FR2420540A1 - Procede de fabrication de monoethylphosphite d'aluminium - Google Patents
Procede de fabrication de monoethylphosphite d'aluminiumInfo
- Publication number
- FR2420540A1 FR2420540A1 FR7809965A FR7809965A FR2420540A1 FR 2420540 A1 FR2420540 A1 FR 2420540A1 FR 7809965 A FR7809965 A FR 7809965A FR 7809965 A FR7809965 A FR 7809965A FR 2420540 A1 FR2420540 A1 FR 2420540A1
- Authority
- FR
- France
- Prior art keywords
- monoethylphosphite
- aluminum
- degrees
- mixture
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- -1 ALUMINUM MONOETHYLPHOSPHITE Chemical compound 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title 1
- 239000000203 mixture Substances 0.000 abstract 2
- AZDRQVAHHNSJOQ-UHFFFAOYSA-N alumane Chemical class [AlH3] AZDRQVAHHNSJOQ-UHFFFAOYSA-N 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- LXCYSACZTOKNNS-UHFFFAOYSA-N diethoxy(oxo)phosphanium Chemical compound CCO[P+](=O)OCC LXCYSACZTOKNNS-UHFFFAOYSA-N 0.000 abstract 1
- ZUNGGJHBMLMRFJ-UHFFFAOYSA-O ethoxy-hydroxy-oxophosphanium Chemical compound CCO[P+](O)=O ZUNGGJHBMLMRFJ-UHFFFAOYSA-O 0.000 abstract 1
- 230000000855 fungicidal effect Effects 0.000 abstract 1
- 238000009776 industrial production Methods 0.000 abstract 1
- 150000007529 inorganic bases Chemical class 0.000 abstract 1
- 230000003472 neutralizing effect Effects 0.000 abstract 1
- OJMIONKXNSYLSR-UHFFFAOYSA-N phosphorous acid Chemical class OP(O)O OJMIONKXNSYLSR-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/06—Phosphorus compounds without P—C bonds
- C07F9/08—Esters of oxyacids of phosphorus
- C07F9/141—Esters of phosphorous acids
- C07F9/142—Esters of phosphorous acids with hydroxyalkyl compounds without further substituents on alkyl
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Procédé de fabrication en continu de monoéthylphosphite d'aluminium. Il consiste successivement à préparer un mélange de composés phosphites comprenant au moins 70 % en mole de diéthylphosphite, à saponifier et neutraliser ce mélange par une base minérale à une température de 20 à 85 degrés C, en maintenant le pH de 4,5 à 8,5, puis à faire réagir la solution aqueuse résiduelle de monoéthylphosphite alcalin, soutirée en continu de l'opération précédente, avec une quantité sensiblement stoéchiométrique d'un sel hydrosoluble d'aluminium, à une température de 70 à 95 degrés C, à un pH d'environ 3,5 à 4,5 et que l'on soutire en continu le monoéthylphosphite d'aluminium précipité Obtention industrielle de ce produit fongicide pour la protection des plantes.
Priority Applications (25)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7809965A FR2420540A1 (fr) | 1978-03-24 | 1978-03-24 | Procede de fabrication de monoethylphosphite d'aluminium |
CA000323962A CA1117967A (fr) | 1978-03-24 | 1979-03-22 | Procede industriel d'obtention de monoethyl- phosphite d'aluminium |
IL56936A IL56936A (en) | 1978-03-24 | 1979-03-22 | Process for the continuous manufacture of aluminium monoethyl-phosphite |
DD79211746A DD142535A5 (de) | 1978-03-24 | 1979-03-22 | Verfahren zur herstellung von aluminiummonoaethylphosphit |
ZA791379A ZA791379B (en) | 1978-03-24 | 1979-03-22 | Process for the manufacture of aliminium monoethy phosphite |
GB7910175A GB2017706B (en) | 1978-03-24 | 1979-03-22 | Process for the manufacture of aluminium monoethylphosphite |
