FR2399449A1 - PREPARATION OF CURING UREA / FORMALDEHYDE RESIN SOLUTIONS, ESPECIALLY FOR IMPREGNING AND COATING SUPPORT AND PANEL STRIPS - Google Patents
PREPARATION OF CURING UREA / FORMALDEHYDE RESIN SOLUTIONS, ESPECIALLY FOR IMPREGNING AND COATING SUPPORT AND PANEL STRIPSInfo
- Publication number
- FR2399449A1 FR2399449A1 FR7822595A FR7822595A FR2399449A1 FR 2399449 A1 FR2399449 A1 FR 2399449A1 FR 7822595 A FR7822595 A FR 7822595A FR 7822595 A FR7822595 A FR 7822595A FR 2399449 A1 FR2399449 A1 FR 2399449A1
- Authority
- FR
- France
- Prior art keywords
- degrees
- urea
- preparation
- impregning
- mmol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B38/00—Ancillary operations in connection with laminating processes
- B32B38/08—Impregnating
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/04—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
- C08G12/043—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds with at least two compounds covered by more than one of the groups C08G12/06 - C08G12/24
- C08G12/046—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds with at least two compounds covered by more than one of the groups C08G12/06 - C08G12/24 one being urea or thiourea
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B21/00—Layered products comprising a layer of wood, e.g. wood board, veneer, wood particle board
- B32B21/04—Layered products comprising a layer of wood, e.g. wood board, veneer, wood particle board comprising wood as the main or only constituent of a layer, which is next to another layer of the same or of a different material
- B32B21/06—Layered products comprising a layer of wood, e.g. wood board, veneer, wood particle board comprising wood as the main or only constituent of a layer, which is next to another layer of the same or of a different material of paper or cardboard
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/02—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes
- C08G12/04—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
- C08G12/10—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds with acyclic compounds having the moiety X=C(—N<)2 in which X is O, S or —N
- C08G12/12—Ureas; Thioureas
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G12/00—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08G12/46—Block or graft polymers prepared by polycondensation of aldehydes or ketones on to macromolecular compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L61/00—Compositions of condensation polymers of aldehydes or ketones; Compositions of derivatives of such polymers
- C08L61/20—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen
- C08L61/22—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds
- C08L61/24—Condensation polymers of aldehydes or ketones with only compounds containing hydrogen attached to nitrogen of aldehydes with acyclic or carbocyclic compounds with urea or thiourea
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/46—Synthetic macromolecular compounds obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/47—Condensation polymers of aldehydes or ketones
- D21H17/49—Condensation polymers of aldehydes or ketones with compounds containing hydrogen bound to nitrogen
- D21H17/50—Acyclic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2260/00—Layered product comprising an impregnated, embedded, or bonded layer wherein the layer comprises an impregnation, embedding, or binder material
- B32B2260/02—Composition of the impregnated, bonded or embedded layer
- B32B2260/028—Paper layer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B32—LAYERED PRODUCTS
- B32B—LAYERED PRODUCTS, i.e. PRODUCTS BUILT-UP OF STRATA OF FLAT OR NON-FLAT, e.g. CELLULAR OR HONEYCOMB, FORM
- B32B2260/00—Layered product comprising an impregnated, embedded, or bonded layer wherein the layer comprises an impregnation, embedding, or binder material
- B32B2260/04—Impregnation, embedding, or binder material
- B32B2260/046—Synthetic resin
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Phenolic Resins Or Amino Resins (AREA)
- Paper (AREA)
Abstract
