
- C08H8/00—Macromolecular compounds derived from lignocellulosic materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E50/00—Technologies for the production of fuel of non-fossil origin
- Y02E50/10—Biofuels, e.g. bio-diesel
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Polymers & Plastics (AREA)
- Health & Medical Sciences (AREA)
- Materials Engineering (AREA)
- Medicinal Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Preparation Of Compounds By Using Micro-Organisms (AREA)
- Processing Of Solid Wastes (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Claims (12)
1. Postupak proizvodnje furfurala iz lignoceluloznog materijala se sastoji od slijedećih koraka:
a) obrade lignoceluloznog materijala parom;
b) odvajanja pare koja sadrži furfural od obrađenog lignoceluloznog materijala;
c) prijenos izdvojene pare do uređaja za odvajanje;
d) razdvajanja faze koja sadrži furfural od pare;
e) podvrgavanja pare stupnju iskorištavanja;
naznačen time da se razdvajanje prema koraku d) se vrši adsorbcijom i gdje je stupanj iskorištenja e) zagrijavanje.
2. Postupak prema patentnom zahtjevu 1, naznačen time da razdvajanje uključuje parnu transformaciju pare koja sadrži furfural.
3. Postupak prema patentnom zahtjevu 2, naznačen time da razdvajanje uključuje dekantiranje faze koja sadrži furfural iz transformirane pare.
4. Postupak prema patentnom zahtjevu 3, naznačen time da rezidualna vodenasta faza je reciklirana do koraka d) nakon dekantiranja faze koja sadrži furfural.
5. Postupak prema bilo kojem od prethodnih patentnih zahtjeva, naznačen time da dalje obuhvaća korak f) kondenzaciju iskorištene pare iz koraka e).
6. Postupak prema bilo kojem od prethodnih patentnih zahtjeva, naznačen time da dalje sadrži korak g) recikliranja iskorištene pare.
7. Postupak prema patentnom zahtjevu 6, naznačen time da se iskorištena para reciklira do koraka a) postupka.
8. Postupak proizvodnje furfurala iz lignoceluloznog materijala se sastoji od slijedećih koraka:
a) obrade lignoceluloznog materijala parom;
b) odvajanja pare koja sadrži furfural od obrađenog lignoceluloznog materijala; b1) podvrgavanja izdvojene pare koraku iskorištavanja;
c1) prijenos mlaza iskorištene pare u uređaj za razdvajanje;
d1) razdvajanje faze koja sadrži furfural od mlaza iskorištene pare;
g1) recikliranja mlaza iz koraka d1) naznačeno time da se razdvajanje prema koraku d1) provodi adsorpcijom i pri čemu se stupanj iskorištenja b1) zagrijava.
9. Sustav za postupak proizvodnje furfurala iz lignoceluloznog materijala se sastoji od:
i) reaktora za obradu lignoceluloznog materijala prema koraku a) postupka kako je određeno prema bilo kojem patentnom zahtjevu 1 do 8;
ii) uređaja za odvajanje pare a za odvajanje pare koja sadrži furfural od tretiranog lignoceluloznog materijala prema koraku b) postupka kako je određeno prema bilo kojem patentnom zahtjevu 1 do 8;
iii) uređaja za razdvajanje pare a za razdvajanje faze koja sadrži furfural od pare prema koraku d) kako je određeno u bilo kojem patentnom zahtjevu 1 do 8;
iv) uređaja za iskorištavanje, a za iskorištavanje energije pare,
naznačen time da uređaj za razdvajanje pare (iii) je adsorpcijsi stup, a uređaj za iskorištavanje (iv) je uređaj za zagrijavanje.
10. Sustav prema patentnom zahtjevu 9, naznačen time da dalje sadrži kondenzator (v) za kondenzaciju iskorištene pare.
11. Sustav prema patentnom zahtjevu 9 ili 10, naznačen time da uređaj za razdvajanje pare (iii) sadrži transformator pare.