YU690/79A YU41150B (en) | 1978-03-24 | 1979-03-22 | Process for producing aluminium methylphosphite |
DK120079A DK146628C (da) | 1978-03-24 | 1979-03-23 | Fremgangsmaade til fremstilling af aluminiummonoethylphosphit |
BE0/194208A BE875081A (fr) | 1978-03-24 | 1979-03-23 | Procede de fabrication de monoethylphosphite d'aluminium |
AT0218779A AT376223B (de) | 1978-03-24 | 1979-03-23 | Verfahren zur kontinuierlichen herstellung von aluminiummonoaethylphosphit |
ES478893A ES8107239A1 (es) | 1978-03-24 | 1979-03-23 | Un procedimiento de fabricacion de modo continuo de monoe- tilfosfito de aluminio. |
PT69389A PT69389A (fr) | 1978-03-24 | 1979-03-23 | Procede de preparation de monoethylphosphite d'aluminium |
CH274379A CH636624A5 (fr) | 1978-03-24 | 1979-03-23 | Procede de fabrication de monoethylphosphite d'aluminium. |
PL1979214335A PL126412B1 (en) | 1978-03-24 | 1979-03-23 | Method of obtaining aluminium monoethylphosphite |
IT21266/79A IT1114217B (it) | 1978-03-24 | 1979-03-23 | Procedimento per la fabbricazione monoetilfosfito d'alluminio |
RO7997025A RO77719A (fr) | 1978-03-24 | 1979-03-23 | Procede pour la preparation continue du monoethylphosphite d'aluminium |
DE19792911516 DE2911516A1 (de) | 1978-03-24 | 1979-03-23 | Verfahren zur herstellung von aluminiummonoaethylphosphit |
LU81073A LU81073A1 (fr) | 1978-03-24 | 1979-03-23 | Procede de fabrication de monoethylphosphite d'aluminium |
JP3417379A JPS54132526A (en) | 1978-03-24 | 1979-03-23 | Manufacture of monoethyllaluminum phosphite |
NLAANVRAGE7902320,A NL188698C (nl) | 1978-03-24 | 1979-03-23 | Werkwijze ter bereiding van aluminiummonoethylfosfiet. |
SE7902656A SE447655B (sv) | 1978-03-24 | 1979-03-23 | Forfarande for framstellning av aluminiummonoetylfosfit |
BR7901800A BR7901800A (pt) | 1978-03-24 | 1979-03-23 | Processo para preparacao de monoetilfosfito de aluminio |
SU792739698A SU971102A3 (ru) | 1978-03-24 | 1979-03-24 | Способ получени моноэтилфосфита алюмини |
US06/051,753 US4272448A (en) | 1978-03-24 | 1979-06-25 | Process for the manufacture of aluminum monoethyl phosphite |
IE636/79A IE47939B1 (en) | 1978-03-24 | 1979-08-08 | Process for the manufacture of aluminium monoethyl-phosphite |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR7809965A FR2420540A1 (fr) | 1978-03-24 | 1978-03-24 | Procede de fabrication de monoethylphosphite d'aluminium |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2420540A1 true FR2420540A1 (fr) | 1979-10-19 |
FR2420540B1 FR2420540B1 (fr) | 1980-08-29 |
Family
ID=9206658
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7809965A Granted FR2420540A1 (fr) | 1978-03-24 | 1978-03-24 | Procede de fabrication de monoethylphosphite d'aluminium |
Country Status (25)
Country | Link |
---|---|
US (1) | US4272448A (fr) |
JP (1) | JPS54132526A (fr) |
AT (1) | AT376223B (fr) |
BE (1) | BE875081A (fr) |
BR (1) | BR7901800A (fr) |
CA (1) | CA1117967A (fr) |
CH (1) | CH636624A5 (fr) |
DD (1) | DD142535A5 (fr) |
DE (1) | DE2911516A1 (fr) |
DK (1) | DK146628C (fr) |
ES (1) | ES8107239A1 (fr) |
FR (1) | FR2420540A1 (fr) |
GB (1) | GB2017706B (fr) |
IE (1) | IE47939B1 (fr) |
IL (1) | IL56936A (fr) |
IT (1) | IT1114217B (fr) |
LU (1) | LU81073A1 (fr) |
NL (1) | NL188698C (fr) |
PL (1) | PL126412B1 (fr) |
PT (1) | PT69389A (fr) |
RO (1) | RO77719A (fr) |
SE (1) | SE447655B (fr) |
SU (1) | SU971102A3 (fr) |
YU (1) | YU41150B (fr) |
