GB490567A - Process for increasing the wetting-out and penetrating action of strong alkaline solutions - Google Patents
Process for increasing the wetting-out and penetrating action of strong alkaline solutionsInfo
- Publication number
- GB490567A GB490567A GB15437/37A GB1543737A GB490567A GB 490567 A GB490567 A GB 490567A GB 15437/37 A GB15437/37 A GB 15437/37A GB 1543737 A GB1543737 A GB 1543737A GB 490567 A GB490567 A GB 490567A
- Authority
- GB
- United Kingdom
- Prior art keywords
- dihydroxypropyl
- wetting
- aliphatic
- alcohols
- lyes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 230000000149 penetrating effect Effects 0.000 title abstract 3
- 239000012670 alkaline solution Substances 0.000 title 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 9
- -1 hydroxyethyl groups Chemical group 0.000 abstract 6
- 239000003513 alkali Substances 0.000 abstract 5
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerol Natural products OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 4
- 239000002253 acid Substances 0.000 abstract 4
- 150000007513 acids Chemical class 0.000 abstract 4
- 125000001931 aliphatic group Chemical group 0.000 abstract 4
- 235000011121 sodium hydroxide Nutrition 0.000 abstract 4
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 abstract 3
- CTKINSOISVBQLD-UHFFFAOYSA-N Glycidol Chemical compound OCC1CO1 CTKINSOISVBQLD-UHFFFAOYSA-N 0.000 abstract 3
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical class ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 abstract 3
- 150000003868 ammonium compounds Chemical class 0.000 abstract 3
- 125000004432 carbon atom Chemical group C* 0.000 abstract 3
- 238000009736 wetting Methods 0.000 abstract 3
- KYUXDQVFKCEYRU-UHFFFAOYSA-N 2-(3-methylbutylamino)ethane-1,1-diol Chemical compound OC(CNCCC(C)C)O KYUXDQVFKCEYRU-UHFFFAOYSA-N 0.000 abstract 2
- FQDRKZIUGTXTHV-UHFFFAOYSA-N 3-[3,3-dihydroxypropyl(3-methylbutyl)amino]propane-1,1-diol Chemical compound OC(CCN(CCC(C)C)CCC(O)O)O FQDRKZIUGTXTHV-UHFFFAOYSA-N 0.000 abstract 2
- PAYRUJLWNCNPSJ-UHFFFAOYSA-N Aniline Chemical compound NC1=CC=CC=C1 PAYRUJLWNCNPSJ-UHFFFAOYSA-N 0.000 abstract 2
- 239000004215 Carbon black (E152) Substances 0.000 abstract 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical class CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 abstract 2
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical class OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 2
- 150000001412 amines Chemical class 0.000 abstract 2
- 239000007795 chemical reaction product Substances 0.000 abstract 2
- JQVDAXLFBXTEQA-UHFFFAOYSA-N dibutylamine Chemical compound CCCCNCCCC JQVDAXLFBXTEQA-UHFFFAOYSA-N 0.000 abstract 2
- 235000011187 glycerol Nutrition 0.000 abstract 2
- 229930195733 hydrocarbon Natural products 0.000 abstract 2
- 150000002430 hydrocarbons Chemical group 0.000 abstract 2
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 abstract 2
- JIAARYAFYJHUJI-UHFFFAOYSA-L zinc dichloride Chemical compound [Cl-].[Cl-].[Zn+2] JIAARYAFYJHUJI-UHFFFAOYSA-L 0.000 abstract 2
- SAUITLHMZXFAAL-UHFFFAOYSA-N 1-(ethylamino)butane-1,1-diol Chemical compound OC(CCC)(NCC)O SAUITLHMZXFAAL-UHFFFAOYSA-N 0.000 abstract 1
- CZZZABOKJQXEBO-UHFFFAOYSA-N 2,4-dimethylaniline Chemical group CC1=CC=C(N)C(C)=C1 CZZZABOKJQXEBO-UHFFFAOYSA-N 0.000 abstract 1
- MNCTZQWOTVEPJP-UHFFFAOYSA-N 2-(3-butoxypropylamino)ethane-1,1-diol Chemical compound OC(CNCCCOCCCC)O MNCTZQWOTVEPJP-UHFFFAOYSA-N 0.000 abstract 1