12. Sustav prema bilo kojem patentnom zahtjevu 9 do 11, naznačen time da uređaj za razdvajanje (iii) sadrži dekanter.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP14002758.2A EP2982703A1 (en) | 2014-08-06 | 2014-08-06 | Energy-efficient and environmentally friendly process for the production of target chemical compounds from cellulosic material |
| EP15757144.9A EP3177672B1 (en) | 2014-08-06 | 2015-07-30 | Energy-efficient and environmentally friendly process for the production of furfural from lignocellulosic material |
| PCT/EP2015/067573 WO2016020269A1 (en) | 2014-08-06 | 2015-07-30 | Energy-efficient and environmentally friendly process for the production of target chemical compounds from cellulosic material |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| HRP20210363T1 true HRP20210363T1 (hr) | 2021-04-16 |
Family
ID=51298513
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| HRP20210363TT HRP20210363T1 (hr) | 2014-08-06 | 2021-03-03 | Energetski učinkovit i ekološki prihvatljiv postupak proizvodnje furfurala iz lignoceluloznog materijala |
Country Status (18)
| Country | Link |
|---|---|
| US (2) | US10202358B2 (hr) |
| EP (3) | EP2982703A1 (hr) |
| CN (2) | CN106573866A (hr) |
| AR (1) | AR102807A1 (hr) |
| AU (2) | AU2015299202B2 (hr) |
| BR (1) | BR112017002405B8 (hr) |
| CA (2) | CA2958113C (hr) |
| DK (1) | DK3177672T3 (hr) |
| EA (1) | EA201790320A1 (hr) |
| ES (1) | ES2848324T3 (hr) |
| HR (1) | HRP20210363T1 (hr) |
| HU (1) | HUE053597T2 (hr) |
| MY (1) | MY177516A (hr) |
| PL (1) | PL3177672T3 (hr) |
| PT (1) | PT3177672T (hr) |
| RS (1) | RS61537B1 (hr) |
| SI (1) | SI3177672T1 (hr) |
| WO (1) | WO2016020269A1 (hr) |
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP2982703A1 (en) * | 2014-08-06 | 2016-02-10 | Clariant International Ltd. | Energy-efficient and environmentally friendly process for the production of target chemical compounds from cellulosic material |
| FI129729B (en) * | 2016-12-30 | 2022-08-15 | Upm Kymmene Corp | Method and apparatus for recovering furfural |
| FI129405B (en) * | 2016-12-30 | 2022-01-31 | Upm Kymmene Corp | Method and apparatus for separating furfural |
| DE102017207817A1 (de) * | 2017-05-09 | 2018-11-15 | Clariant International Ltd | Zeolithhaltiges Adsorbens zur selektiven Abtrennung von Isomeren aus aromatischen Kohlenwasserstoffgemischen, seine Herstellung und Verwendung |
| CN108325236B (zh) * | 2018-03-23 | 2020-05-08 | 青岛大学附属医院 | 一种药学用压榨型连续中药萃取装置 |
| SE2050186A1 (en) * | 2020-02-20 | 2021-03-09 | Valmet Oy | Recovery of energy and chemicals from a steam explosion process |
| FI128936B (en) * | 2020-03-11 | 2021-03-31 | Luonnonvarakeskus | RECOVERY OF VALUE COMPONENTS FROM BIOMASS |
| WO2023192421A1 (en) | 2022-03-30 | 2023-10-05 | Donaldson Company, Inc. | System and method for reclaiming solvent |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4136207A (en) * | 1977-01-24 | 1979-01-23 | Stake Technology Ltd. | Method of treating lignocellulose materials to produce ruminant feed |
| SU1648547A1 (ru) * | 1989-05-24 | 1991-05-15 | Грозненский Филиал Всесоюзного Научно-Исследовательского И Проектно-Конструкторского Института Биологической Техники | Адсорбент дл очистки фурфурола |
| EA011136B1 (ru) | 2004-08-31 | 2008-12-30 | Биотек Прогресс, А.С. | Способ и устройство для непрерывной переработки возобновляемого сырья |
| BRPI0809289A2 (pt) | 2007-03-19 | 2014-10-14 | Sued Chemie Ag | Geração de blocos de construção química a partir de biomassa vegeral por despolimerização seletiva |
| EP2421912B1 (en) * | 2009-04-23 | 2018-07-11 | Greenfield Ethanol Inc. | Fractionation of biomass for cellulosic ethanol and chemical production |
| EP2679690A1 (en) * | 2009-06-23 | 2014-01-01 | American Process, Inc. | Process for producing alcohol and other bioproducts from biomass used in thermal conversion to energy and stepwise enzymatic hydrolysis process for cellulosic fiber |
| ES2630053T3 (es) * | 2009-09-29 | 2017-08-17 | Nova Pangaea Technologies Limited | Método y sistema para el fraccionamiento de biomasa lignocelulósica |
| US8236973B2 (en) * | 2009-11-05 | 2012-08-07 | Battelle Memorial Institute | Adsorption separation processes for ionic liquid catalytic processes |
