GB1234742A - Process for the production of palladium acetyl acetone - Google Patents

Process for the production of palladium acetyl acetone

Info

Publication number
GB1234742A
GB1234742A GB178470A GB178470A GB1234742A GB 1234742 A GB1234742 A GB 1234742A GB 178470 A GB178470 A GB 178470A GB 178470 A GB178470 A GB 178470A GB 1234742 A GB1234742 A GB 1234742A
Authority
GB
United Kingdom
Prior art keywords
palladium
acetyl acetonate
palladium acetyl
waterinsoluble
jan
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB178470A
Inventor
Wolfgang Swodenk
Gerhard Scharfe
Wolfram Dornfeldt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Bayer AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Publication of GB1234742A publication Critical patent/GB1234742A/en
Expired legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
    • C07F15/00—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic System
    • C07F15/0006—Compounds containing elements of Groups 8, 9, 10 or 18 of the Periodic System compounds of the platinum group
    • C07F15/006—Palladium compounds
    • C07F15/0066—Palladium compounds without a metal-carbon linkage

Abstract

1,234,742. Palladium acetyl acetonate. FARBENFABRIKEN BAYER A.G. 14 Jan., 1970 [29 Jan., 1969], No. 1784/70. Heading C2C. Palladium acetyl acetonate having a low organically bound chlorine content (i.e. less than 0.05% by weight) is prepared by adding an aqueous alkali metal hydroxide solution to an aqueous alkali metal palladium chloride solution in a quantity sufficient to make the latter waterinsoluble; adding acetylacetone thereto in a quantity sufficient to convert the waterinsoluble palladium compound into palladium acetyl acetonate and agitating the resulting mixture until a deposit is formed which after washing and drying is at least 99% soluble in benzene. The reaction is preferably carried out at a temperature of from 10‹ to 40‹ C.
GB178470A 1969-01-29 1970-01-14 Process for the production of palladium acetyl acetone Expired GB1234742A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19691904235 DE1904235C3 (en) 1969-01-29 1969-01-29 Process for the production of palladium acetylacetonate

Publications (1)

Publication Number Publication Date
GB1234742A true GB1234742A (en) 1971-06-09

Family

ID=5723633

Family Applications (1)

Application Number Title Priority Date Filing Date
GB178470A Expired GB1234742A (en) 1969-01-29 1970-01-14 Process for the production of palladium acetyl acetone

Country Status (6)

Country Link
JP (1) JPS4945849B1 (en)
BE (1) BE745159A (en)
DE (1) DE1904235C3 (en)
FR (1) FR2029649A1 (en)
GB (1) GB1234742A (en)
NL (1) NL7000988A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100439381C (en) * 2005-07-18 2008-12-03 昆明贵金属研究所 Di(acetylacetone)palladium(II)synthesis method
RU2495880C1 (en) * 2012-07-03 2013-10-20 Федеральное государственное бюджетное учреждение науки Институт неорганической химии им. А.В. Николаева Сибирского отделения Российской академии наук (ИНХ СО РАН) Method of producing acetylacetonates of platinum group metals
RU2641893C1 (en) * 2016-12-05 2018-01-23 Общество с ограниченной ответственностью "Мембраны-НЦ" (ООО "Мембраны-НЦ") Method of producing beta-diketonate of palladium (ii)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP4976706B2 (en) * 2006-02-21 2012-07-18 北興化学工業株式会社 Method for producing palladium acetylacetonate

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100439381C (en) * 2005-07-18 2008-12-03 昆明贵金属研究所 Di(acetylacetone)palladium(II)synthesis method
RU2495880C1 (en) * 2012-07-03 2013-10-20 Федеральное государственное бюджетное учреждение науки Институт неорганической химии им. А.В. Николаева Сибирского отделения Российской академии наук (ИНХ СО РАН) Method of producing acetylacetonates of platinum group metals
RU2641893C1 (en) * 2016-12-05 2018-01-23 Общество с ограниченной ответственностью "Мембраны-НЦ" (ООО "Мембраны-НЦ") Method of producing beta-diketonate of palladium (ii)

Also Published As

Publication number Publication date
DE1904235C3 (en) 1973-09-27
NL7000988A (en) 1970-07-31
BE745159A (en) 1970-07-29
JPS4945849B1 (en) 1974-12-06
DE1904235A1 (en) 1970-08-06
FR2029649A1 (en) 1970-10-23
DE1904235B2 (en) 1973-02-22

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