- SOCHNULDZXESJP-UHFFFAOYSA-N 2-[2-hydroxyethyl(4-methylpentyl)amino]ethanol Chemical compound CC(C)CCCN(CCO)CCO SOCHNULDZXESJP-UHFFFAOYSA-N 0.000 abstract 1
- VKGUUNHFDKMHDI-UHFFFAOYSA-N 2-hydroxyhexane-2-sulfonic acid Chemical compound C(CCC)C(C)(S(=O)(=O)O)O VKGUUNHFDKMHDI-UHFFFAOYSA-N 0.000 abstract 1
- NAEBNUZNSRQDHP-UHFFFAOYSA-N 3-(2-methylpropylamino)propane-1,1-diol Chemical compound OC(CCNCC(C)C)O NAEBNUZNSRQDHP-UHFFFAOYSA-N 0.000 abstract 1
- XGEGPDLCMNOIQM-UHFFFAOYSA-N 3-(4-methylpentylamino)propane-1,1-diol Chemical compound OC(CCNCCCC(C)C)O XGEGPDLCMNOIQM-UHFFFAOYSA-N 0.000 abstract 1
- PMJRBXVYQSSURK-UHFFFAOYSA-N 3-(diethylamino)propane-1,1-diol Chemical compound CCN(CC)CCC(O)O PMJRBXVYQSSURK-UHFFFAOYSA-N 0.000 abstract 1
- WRYWZDADPAUKLG-UHFFFAOYSA-N 3-(dipropylamino)propane-1,1-diol Chemical compound CCCN(CCC)CCC(O)O WRYWZDADPAUKLG-UHFFFAOYSA-N 0.000 abstract 1
- LAZPSNVCCYJLDR-UHFFFAOYSA-N 3-(heptylamino)propane-1,1-diol Chemical compound OC(CCNCCCCCCC)O LAZPSNVCCYJLDR-UHFFFAOYSA-N 0.000 abstract 1
- WBBOAOROAVRLDZ-UHFFFAOYSA-N 3-[3,3-dihydroxypropyl(hexyl)amino]propane-1,1-diol Chemical compound OC(CCN(CCCCCC)CCC(O)O)O WBBOAOROAVRLDZ-UHFFFAOYSA-N 0.000 abstract 1
- QKNRWCPOWHRQTB-UHFFFAOYSA-N 3-[bis(3-methylbutyl)amino]propane-1,1-diol Chemical compound OC(CCN(CCC(C)C)CCC(C)C)O QKNRWCPOWHRQTB-UHFFFAOYSA-N 0.000 abstract 1
- UMGNTWFXJCNESZ-UHFFFAOYSA-N 3-[butyl(3,3-dihydroxypropyl)amino]propane-1,1-diol Chemical compound CCCCN(CCC(O)O)CCC(O)O UMGNTWFXJCNESZ-UHFFFAOYSA-N 0.000 abstract 1
- PWYNLGLQEVEAAG-UHFFFAOYSA-N 3-[cyclohexyl(3,3-dihydroxypropyl)amino]propane-1,1-diol Chemical compound C1(CCCCC1)N(CCC(O)O)CCC(O)O PWYNLGLQEVEAAG-UHFFFAOYSA-N 0.000 abstract 1
- HYZYOKHLDUXUQK-UHFFFAOYSA-N 3-methylbutane-1-sulfonic acid Chemical compound CC(C)CCS(O)(=O)=O HYZYOKHLDUXUQK-UHFFFAOYSA-N 0.000 abstract 1
- OOVZHGAEBVZNPN-UHFFFAOYSA-N 5-aminooctane-1,1-diol Chemical compound OC(CCCC(CCC)N)O OOVZHGAEBVZNPN-UHFFFAOYSA-N 0.000 abstract 1
- GAWIXWVDTYZWAW-UHFFFAOYSA-N C[CH]O Chemical group C[CH]O GAWIXWVDTYZWAW-UHFFFAOYSA-N 0.000 abstract 1
- 229920000742 Cotton Polymers 0.000 abstract 1
- PAFZNILMFXTMIY-UHFFFAOYSA-N Cyclohexylamine Natural products NC1CCCCC1 PAFZNILMFXTMIY-UHFFFAOYSA-N 0.000 abstract 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 1
- 229920000297 Rayon Polymers 0.000 abstract 1
- 239000004115 Sodium Silicate Substances 0.000 abstract 1
- OAGVAYDQAOXEPY-UHFFFAOYSA-M [Cl-].OC(CC[N+](CCC(C)C)(CCC(C)C)CCC(O)O)O Chemical compound [Cl-].OC(CC[N+](CCC(C)C)(CCC(C)C)CCC(O)O)O OAGVAYDQAOXEPY-UHFFFAOYSA-M 0.000 abstract 1
- 150000001241 acetals Chemical class 0.000 abstract 1
- 150000001298 alcohols Chemical class 0.000 abstract 1
- 150000001299 aldehydes Chemical class 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 229920002678 cellulose Polymers 0.000 abstract 1
- 239000001913 cellulose Substances 0.000 abstract 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 abstract 1
- 229940028356 diethylene glycol monobutyl ether Drugs 0.000 abstract 1
- 239000002270 dispersing agent Substances 0.000 abstract 1
- 150000002170 ethers Chemical class 0.000 abstract 1
- 229930182478 glucoside Chemical class 0.000 abstract 1
- 150000008131 glucosides Chemical class 0.000 abstract 1
- 150000002334 glycols Chemical class 0.000 abstract 1
- 125000000623 heterocyclic group Chemical group 0.000 abstract 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 1
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 abstract 1
- 150000002576 ketones Chemical class 0.000 abstract 1
