GB595148A - Improvements in or relating to the electrodeposition of lead - Google Patents
Improvements in or relating to the electrodeposition of leadInfo
- Publication number
- GB595148A GB595148A GB343945A GB343945A GB595148A GB 595148 A GB595148 A GB 595148A GB 343945 A GB343945 A GB 343945A GB 343945 A GB343945 A GB 343945A GB 595148 A GB595148 A GB 595148A
- Authority
- GB
- United Kingdom
- Prior art keywords
- reacted
- ethylene oxide
- acids
- residue
- oxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000004070 electrodeposition Methods 0.000 title 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Natural products OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 5
- 150000001875 compounds Chemical class 0.000 abstract 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N oxane Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 abstract 4
- CSCPPACGZOOCGX-UHFFFAOYSA-N acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 abstract 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 3
- LYCAIKOWRPUZTN-UHFFFAOYSA-N glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 3
- -1 polyethylene, propylene, butylene Polymers 0.000 abstract 3
- ZWEHNKRNPOVVGH-UHFFFAOYSA-N 2-butanone Chemical compound CCC(C)=O ZWEHNKRNPOVVGH-UHFFFAOYSA-N 0.000 abstract 2
- HUMNYLRZRPPJDN-UHFFFAOYSA-N Benzaldehyde Chemical compound O=CC1=CC=CC=C1 HUMNYLRZRPPJDN-UHFFFAOYSA-N 0.000 abstract 2
- YCIMNLLNPGFGHC-UHFFFAOYSA-N Catechol Chemical compound OC1=CC=CC=C1O YCIMNLLNPGFGHC-UHFFFAOYSA-N 0.000 abstract 2
- DTUQWGWMVIHBKE-UHFFFAOYSA-N Phenylacetaldehyde Chemical compound O=CCC1=CC=CC=C1 DTUQWGWMVIHBKE-UHFFFAOYSA-N 0.000 abstract 2
- 239000004721 Polyphenylene oxide Substances 0.000 abstract 2
- WUOACPNHFRMFPN-UHFFFAOYSA-N Terpineol Chemical group CC1=CCC(C(C)(C)O)CC1 WUOACPNHFRMFPN-UHFFFAOYSA-N 0.000 abstract 2
- IKHGUXGNUITLKF-UHFFFAOYSA-N acetaldehyde Chemical compound CC=O IKHGUXGNUITLKF-UHFFFAOYSA-N 0.000 abstract 2
- 150000001298 alcohols Chemical class 0.000 abstract 2
- 125000002947 alkylene group Chemical group 0.000 abstract 2
- YXVFYQXJAXKLAK-UHFFFAOYSA-N biphenyl-4-ol Chemical group C1=CC(O)=CC=C1C1=CC=CC=C1 YXVFYQXJAXKLAK-UHFFFAOYSA-N 0.000 abstract 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 abstract 2
- 229920000570 polyether Polymers 0.000 abstract 2
- KLRNMDPLGYEZCJ-AOWDYJTJSA-N (2S,3R)-butane-1,2,3,4-tetrol;(2R,3R,4R,5S)-hexane-1,2,3,4,5,6-hexol Chemical compound OC[C@H](O)[C@H](O)CO.OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)CO KLRNMDPLGYEZCJ-AOWDYJTJSA-N 0.000 abstract 1
- SPEUIVXLLWOEMJ-UHFFFAOYSA-N 1,1-dimethoxyethane Chemical compound COC(C)OC SPEUIVXLLWOEMJ-UHFFFAOYSA-N 0.000 abstract 1
- KJCVRFUGPWSIIH-UHFFFAOYSA-N 1-Naphthol Chemical compound C1=CC=C2C(O)=CC=CC2=C1 KJCVRFUGPWSIIH-UHFFFAOYSA-N 0.000 abstract 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N 2,2-bis(hydroxymethyl)propane-1,3-diol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 abstract 1
- WNJSKZBEWNVKGU-UHFFFAOYSA-N 2,2-dimethoxyethylbenzene Chemical compound COC(OC)CC1=CC=CC=C1 WNJSKZBEWNVKGU-UHFFFAOYSA-N 0.000 abstract 1
- WPYMKLBDIGXBTP-UHFFFAOYSA-N Benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 abstract 1
- 239000004215 Carbon black (E152) Substances 0.000 abstract 1
- 239000001263 FEMA 3042 Substances 0.000 abstract 1
- UHUFTBALEZWWIH-UHFFFAOYSA-N Myristyl aldehyde Chemical compound CCCCCCCCCCCCCC=O UHUFTBALEZWWIH-UHFFFAOYSA-N 0.000 abstract 1
- 229920003171 Poly (ethylene oxide) Polymers 0.000 abstract 1
- KRIOVPPHQSLHCZ-UHFFFAOYSA-N Propiophenone Chemical compound CCC(=O)C1=CC=CC=C1 KRIOVPPHQSLHCZ-UHFFFAOYSA-N 0.000 abstract 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N Stearic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 abstract 1
