FR2432014A1 - Procede d'obtention d'a,a'-dinitro-anthraquinones de haute purete - Google Patents

Procede d'obtention d'a,a'-dinitro-anthraquinones de haute purete

Info

Publication number
FR2432014A1
FR2432014A1 FR7822217A FR7822217A FR2432014A1 FR 2432014 A1 FR2432014 A1 FR 2432014A1 FR 7822217 A FR7822217 A FR 7822217A FR 7822217 A FR7822217 A FR 7822217A FR 2432014 A1 FR2432014 A1 FR 2432014A1
Authority
FR
France
Prior art keywords
anthraquinones
dinitro
alpha
high purity
obtaining high
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
FR7822217A
Other languages
English (en)
Other versions
FR2432014B1 (fr
Inventor
Maurice Vallette
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Produits Chimiques Ugine Kuhlmann
Ugine Kuhlmann SA
Original Assignee
Produits Chimiques Ugine Kuhlmann
Ugine Kuhlmann SA
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Produits Chimiques Ugine Kuhlmann, Ugine Kuhlmann SA filed Critical Produits Chimiques Ugine Kuhlmann
Priority to FR7822217A priority Critical patent/FR2432014A1/fr
Priority to FR7914683A priority patent/FR2458536A2/fr
Priority to US06/052,884 priority patent/US4307022A/en
Priority to IN509/DEL/79A priority patent/IN152549B/en
Priority to GB7925757A priority patent/GB2026488B/en
Priority to JP9432279A priority patent/JPS5520765A/ja
Priority to DE19792930366 priority patent/DE2930366A1/de
Priority to DD79214637A priority patent/DD145098A5/de
Publication of FR2432014A1 publication Critical patent/FR2432014A1/fr
Application granted granted Critical
Publication of FR2432014B1 publication Critical patent/FR2432014B1/fr
Granted legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06Preparation of nitro compounds
    • C07C201/16Separation; Purification; Stabilisation; Use of additives
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/45Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by at least one doubly—bound oxygen atom, not being part of a —CHO group
    • C07C205/46Compounds containing nitro groups bound to a carbon skeleton the carbon skeleton being further substituted by at least one doubly—bound oxygen atom, not being part of a —CHO group the carbon skeleton containing carbon atoms of quinone rings
    • C07C205/47Anthraquinones containing nitro groups

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

L'invention a pour objet un procédé d'obtention d' alpha , alpha '-dinitro-anthraquinones de haute pureté à partir de mélanges bruts issus de la dinitration de l'anthraquinone. On met en contact un tel mélange avec un ester de point d'ébullition supérieur à 120 degrés C dérive d'acide mono- ou dicarboxylique ou d'acide phosphorique, à une température comprise entre 20 et 200 degrés C, puis, après refroidissement éventuel, on sépare l'insoluble constitué essentiellement par les alpha , alpha '-dinitro-anthraquinones.
FR7822217A 1978-07-27 1978-07-27 Procede d'obtention d'a,a'-dinitro-anthraquinones de haute purete Granted FR2432014A1 (fr)

Priority Applications (8)

Application Number Priority Date Filing Date Title
FR7822217A FR2432014A1 (fr) 1978-07-27 1978-07-27 Procede d'obtention d'a,a'-dinitro-anthraquinones de haute purete
FR7914683A FR2458536A2 (fr) 1978-07-27 1979-06-08 Procede d'obtention d'a,a'-dinitro-anthraquinones de haute purete
US06/052,884 US4307022A (en) 1978-07-27 1979-06-28 Process for obtaining α,α'-dinitro anthraquinones of high purity
IN509/DEL/79A IN152549B (fr) 1978-07-27 1979-07-13
GB7925757A GB2026488B (en) 1978-07-27 1979-07-24 Process for the preparation of , '-dinitro-anthraquinones
JP9432279A JPS5520765A (en) 1978-07-27 1979-07-26 Method of obtaining highly pure alpha*alpha** dinitrooanthraquinone
DE19792930366 DE2930366A1 (de) 1978-07-27 1979-07-26 Verfahren zur gewinnung von alpha , alpha '-dinitroanthrachinonen mit hoher reinheit
DD79214637A DD145098A5 (de) 1978-07-27 1979-07-26 Verfahren zur gewinnung von alpha,alpha'-dinitroanthrachinonen mit hoher reinheit

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
FR7822217A FR2432014A1 (fr) 1978-07-27 1978-07-27 Procede d'obtention d'a,a'-dinitro-anthraquinones de haute purete

Publications (2)

Publication Number Publication Date
FR2432014A1 true FR2432014A1 (fr) 1980-02-22
FR2432014B1 FR2432014B1 (fr) 1980-12-12

Family

ID=9211238

Family Applications (1)

Application Number Title Priority Date Filing Date
FR7822217A Granted FR2432014A1 (fr) 1978-07-27 1978-07-27 Procede d'obtention d'a,a'-dinitro-anthraquinones de haute purete

Country Status (7)

Country Link
US (1) US4307022A (fr)
JP (1) JPS5520765A (fr)
DD (1) DD145098A5 (fr)
DE (1) DE2930366A1 (fr)
FR (1) FR2432014A1 (fr)
GB (1) GB2026488B (fr)
IN (1) IN152549B (fr)

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE3731809A1 (de) * 1987-09-22 1989-03-30 Basf Ag Verfahren zur herstellung von alkoxy(iso)-violanthrendionen

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2243931A1 (fr) * 1973-09-14 1975-04-11 Bayer Ag
FR2313349A1 (fr) * 1975-06-04 1976-12-31 Basf Ag Procede d'isolement de dinitroanthraquinones a teneur elevee en derives a-a'-dinitres
FR2362111A1 (fr) * 1976-08-21 1978-03-17 Bayer Ag Procede de separation de melanges de dinitroanthraquinones

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2545699A1 (de) * 1975-10-11 1977-04-21 Basf Ag Verfahren zur trennung von 1,5- und 1,8-dinitroanthrachinon

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2243931A1 (fr) * 1973-09-14 1975-04-11 Bayer Ag
FR2313349A1 (fr) * 1975-06-04 1976-12-31 Basf Ag Procede d'isolement de dinitroanthraquinones a teneur elevee en derives a-a'-dinitres
FR2362111A1 (fr) * 1976-08-21 1978-03-17 Bayer Ag Procede de separation de melanges de dinitroanthraquinones

Also Published As

Publication number Publication date
GB2026488B (en) 1982-09-29
US4307022A (en) 1981-12-22
DE2930366A1 (de) 1980-02-14
FR2432014B1 (fr) 1980-12-12
IN152549B (fr) 1984-02-11
DD145098A5 (de) 1980-11-19
JPS5520765A (en) 1980-02-14
GB2026488A (en) 1980-02-06

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