- WGYKZJWCGVVSQN-UHFFFAOYSA-N mono-n-propyl amine Natural products CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 abstract 1
- 239000003921 oil Substances 0.000 abstract 1
- JCGNDDUYTRNOFT-UHFFFAOYSA-N oxolane-2,4-dione Chemical compound O=C1COC(=O)C1 JCGNDDUYTRNOFT-UHFFFAOYSA-N 0.000 abstract 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 abstract 1
- 229920000151 polyglycol Polymers 0.000 abstract 1
- 239000010695 polyglycol Substances 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 abstract 1
- 229910052911 sodium silicate Inorganic materials 0.000 abstract 1
- 235000010265 sodium sulphite Nutrition 0.000 abstract 1
- 235000000346 sugar Nutrition 0.000 abstract 1
- 150000005846 sugar alcohols Polymers 0.000 abstract 1
- 150000008163 sugars Chemical class 0.000 abstract 1
- NVBFHJWHLNUMCV-UHFFFAOYSA-N sulfamide Chemical class NS(N)(=O)=O NVBFHJWHLNUMCV-UHFFFAOYSA-N 0.000 abstract 1
- 239000011592 zinc chloride Substances 0.000 abstract 1
- 235000005074 zinc chloride Nutrition 0.000 abstract 1
Classifications
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/372—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen containing etherified or esterified hydroxy groups ; Polyethers of low molecular weight
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/38—Oxides or hydroxides of elements of Groups 1 or 11 of the Periodic Table
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/322—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing nitrogen
- D06M13/368—Hydroxyalkylamines; Derivatives thereof, e.g. Kritchevsky bases
Landscapes
- Engineering & Computer Science (AREA)
- Textile Engineering (AREA)
- Detergent Compositions (AREA)
- Cosmetics (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
Abstract
The wetting-out and penetrating properties of strong alkali lyes are improved by adding such amines or ammonium compounds as contain at least one terminal hydrocarbon radicle with at least three carbon atoms or several hydrocarbon radicles with at least two carbon atoms each and one or several aliphatic hydroxy groups, but no chains with more than five ethanoxy groups. The use of amines having a polyglycerine radicle or one or two hydroxyethyl groups and at the same time a benzene residue or a cyclohexane residue and also saturated heterocyclic amines having a mono or polyhydroxyalkyl group is excluded. The wetting &c. property can be further improved when necessary, e.g. with lyes of insufficient concentration of alkali by the addition of ether-alcohols of the aliphatic, cycloaliphatic, araliphatic and heterocyclic series. Ethers of glycols and other polyhydric alcohols, and acetals of ketones and aldehydes are suitable. When alkali lyes of such strength are used that they tend to precipitate the hydroxyamines or ammonium compounds, the following dispersing agents may be added: highly sulphonated oils, benzene mono and polysulphonic acids and their sulphamides, the homologues of phenol, mono and poly sulphonic acids, aliphatic sulphonic acids, e.g. isopentanesulphonic acid, butylhydroxyethanesulphonic acid and sulphonic acids obtained by reacting sulphuric acid esters of glycol, polyglycol and glycerol ethers with sodium sulphite, sulphuric acid esters of aliphatic and cyclic alcohols, aliphatic monocarboxylic acids with 3-12 carbon atoms and glucoside derivatives of sugars, alcohols or ether - alcohols. In examples, the following hydroxyamines and ammonium compounds are added to alkali lyes: dihydroxyethylisoamylamine, di-(dihydroxypropyl) - isoamylamine, dihydroxy-ethyl - n - butylamine, monodihydroxypropyl-monoisoamylamine, b : g - dihydroxypropyl-mono and di-n-butylamine, dihydroxypropyl-diisoamylamine, hydroxyethyl(di - b - propylamine, di(dihydroxypropyl) - n - hexylamine, dihydroxypropylnaphtheneamine, di(dihydroxypropyl)naphtheneamine, triisoamyldihydroxypropylammoniumchloride, dihydroxypropyl-2-aminopentane, di(dihydroxypropyl)-n-butylamine, di(hydroxyethyl)isohexylamine, dihydroxypropylisohexylamine, dihydroxypropyl-n-heptylamine, dihydroxypropyldiethylamine, N - dihydroxyethylaminopropyl - n - butylether, diisoamyldi (dihydroxypropyl) ammoniumchloride, dihydroxyethylisoamylamine, N-di-(dihydroxypropyl)aniline, cyclohexyldi(di-hydroxypropyl)amine, a - isoamylhydroxy - b -hydroxy - g - aminopropane, dihydroxypropyl-dipropylamine, the reaction product of glycide with asym-diethylenediamine and the reaction product of 1 mol. metaxylidine with 2 mols. glycide. Glycerinemonoamylether, isoamylglucoside and diethyleneglycolmonobutylether are used in examples to increase the wetting properties of hydroxyamines. In another example, dihydroxypropylisobutylamine is added to lyes containing (a) sodium chloride to increase the density of the lye; (b) sodium silicate to reduce the shrinkage of the cotton; (c) glycerine to increase the viscosity of the lye; and (d) zinc chloride. In each case the wetting and penetrating effect is improved. A caustic soda lye containing monodihydroxypropylmonoisoamylamine may be used for the lanification of tissues and for the preparation of alkali cellulose for the viscose industry. Specifications 27020/97, [Class 42], 210,484, 323,307, [both in Class 42 (i)], 372,325, and 459,309 are referred to. Di (dihydroxypropyl)isoamylamine and di-(dihydroxypropyl) cyclohexyl amine are prepared by reacting 1 mol. of the appropriate base with 2 mols. of glycide. Reference has been directed by the Comptroller to Specification 480,837.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH490567X | 1936-06-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB490567A true GB490567A (en) | 1938-08-17 |
Family
ID=4516593
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB15437/37A Expired GB490567A (en) | 1936-06-04 | 1937-06-03 | Process for increasing the wetting-out and penetrating action of strong alkaline solutions |
Country Status (4)
| Country | Link |
|---|---|
| CH (1) | CH194167A (en) |
| DE (1) | DE719432C (en) |
| FR (1) | FR822637A (en) |
| GB (1) | GB490567A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4568349A (en) * | 1981-08-22 | 1986-02-04 | Sandoz Ltd. | Alkali treatment of cellulosic fiber goods |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP3718988A1 (en) * | 2019-04-03 | 2020-10-07 | Yara International ASA | Corrosion inhibition of metal reinforcement present in a hardened concrete construction having one or more surfaces that are exposed to chloride intrusion |
-
1936
- 1936-06-04 CH CH194167D patent/CH194167A/en unknown
-
1937
- 1937-06-02 DE DEC52874D patent/DE719432C/en not_active Expired
- 1937-06-03 FR FR822637D patent/FR822637A/en not_active Expired
- 1937-06-03 GB GB15437/37A patent/GB490567A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4568349A (en) * | 1981-08-22 | 1986-02-04 | Sandoz Ltd. | Alkali treatment of cellulosic fiber goods |
Also Published As
| Publication number | Publication date |
|---|---|
| DE719432C (en) | 1942-04-16 |
| FR822637A (en) | 1938-01-05 |
| CH194167A (en) | 1937-11-30 |
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