GB1033009A - Process for manufacturing flexible carbonaceous textile material - Google Patents

Process for manufacturing flexible carbonaceous textile material

Info

Publication number
GB1033009A
GB1033009A GB36100/63A GB3610063A GB1033009A GB 1033009 A GB1033009 A GB 1033009A GB 36100/63 A GB36100/63 A GB 36100/63A GB 3610063 A GB3610063 A GB 3610063A GB 1033009 A GB1033009 A GB 1033009A
Authority
GB
United Kingdom
Prior art keywords
starting material
cellulosic
acid
solution
textile
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB36100/63A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Union Carbide Corp
Original Assignee
Union Carbide Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Union Carbide Corp filed Critical Union Carbide Corp
Publication of GB1033009A publication Critical patent/GB1033009A/en
Expired legal-status Critical Current

Links

Classifications

    • D—TEXTILES; PAPER
    • D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
    • D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
    • D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
    • D01F9/12—Carbon filaments; Apparatus specially adapted for the manufacture thereof
    • D01F9/14—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments
    • D01F9/16—Carbon filaments; Apparatus specially adapted for the manufacture thereof by decomposition of organic filaments from products of vegetable origin or derivatives thereof, e.g. from cellulose acetate
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
    • Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y10S264/00—Plastic and nonmetallic article shaping or treating: processes
    • Y10S264/19—Inorganic fiber

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Carbon And Carbon Compounds (AREA)
  • Chemical Or Physical Treatment Of Fibers (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Inorganic Fibers (AREA)

Abstract

Carbon or graphite materials possessing textile characteristics are prepared by subjecting to carbonization and/or graphitization temperatures a permanently dehydrated heat-treated material which retains the characteristic physical attributes of the cellulosic starting material, and which is prepared by subjecting natural or regenerated cellulosic textile material in an oxidizing atmosphere to a temperature of 100-350 DEG C. for a time sufficient to cause the starting material to realize a weight loss based on the starting material of 20 to 50% and to have a volatile content of from 45 to 70%. The textile starting material, e.g. cotton, linen, jute or rayon, may be impregnated with an up to 50% by volume acid solution and then dried in air at room temperature prior to being heated. The acid constituent of the solution may be phosphoric, sulphuric, hydrochloric or nitric acid, diammonium phosphate or diethylchloro phosphate and the solvent may be water, alcohol or ketone. The cellulosic material may be in the form of fibres, filaments, yarns and battings or cloth and impregnated with a solution of acid initial decomposition of the cellulose molecule involving rupture of the C-O and C-H bonds with the evolution of H2O and ends at a point just prior to the scission of the main cellulosic molecule, the rupture of C-C bonds, and the evolution of hydrogen.ALSO:A permanently dehydrated heat-treated material retaining the characteristic physical attributes of the cellulosic starting material is prepared by subjecting natural or regenerated cellulosic textile material in an oxidizing atmosphere to a temperature of 100-350 DEG C. for a time sufficient to cause the starting material to realize a weight loss based on the starting material of 20 to 50% and to have a volatile content of 45 to 70%. The material produced may subsequently be subjected to carbonization and/or graphitization temperature (see Division C1). The textile starting material, e.g. cotton, linen, jute or rayon may be impregnated with an up to 50% by volume acid solution and then dried in air at room temperature prior to heating. The acid constituent of the solution may be phosphoric, sulphuric, hydrochloric or nitric acid, diammonium phosphate or diethylchloro phosphate and the solvent may be water, alcohol or ketone. The cellulosic material may be in the form of fibres, filaments, yarns and battings or cloth and impregnated with a solution of acid concentration 3 or 7% by volume respectively. The heat treatment commences with the concentration 3 or 7% by volume respectively.
GB36100/63A 1962-09-20 1963-09-13 Process for manufacturing flexible carbonaceous textile material Expired GB1033009A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US224989A US3305315A (en) 1962-09-20 1962-09-20 Process for manufacturing flexible carbonaceous textile material

Publications (1)

Publication Number Publication Date
GB1033009A true GB1033009A (en) 1966-06-15

Family

ID=22843081

Family Applications (1)

Application Number Title Priority Date Filing Date
GB36100/63A Expired GB1033009A (en) 1962-09-20 1963-09-13 Process for manufacturing flexible carbonaceous textile material

Country Status (3)

