GB1152983A - Perfluoro Carboxylic Acid Fluorides and their preparation - Google Patents
Perfluoro Carboxylic Acid Fluorides and their preparationInfo
- Publication number
- GB1152983A GB1152983A GB19585/66A GB1958566A GB1152983A GB 1152983 A GB1152983 A GB 1152983A GB 19585/66 A GB19585/66 A GB 19585/66A GB 1958566 A GB1958566 A GB 1958566A GB 1152983 A GB1152983 A GB 1152983A
- Authority
- GB
- United Kingdom
- Prior art keywords
- acid
- tertiary amino
- hcl
- amino group
- carboxylic acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25B—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES FOR THE PRODUCTION OF COMPOUNDS OR NON-METALS; APPARATUS THEREFOR
- C25B3/00—Electrolytic production of organic compounds
- C25B3/20—Processes
- C25B3/27—Halogenation
- C25B3/28—Fluorination
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S516/00—Colloid systems and wetting agents; subcombinations thereof; processes of
- Y10S516/01—Wetting, emulsifying, dispersing, or stabilizing agents
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Electrochemistry (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1,152,983. Perfluoro-aminocarboxylic acids and derivatives thereof. MINNESOTA MINING & MFG. CO. 3 May, 1966 [3 May, 1965], No. 19585/66. Heading C2C. [Also in Division C7] The invention comprises perfluorocarboxylic acid fluorides substituted by a tertiary amino group and having only a perfluoroalkylene group between the acid fluoride radical and the nitrogen atom of the tertiary amino group. The compounds are prepared by electrofluorination of a tertiary amino-substituted carboxylic acid halide having only an alkylene group between the acid halide radical and the nitrogen atom of the tertiary amino group. The acid fluorides may be converted to the corresponding acids, salts and esters by conventional methods. Ethyliminodipropionyl chloride hydrochloride is prepared by reacting ethylamine with ethyl acrylate to give diethyl ethyliminodipropionate, C 2 H 5 N(CH 2 CH 2 COOC 2 H 5 ) 2 , which is then hydrolysed with HCl to give ethyliminodipropionic acid hydrochloride, C 2 H 5 N(CH 2 CH 2 COOH) 2 .HCl, which is converted by reaction with PCl 5 to the desired acid chloride, C 2 H 5 N(CH 2 CH 2 COCl) 2 .HCl.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US45284565A | 1965-05-03 | 1965-05-03 |
Publications (1)
Publication Number | Publication Date |
---|---|
GB1152983A true GB1152983A (en) | 1969-05-21 |
Family
ID=23798183
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
GB19585/66A Expired GB1152983A (en) | 1965-05-03 | 1966-05-03 | Perfluoro Carboxylic Acid Fluorides and their preparation |
Country Status (3)
Country | Link |
---|---|
US (1) | US3471484A (en) |
DE (1) | DE1595998C3 (en) |
GB (1) | GB1152983A (en) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
USRE29255E (en) * | 1968-10-16 | 1977-06-07 | E. I. Du Pont De Nemours And Company | Photographic layers containing perfluoro compounds and coating thereof |
US4985556A (en) * | 1987-09-10 | 1991-01-15 | Agency Of Industrial Science & Technology | Perfluoro(dialkylaminopropene) derivatives |
JP6461573B2 (en) | 2014-07-30 | 2019-01-30 | 三菱マテリアル株式会社 | Oil / water separator / collector |
WO2016017686A1 (en) | 2014-07-30 | 2016-02-04 | 三菱マテリアル株式会社 | Hydrophilic oil repellent agent and method for manufacturing same, and surface covering material, coating film, resin composition, oil-water separation filter medium, and porous body |
WO2016017761A1 (en) | 2014-07-30 | 2016-02-04 | 三菱マテリアル株式会社 | Surface-coating material, coated film, and hydrophilic/oil-repellent material |
JP5879013B1 (en) | 2014-07-30 | 2016-03-08 | 三菱マテリアル株式会社 | Filter medium, filter medium manufacturing method, water treatment module and water treatment apparatus |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2500388A (en) * | 1948-07-21 | 1950-03-14 | Minnesota Mining & Mfg | Fluorocarbon ethers |
US2519983A (en) * | 1948-11-29 | 1950-08-22 | Minnesota Mining & Mfg | Electrochemical process of making fluorine-containing carbon compounds |
US2567011A (en) * | 1949-01-10 | 1951-09-04 | Minnesota Mining & Mfg | Fluorocarbon acids and derivatives |
US2616927A (en) * | 1950-05-12 | 1952-11-04 | Minnesota Mining & Mfg | Fluorocarbon tertiary amines |
GB763673A (en) * | 1953-12-21 | 1956-12-12 | Minnesota Mining & Mfg | Improvements in and relating to fluorocarbon acids and derivatives |
US2950317A (en) * | 1957-10-21 | 1960-08-23 | Minnesota Mining & Mfg | Process for preparation of perfluoroalkyl sulfonyl chlorides |
-
1965
- 1965-05-03 US US452845A patent/US3471484A/en not_active Expired - Lifetime
-
1966
- 1966-05-02 DE DE1595998A patent/DE1595998C3/en not_active Expired
- 1966-05-03 GB GB19585/66A patent/GB1152983A/en not_active Expired
Also Published As
Publication number | Publication date |
---|---|
DE1595998B2 (en) | 1980-03-20 |
DE1595998A1 (en) | 1970-03-19 |
US3471484A (en) | 1969-10-07 |
DE1595998C3 (en) | 1980-11-20 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
PS | Patent sealed [section 19, patents act 1949] | ||
PE | Patent expired |