- 239000005864 Sulphur Substances 0.000 abstract 1
- 229940033123 Tannic Acid Drugs 0.000 abstract 1
- LRBQNJMCXXYXIU-NRMVVENXSA-N Tannic acid Chemical compound OC1=C(O)C(O)=CC(C(=O)OC=2C(=C(O)C=C(C=2)C(=O)OC[C@@H]2[C@H]([C@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)[C@@H](OC(=O)C=3C=C(OC(=O)C=4C=C(O)C(O)=C(O)C=4)C(O)=C(O)C=3)O2)OC(=O)C=2C=C(OC(=O)C=3C=C(O)C(O)=C(O)C=3)C(O)=C(O)C=2)O)=C1 LRBQNJMCXXYXIU-NRMVVENXSA-N 0.000 abstract 1
- 229940116411 Terpineol Drugs 0.000 abstract 1
- FRPZMMHWLSIFAZ-UHFFFAOYSA-N Undecylenic acid Chemical class OC(=O)CCCCCCCCC=C FRPZMMHWLSIFAZ-UHFFFAOYSA-N 0.000 abstract 1
- 150000001241 acetals Chemical class 0.000 abstract 1
- QTBSBXVTEAMEQO-UHFFFAOYSA-N acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 150000007513 acids Chemical class 0.000 abstract 1
- 150000001299 aldehydes Chemical class 0.000 abstract 1
- 150000001408 amides Chemical class 0.000 abstract 1
- 150000001412 amines Chemical class 0.000 abstract 1
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 1
- 229940095076 benzaldehyde Drugs 0.000 abstract 1
- KXDAEFPNCMNJSK-UHFFFAOYSA-N benzamide Chemical compound NC(=O)C1=CC=CC=C1 KXDAEFPNCMNJSK-UHFFFAOYSA-N 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 150000001896 cresols Chemical class 0.000 abstract 1
- XDTMQSROBMDMFD-UHFFFAOYSA-N cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 abstract 1
- 150000002170 ethers Chemical class 0.000 abstract 1
- QUSNBJAOOMFDIB-UHFFFAOYSA-N ethyl amine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 125000004435 hydrogen atoms Chemical class [H]* 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- 150000002576 ketones Chemical class 0.000 abstract 1
- 150000002689 maleic acids Chemical class 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 abstract 1
- 150000002763 monocarboxylic acids Chemical class 0.000 abstract 1
- LYRFLYHAGKPMFH-UHFFFAOYSA-N octadecanamide Chemical compound CCCCCCCCCCCCCCCCCC(N)=O LYRFLYHAGKPMFH-UHFFFAOYSA-N 0.000 abstract 1
- MUBZPKHOEPUJKR-UHFFFAOYSA-N oxalic acid Chemical compound OC(=O)C(O)=O MUBZPKHOEPUJKR-UHFFFAOYSA-N 0.000 abstract 1
- MYMOFIZGZYHOMD-UHFFFAOYSA-N oxygen Chemical group O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 abstract 1
- 239000001301 oxygen Substances 0.000 abstract 1
- 229910052760 oxygen Inorganic materials 0.000 abstract 1
- 125000000913 palmityl group Chemical group [H]C([*])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])C([H])([H])[H] 0.000 abstract 1
- 229960001735 pentaerythritol Drugs 0.000 abstract 1
- 150000002989 phenols Chemical class 0.000 abstract 1
- 229940100595 phenylacetaldehyde Drugs 0.000 abstract 1
- 125000000286 phenylethyl group Chemical group [H]C1=C([H])C([H])=C(C([H])=C1[H])C([H])([H])C([H])([H])* 0.000 abstract 1
- 150000003022 phthalic acids Chemical class 0.000 abstract 1
- 238000007747 plating Methods 0.000 abstract 1
- 229920000233 poly(alkylene oxides) Polymers 0.000 abstract 1
- 229920000223 polyglycerol Polymers 0.000 abstract 1
- 229920000151 polyglycol Polymers 0.000 abstract 1
- 239000010695 polyglycol Substances 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- AWMVMTVKBNGEAK-UHFFFAOYSA-N styrene oxide Chemical class C1OC1C1=CC=CC=C1 AWMVMTVKBNGEAK-UHFFFAOYSA-N 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 125000001424 substituent group Chemical group 0.000 abstract 1
- 238000006467 substitution reaction Methods 0.000 abstract 1
- NINIDFKCEFEMDL-UHFFFAOYSA-N sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 1
- 235000015523 tannic acid Nutrition 0.000 abstract 1
- 229920002258 tannic acid Polymers 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/02—Electroplating: Baths therefor from solutions