Country Link
US (1) US3305315A (en)
DE (1) DE1242551B (en)
GB (1) GB1033009A (en)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3479150A (en) * 1965-07-14 1969-11-18 Hitco Carbonization method for cellulosic fibers
US3441378A (en) * 1966-05-10 1969-04-29 Union Carbide Corp Process for the manufacture of carbon textiles
DE1671274A1 (en) * 1967-07-26 1972-02-10 Wacker Chemie Gmbh Process for the production of carbon fibers
US3508874A (en) * 1968-01-12 1970-04-28 Celanese Corp Production of carbon yarns
GB1256072A (en) * 1968-02-02 1971-12-08 Morganite Res & Dev Ltd Improvements in or relating to the manufacture of filamentary carbon materials
US3639140A (en) * 1968-10-12 1972-02-01 Nitto Boseki Co Ltd Process for carbonized cellulose fiber or the products thereof
US3661616A (en) * 1968-11-06 1972-05-09 Notto Boseki Co Ltd Process for carbonizing cellulose fiber or the products thereof
US3649196A (en) * 1968-12-18 1972-03-14 Allied Chem Preparation of carbon paper
US3661503A (en) * 1969-05-29 1972-05-09 Union Carbide Corp Process for dehydrating cellulosic textile material
US3539296A (en) * 1969-06-16 1970-11-10 Kimberly Clark Co Method of making carbonized cellulose fibers for incorporation in electrically conductive paper
US3652221A (en) * 1969-07-30 1972-03-28 Union Carbide Corp Process for producing carbon fibers
US3716331A (en) * 1970-04-10 1973-02-13 Union Carbide Corp Process for producing carbon fibers having a high young's modulus of elasticity
US3716332A (en) * 1970-07-27 1973-02-13 Ducommun Inc Carbonization of wool
US3954947A (en) * 1972-11-17 1976-05-04 Union Carbide Corporation Rapid stabilization of polyacrylonitrile fibers prior to carbonization
US4056272A (en) * 1974-03-01 1977-11-01 Charles Donovan Morrill Seal
US3903248A (en) * 1974-04-15 1975-09-02 Celanese Corp Process for the production of large denier carbon fibers
US4534886A (en) * 1981-01-15 1985-08-13 International Paper Company Non-woven heating element
US5102855A (en) * 1990-07-20 1992-04-07 Ucar Carbon Technology Corporation Process for producing high surface area activated carbon
JPH0624724A (en) * 1992-05-05 1994-02-01 Ucar Carbon Technol Corp Sulfur-containing activated carbon with high specific surface area
US5372619A (en) * 1992-10-14 1994-12-13 Ucar Carbon Technology Corporation Method for storing methane using a halogenating agent treated activated carbon
IL108883A (en) 1994-03-07 1998-03-10 Rotem Ind Ltd Process for the production of hollow carbon fiber membranes
US6051034A (en) * 1998-09-30 2000-04-18 Springs Industries, Inc. Methods for reducing pilling of towels
EP1622830A2 (en) * 2003-05-09 2006-02-08 McGill University Process for the production of activated carbon
JP2010501320A (en) * 2006-08-23 2010-01-21 カーボン ソリューションズ インコーポレイテッド Acid impregnated activated carbon and method for forming and using the same
TWI589741B (en) * 2012-01-23 2017-07-01 茵芬提亞公司 Method for stabilizing lignin fiber for further conversion to carbon fiber
RU2748254C1 (en) * 2020-07-17 2021-05-21 Российская Федерация в лице Государственной корпорации по атомной энергии "Росатом" Method for producing medical napkins from graphitized carbon fabric based on viscose
CN113502682B (en) * 2021-06-29 2022-10-25 华南理工大学 Cellulose-based activated carbon fiber paper and preparation method and application thereof

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1060065A (en) * 1912-09-30 1913-04-29 Int Precipitation Co Filtering medium and process for making the same.
US2488212A (en) * 1945-10-18 1949-11-15 Visking Corp Method of sealing thermoplastic material
US2739096A (en) * 1952-11-14 1956-03-20 Bayon Patrice Marie Method for the manufacture of leather belts and bracelets formed by two elongated leather strips
US3011981A (en) * 1958-04-21 1961-12-05 Soltes William Timot Electrically conducting fibrous carbon
US3053775A (en) * 1959-11-12 1962-09-11 Carbon Wool Corp Method for carbonizing fibers
US3116975A (en) * 1961-02-08 1964-01-07 Union Carbide Corp Artificial graphite process

Also Published As

Publication number Publication date
US3305315A (en) 1967-02-21
DE1242551B (en) 1967-06-22

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