| KR20110088841A (ko) | 2010-01-29 | 2011-08-04 | 주식회사에이앤에이엠디 | 풍선 카테터 및 이를 이용한 혈관확장장치 |
| WO2012041990A1 (en) | 2010-09-30 | 2012-04-05 | Shell Internationale Research Maatschappij B.V. | Process for producing furfural |
| ES2507240T3 (es) | 2010-12-23 | 2014-10-14 | Clariant Produkte (Deutschland) Gmbh | Procedimiento para la preparación de compuestos orgánicos a través de fermentación de biomasa y catálisis zeolítica |
| EP2471940A1 (en) | 2010-12-31 | 2012-07-04 | Süd-Chemie AG | Efficient lignocellulose hydrolysis with integrated enzyme production |
| PT2537841E (pt) | 2011-06-22 | 2013-12-19 | Dsm Ip Assets Bv | Produção continua de furfural e de ácido levulínico |
| US20140171664A1 (en) | 2011-08-12 | 2014-06-19 | E I Du Pont De Nemours And Company | Furfural production from biomass |
| EP2623607A1 (en) | 2012-02-02 | 2013-08-07 | Sekab E-Technology AB | Method and system for production of a target chemical from a cellulosic material |
| CN103214439B (zh) * | 2013-04-09 | 2016-03-02 | 江苏清泉化学股份有限公司 | 一种分离提纯糠醛的方法 |
| EP2982703A1 (en) * | 2014-08-06 | 2016-02-10 | Clariant International Ltd. | Energy-efficient and environmentally friendly process for the production of target chemical compounds from cellulosic material |
-
2014
- 2014-08-06 EP EP14002758.2A patent/EP2982703A1/en not_active Withdrawn
-
2015
- 2015-07-30 ES ES15757144T patent/ES2848324T3/es active Active
- 2015-07-30 BR BR112017002405A patent/BR112017002405B8/pt active IP Right Grant
- 2015-07-30 WO PCT/EP2015/067573 patent/WO2016020269A1/en active Application Filing
- 2015-07-30 MY MYPI2017700143A patent/MY177516A/en unknown
- 2015-07-30 SI SI201531540T patent/SI3177672T1/sl unknown
- 2015-07-30 RS RS20210257A patent/RS61537B1/sr unknown
- 2015-07-30 AU AU2015299202A patent/AU2015299202B2/en not_active Ceased
- 2015-07-30 CA CA2958113A patent/CA2958113C/en active Active
- 2015-07-30 DK DK15757144.9T patent/DK3177672T3/da active
- 2015-07-30 PL PL15757144T patent/PL3177672T3/pl unknown
- 2015-07-30 PT PT157571449T patent/PT3177672T/pt unknown
- 2015-07-30 EA EA201790320A patent/EA201790320A1/ru unknown
- 2015-07-30 US US15/501,482 patent/US10202358B2/en active Active
- 2015-07-30 HU HUE15757144A patent/HUE053597T2/hu unknown
- 2015-07-30 CN CN201580042443.XA patent/CN106573866A/zh active Pending
- 2015-07-30 EP EP20207125.4A patent/EP3822304A1/en not_active Withdrawn
- 2015-07-30 EP EP15757144.9A patent/EP3177672B1/en active Active
- 2015-07-30 CA CA3084195A patent/CA3084195A1/en not_active Abandoned
- 2015-07-30 CN CN202010577456.XA patent/CN111689842A/zh active Pending
- 2015-08-05 AR ARP150102505A patent/AR102807A1/es active IP Right Grant
-
2018
- 2018-08-29 AU AU2018222944A patent/AU2018222944B2/en not_active Ceased
-
2019
- 2019-02-12 US US16/273,619 patent/US10968191B2/en active Active
-
2021
- 2021-03-03 HR HRP20210363TT patent/HRP20210363T1/hr unknown
Also Published As
| Publication number | Publication date |
|---|---|
| BR112017002405A2 (pt) | 2017-12-05 |
| US20190177292A1 (en) | 2019-06-13 |
| EP3177672A1 (en) | 2017-06-14 |
| SI3177672T1 (sl) | 2021-04-30 |
| PT3177672T (pt) | 2021-02-15 |
| EP3822304A1 (en) | 2021-05-19 |
| CA2958113A1 (en) | 2016-02-11 |
| EP2982703A1 (en) | 2016-02-10 |
| AR102807A1 (es) | 2017-03-29 |
| CA3084195A1 (en) | 2016-02-11 |
| DK3177672T3 (da) | 2021-02-01 |
| BR112017002405B1 (pt) | 2021-08-24 |
| CN111689842A (zh) | 2020-09-22 |
| US20170233359A1 (en) | 2017-08-17 |
| AU2018222944B2 (en) | 2020-05-21 |
| WO2016020269A1 (en) | 2016-02-11 |
| AU2015299202A1 (en) | 2017-02-16 |
| RS61537B1 (sr) | 2021-04-29 |
| CA2958113C (en) | 2020-08-25 |
| MY177516A (en) | 2020-09-17 |
| PL3177672T3 (pl) | 2021-06-14 |
| HUE053597T2 (hu) | 2021-07-28 |
| BR112017002405B8 (pt) | 2022-08-30 |
| EA201790320A1 (ru) | 2017-06-30 |
| US10202358B2 (en) | 2019-02-12 |
| AU2015299202B2 (en) | 2018-05-31 |
| EP3177672B1 (en) | 2020-12-09 |
| ES2848324T3 (es) | 2021-08-06 |
| AU2018222944A1 (en) | 2018-09-20 |
| CN106573866A (zh) | 2017-04-19 |
| US10968191B2 (en) | 2021-04-06 |
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