ZA (1) | ZA791379B (fr) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1005265B (zh) * | 1985-04-12 | 1989-09-27 | 福建师范大学 | 新型铝体系偶联剂 |
JP2747586B2 (ja) * | 1988-01-29 | 1998-05-06 | 花王株式会社 | ジアルキルリン酸ポリアルミニウム塩の製造方法,該塩からなる油ゲル化剤及び該塩を含有する外用剤組成物 |
DE19639657C2 (de) * | 1996-09-27 | 2000-03-09 | Hoechst Ag | Verfahren zur Herstellung von Aluminium-dialkylphosphinaten |
CN101525302B (zh) * | 2009-04-30 | 2012-02-08 | 山东德浩化学有限公司 | 在乙草胺生产中联产杀菌剂三乙膦酸铝的方法 |
CN102268033A (zh) * | 2011-06-16 | 2011-12-07 | 浙江嘉华化工有限公司 | 0-乙基磷酸钠生产方法 |
CN102766157B (zh) * | 2012-09-05 | 2015-11-11 | 利民化工股份有限公司 | 一种生产三乙膦酸铝原药的方法 |
CN113121595A (zh) * | 2019-12-30 | 2021-07-16 | 江苏剑牌农化股份有限公司 | 一种α-R烷氧基对氯苄基膦酸单酯 |
Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2306211A1 (fr) * | 1975-03-29 | 1976-10-29 | Goldschmidt Ag Th | Composes metalliques de monoesters d'acide phosphoreux notamment pour preparations anti-corrosion |
Family Cites Families (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2254276B1 (fr) * | 1973-12-14 | 1977-03-04 | Philagro Sa | |
DE2456627C2 (de) * | 1973-12-14 | 1984-05-10 | PEPRO - Société pour le Développement et la Vente de Spécialités Chimiques, Lyon | Fungizide Mittel auf der Basis von Phosphonsäureestern |
GB1589670A (en) * | 1976-11-16 | 1981-05-20 | Philagro Sa | Process for the manufacture of aluminium ethylphosphite |
-
1978
- 1978-03-24 FR FR7809965A patent/FR2420540A1/fr active Granted
-
1979
- 1979-03-22 YU YU690/79A patent/YU41150B/xx unknown
- 1979-03-22 ZA ZA791379A patent/ZA791379B/xx unknown
- 1979-03-22 CA CA000323962A patent/CA1117967A/fr not_active Expired
- 1979-03-22 IL IL56936A patent/IL56936A/xx unknown
- 1979-03-22 DD DD79211746A patent/DD142535A5/de not_active IP Right Cessation
- 1979-03-22 GB GB7910175A patent/GB2017706B/en not_active Expired
- 1979-03-23 RO RO7997025A patent/RO77719A/fr unknown
- 1979-03-23 ES ES478893A patent/ES8107239A1/es not_active Expired
- 1979-03-23 CH CH274379A patent/CH636624A5/fr not_active IP Right Cessation
- 1979-03-23 AT AT0218779A patent/AT376223B/de not_active IP Right Cessation
- 1979-03-23 NL NLAANVRAGE7902320,A patent/NL188698C/xx not_active IP Right Cessation
- 1979-03-23 BE BE0/194208A patent/BE875081A/fr not_active IP Right Cessation
- 1979-03-23 DK DK120079A patent/DK146628C/da not_active IP Right Cessation
- 1979-03-23 IT IT21266/79A patent/IT1114217B/it active
- 1979-03-23 LU LU81073A patent/LU81073A1/fr unknown
- 1979-03-23 SE SE7902656A patent/SE447655B/sv not_active IP Right Cessation
- 1979-03-23 BR BR7901800A patent/BR7901800A/pt unknown
- 1979-03-23 PL PL1979214335A patent/PL126412B1/pl unknown
- 1979-03-23 JP JP3417379A patent/JPS54132526A/ja active Granted
- 1979-03-23 PT PT69389A patent/PT69389A/fr unknown
- 1979-03-23 DE DE19792911516 patent/DE2911516A1/de active Granted
- 1979-03-24 SU SU792739698A patent/SU971102A3/ru active
- 1979-06-25 US US06/051,753 patent/US4272448A/en not_active Expired - Lifetime
- 1979-08-08 IE IE636/79A patent/IE47939B1/en not_active IP Right Cessation
Patent Citations (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR2306211A1 (fr) * | 1975-03-29 | 1976-10-29 | Goldschmidt Ag Th | Composes metalliques de monoesters d'acide phosphoreux notamment pour preparations anti-corrosion |
Non-Patent Citations (1)
Title |
---|
HW1964 * |
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