GB892886A - A process for the production of colour photographs and silver halide emulsion layers for use in the production of colour photographs - Google Patents
A process for the production of colour photographs and silver halide emulsion layers for use in the production of colour photographsInfo
- Publication number
- GB892886A GB892886A GB3674758A GB3674758A GB892886A GB 892886 A GB892886 A GB 892886A GB 3674758 A GB3674758 A GB 3674758A GB 3674758 A GB3674758 A GB 3674758A GB 892886 A GB892886 A GB 892886A
- Authority
- GB
- United Kingdom
- Prior art keywords
- sulphophenyl
- pyrazolone
- stearyl
- amino
- prepared
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D417/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00
- C07D417/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00 containing two hetero rings
- C07D417/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and sulfur atoms as the only ring hetero atoms, not provided for by group C07D415/00 containing two hetero rings linked by a chain containing hetero atoms as chain links
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
- C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
- C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
- C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D231/18—One oxygen or sulfur atom
- C07D231/20—One oxygen atom attached in position 3 or 5
- C07D231/22—One oxygen atom attached in position 3 or 5 with aryl radicals attached to ring nitrogen atoms
- C07D231/26—1-Phenyl-3-methyl-5- pyrazolones, unsubstituted or substituted on the phenyl ring
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B39/00—Other azo dyes prepared by diazotising and coupling
-
- G—PHYSICS
- G03—PHOTOGRAPHY; CINEMATOGRAPHY; ANALOGOUS TECHNIQUES USING WAVES OTHER THAN OPTICAL WAVES; ELECTROGRAPHY; HOLOGRAPHY
- G03C—PHOTOSENSITIVE MATERIALS FOR PHOTOGRAPHIC PURPOSES; PHOTOGRAPHIC PROCESSES, e.g. CINE, X-RAY, COLOUR, STEREO-PHOTOGRAPHIC PROCESSES; AUXILIARY PROCESSES IN PHOTOGRAPHY
- G03C7/00—Multicolour photographic processes or agents therefor; Regeneration of such processing agents; Photosensitive materials for multicolour processes
- G03C7/30—Colour processes using colour-coupling substances; Materials therefor; Preparing or processing such materials
- G03C7/32—Colour coupling substances
- G03C7/36—Couplers containing compounds with active methylene groups
- G03C7/38—Couplers containing compounds with active methylene groups in rings
- G03C7/384—Couplers containing compounds with active methylene groups in rings in pyrazolone rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- General Physics & Mathematics (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1 - (o - Amino - p - sulphophenyl) - 3 - stearyl - 5 - pyrazolone is prepared by mixing 2-nitrophenyl-hydrazine-4-sulphonic acid with a -stearoyl ethyl acetate and sodium acetate in isopropanol, adding caustic soda and heating. The nitrocompound formed is reduced to the corresponding amino compound with catalytic hydrogen under pressure. Instead of the above hydrazine, 2 - b - chloroethylamino - 5 - sulphophenyl - hydrazine may be employed to give the corresponding 1 - (2 - b - chloroethylamino - 5 - sulpho - phenyl)-pyrazolone. 1 - [2 - (g - sulphopropylamino) - 4 - sulpho - phenyl]-3-stearyl-5-pyrazolone is prepared by reacting 1 - (2 - amino - 4 - sulphophenyl) - 3 - stearyl-5-pyrazolone with propane sultone. The latter pyrazolone also may be reacted with butane sultone, 4-chloro-3-nitrobenzene-1-sulphonic acid, chloracetic acid, 2-chlorobenzthiazole, m-nitrobenzyl chloride, acrylonitrile, benzoyl chloride, phenyl isocyanate or benzene sulphonyl chloride, to give 1-(2-substituted amino - 4 - sulphophenyl) - 3 - stearyl - 5 - pyrazo - lones wherein the substituent in the amino group is g -sulphobutyl, 2-nitro-4-sulphophenyl (the nitro group of which may be reduced to the corresponding amine), carboxymethyl, 2-benzthiazolyl, m-nitro-benzyl (the nitro group of which may be reduced to the corresponding amine), b -cyanoethyl, benzoyl, phenylcarbamyl and phenylsulpho. 1 - { 2- [2 (g - sulphobutylamino) - 4 - sulpho - phenylamino] - 4 - sulphophenyl} - 3 - stearyl - 5 - pyrazolone is prepared by refluxing 1-[2-(2-amino - 4 - sulphophenylamino) - 4 - sulpho - phenyl]-3-stearyl-5-pyrazolone with butane sultone in ethanol. 1 - {2 - [m - (g - sulphobutylamino) - benzyl - amino] - 4 - sulphophenyl} - 3 - stearyl - 5 - pyrazolone is prepared by refluxing 1-[2-(m-aminobenzylamino) - 4 - sulphophenyl] - 3 - stearyl-5-pyrazolone with butane sultone in ethanol. Bis N, N1 - [2 - (3 - stearyl - 5 - keto - 1 - pyrazolinyl) - 5 - sulphophenyl] ethylene diamine is prepared by refluxing 1-(2-amino-4-sulphophenyl)-3-stearyl-5-pyrazolone and ethylene dibromide in ethanol.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEA28314A DE1046496B (en) | 1957-11-14 | 1957-11-14 | Process for the production of color photographic images by chromogenic development |
Publications (1)
Publication Number | Publication Date |
---|---|
GB892886A true GB892886A (en) | 1962-04-04 |
Family
ID=6926628
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB3674758A Expired GB892886A (en) | 1957-11-14 | 1958-11-14 | A process for the production of colour photographs and silver halide emulsion layers for use in the production of colour photographs |
Country Status (4)
Country | Link |
---|---|
BE (1) | BE572971A (en) |
DE (1) | DE1046496B (en) |
FR (1) | FR1214365A (en) |
GB (1) | GB892886A (en) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE1070030B (en) * | 1958-06-21 | 1959-11-26 | ||
BE590403A (en) * | 1959-04-30 | |||
DE1155979B (en) * | 1961-10-24 | 1963-10-17 | Eastman Kodak Co | Color development processes with 5-pyrazolone derivative color couplers and photographic emulsions used therefor |
DE1150577B (en) * | 1961-12-05 | 1963-06-20 | Ferrania Spa | Color coupler for emulsion or developer containing colored development |
DE1150872B (en) * | 1962-04-17 | 1963-06-27 | Adox Fotowerke Dr C Schleussne | Process for the production of monochrome or multicolor photographic images by chromogenic development of halogen silver emulsion layers |
DE1299224B (en) * | 1963-02-14 | 1969-07-10 | Agfa Ag | Process for producing color photographic images |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2353205A (en) * | 1939-03-31 | 1944-07-11 | Eastman Kodak Co | Color-forming compound containing sulphonamide groups |
US2396917A (en) * | 1942-09-15 | 1946-03-19 | Du Pont | Dye intermediates |
US2411951A (en) * | 1944-09-28 | 1946-12-03 | Gen Aniline & Film Corp | 4,4'-bis (pyrazolone) couplers for color photography |
-
0
- BE BE572971D patent/BE572971A/xx unknown
-
1957
- 1957-11-14 DE DEA28314A patent/DE1046496B/en active Pending
-
1958
- 1958-11-14 GB GB3674758A patent/GB892886A/en not_active Expired
- 1958-11-14 FR FR1214365D patent/FR1214365A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
FR1214365A (en) | 1960-04-08 |
DE1046496B (en) | 1958-12-11 |
BE572971A (en) |
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