- C25D3/34—Electroplating: Baths therefor from solutions of lead
- C25D3/36—Electroplating: Baths therefor from solutions of lead characterised by the organic bath constituents used
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
- Polyethers (AREA)
Abstract
As an addition agent in a lead plating bath there is employed a polyether of the general formula R1X[R2O)n(R3O)n1]n11R, where X is oxygen, NH or sulphur, R1 and R are hydrogen, hydroxyl, or a monovalent organic radical, R2 and R3 are bivalent hydrocarbon radicals and n, n1 and n11 are integers. The polyether preferably has a molecular weight of at least 700. It may be derived from polyethylene, propylene, butylene, cyclohexane, or styrene oxides; substitution may be by a monovalent aliphatic radical or by a monovalent isocyclic radical, e.g. a terpineol residue, a b -naphthol residue or a parahydroxydiphenyl residue. Production of polyalkylene oxides having terminal substituents may be brought about by condensing suitable compounds with the alkylene oxide using a large number of moles of the latter to each mole of the former. Substances which may be reacted with polyethylene oxide include (a) monohydric alcohols such as methyl, cetyl, phenyl ethyl and octadecenyl alcohols, (b) polyhydric alcohols such as ethylene glycol, sorbitol and penta-erythritol, (c) aldehydes such as acetaldehyde, myristic aldehyde, benzaldehyde, phenyl acetaldehyde, (d) monocarboxylic acids such as acetic, stearic, benzoic and undecylenic acids, (e) polycarboxylic acids such as oxalic, maleic and phthalic acids, (f) acetals such as acetal and phenyl acetaldehyde dimethyl acetal, (g) phenols such as phenol, catechol, naphthol and cresol, (h) amines such as ethylamine and aniline, (i) amides such as formamide, benzamide and stearic amide, (j) ketones such as acetone, methyl ethyl ketone or acetophenone, (k) unsaturated compounds having an ethylenic or acetylenic linkage. The following are examples of preparations: (i) one-twelfth mol. of terpineol is reacted with one mol. of ethylene oxide, (ii) parahydroxydiphenyl is reacted with 12 molecular equivalents of ethylene oxide, (iii) equimolecular amounts of phenol and ethylene oxide are reacted, (iv) equimolecular amounts of glycerol and ethylene oxide are reacted. The following are also referred to: glycol and polyglycol ethers of isocyclichydroxyl compounds; monocarboxylic acid esters of polyglycerol and its analogues; a compound prepared by introducing an alkylene oxide into a tannic acid solution at 0-10 DEG C. Specifications 317,770, [Class 2 (iii)], 346,550, 380,431, 406,443, 420,518, 432,356, 434,424, 465,048, 488,907 and 505,016 are referred to.
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB595148A true GB595148A (en) | 1947-11-27 |
Family
ID=1627682
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB343945A Expired GB595148A (en) | 1945-02-12 | Improvements in or relating to the electrodeposition of lead |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB595148A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE959242C (en) * | 1952-06-03 | 1957-02-28 | Gen Motors Corp | Bath for the galvanic deposition of antimony or antimony alloys |
| US2842461A (en) * | 1955-12-02 | 1958-07-08 | Hauserman Co E F | Lead coating process and material |
-
1945
- 1945-02-12 GB GB343945A patent/GB595148A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE959242C (en) * | 1952-06-03 | 1957-02-28 | Gen Motors Corp | Bath for the galvanic deposition of antimony or antimony alloys |
| US2842461A (en) * | 1955-12-02 | 1958-07-08 | Hauserman Co E F | Lead coating process and material |
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