Préparation de solutions de résines urée-formaldéhyde durcissables. On fait réagir à 70-95 degrés C pendant 10-30 mn une solution aqueuse d'urée et de formaldéhyde en rapport molaire de 1:1,5 à 1:2,5 avec 0,2 à 1,0 mmol d'un acide aminosulfonique et 20 à 100 mmol d'ammoniac par mole d'urée, jusqu'à ce que la solution à 50% présente à 20 degrés C une viscosité de 55 à 65 c P; on ajoute 0,8 à 10 mmol d'un acide aminosulfonique, on maintient au moyen d'ammoniac un pH de 4,0 à 4,5 pendant 10-25 mn à 70-95 degrés C jusqu'à ce que la solution à 50 % présente à 20 degrés C une viscosité de 80 à 110 cP; on ajoute 40 à 200 mmol d'ammoniac et 0,1 à 0,3 mole d'urée et on fait réagir à 70-95 degrés C pendant 15-45 mn jusqu'à ce que la solution à 50 % présente à 20 degrés C une viscosité de 85 à 125 cP. Selon l'invention on ajoute à la première étape, à raison de 1 à 10 %, un produit de polymérisation sous forme d'émulsion ou de suspension, formé de monomères de formule :Preparation of solutions of curable urea-formaldehyde resins. An aqueous solution of urea and formaldehyde in a molar ratio of 1: 1.5 to 1: 2.5 is reacted at 70-95 degrees C for 10-30 minutes with 0.2 to 1.0 mmol of a aminosulfonic acid and 20 to 100 mmol of ammonia per mole of urea, until the 50% solution has at 20 degrees C a viscosity of 55 to 65 c P; 0.8 to 10 mmol of an aminosulfonic acid is added, a pH of 4.0 to 4.5 is maintained with ammonia for 10-25 minutes at 70-95 degrees C until the solution is 50% has a viscosity of 80 to 110 cP at 20 degrees C; 40-200 mmol of ammonia and 0.1-0.3 mole of urea are added and reacted at 70-95 degrees C for 15-45 minutes until the 50% solution is present at 20 degrees C a viscosity of 85 to 125 cP. According to the invention, a polymerization product in the form of an emulsion or a suspension, formed of monomers of formula, is added in the first step at a rate of 1 to 10%:
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE2734638A DE2734638C2 (en) | 1977-08-01 | 1977-08-01 | Process for the production of solutions of curable urea-formaldehyde resins for the impregnation and coating of carrier webs for the surface treatment of wood-based panels |
Publications (2)
Publication Number | Publication Date |
---|---|
FR2399449A1 true FR2399449A1 (en) | 1979-03-02 |
FR2399449B1 FR2399449B1 (en) | 1981-07-10 |
Family
ID=6015372
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7822595A Granted FR2399449A1 (en) | 1977-08-01 | 1978-07-31 | PREPARATION OF CURING UREA / FORMALDEHYDE RESIN SOLUTIONS, ESPECIALLY FOR IMPREGNING AND COATING SUPPORT AND PANEL STRIPS |
Country Status (9)
Country | Link |
---|---|
AU (1) | AU3845078A (en) |
BE (1) | BE869436A (en) |
DE (1) | DE2734638C2 (en) |
ES (1) | ES472102A1 (en) |
FR (1) | FR2399449A1 (en) |
GB (1) | GB2003897B (en) |
MX (1) | MX149039A (en) |
SE (1) | SE433614B (en) |
YU (1) | YU39425B (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0498301A2 (en) * | 1991-02-07 | 1992-08-12 | H.B. FULLER LICENSING & FINANCING, INC. | Process for preparing a watersoluble (form)aldehyde resin and adhesive composition containing the same |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3505766A1 (en) * | 1985-02-20 | 1986-08-21 | Cassella Ag, 6000 Frankfurt | SULPHONAMIDE DERIVATIVES, THEIR PRODUCTION AND USE |
DE102005060758B3 (en) * | 2005-12-16 | 2007-08-30 | Kronotec Ag | Substrate for inkjet printing for coating a wood-based panel |
CN109641413A (en) * | 2016-08-24 | 2019-04-16 | 沙特基础工业全球技术有限公司 | Device and method for manufacturing composite construction |
Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3769143A (en) * | 1971-09-08 | 1973-10-30 | Int Paper Co | Resin impregnated cellulosic veneer and laminated panels |
US3790529A (en) * | 1971-10-05 | 1974-02-05 | Rei Tech Inc | Process for producing cationic water soluble polymer by reacting formaldehyde,amine,a polymer of acrylamide or methacrylamide and precipitating said polymer with a water soluble salt of a polybasic acid |
FR2287459A1 (en) * | 1974-10-11 | 1976-05-07 | Goldschmidt Ag Th | PROCESS FOR PREPARING SOLUTIONS OF CURABLE UREA AND FORMALDEHYDE RESINS |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE2536978C3 (en) * | 1975-08-20 | 1979-11-22 | Th. Goldschmidt Ag, 4300 Essen | Modifiers for amino resins |
-
1977
- 1977-08-01 DE DE2734638A patent/DE2734638C2/en not_active Expired
-
1978
- 1978-07-19 YU YU1730/78A patent/YU39425B/en unknown
- 1978-07-24 SE SE7808100A patent/SE433614B/en not_active IP Right Cessation
- 1978-07-25 MX MX174290A patent/MX149039A/en unknown
- 1978-07-27 ES ES472102A patent/ES472102A1/en not_active Expired
- 1978-07-28 AU AU38450/78A patent/AU3845078A/en active Pending
- 1978-07-31 FR FR7822595A patent/FR2399449A1/en active Granted
- 1978-07-31 GB GB7831698A patent/GB2003897B/en not_active Expired
- 1978-08-01 BE BE189638A patent/BE869436A/en not_active IP Right Cessation
Patent Citations (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3769143A (en) * | 1971-09-08 | 1973-10-30 | Int Paper Co | Resin impregnated cellulosic veneer and laminated panels |
US3790529A (en) * | 1971-10-05 | 1974-02-05 | Rei Tech Inc | Process for producing cationic water soluble polymer by reacting formaldehyde,amine,a polymer of acrylamide or methacrylamide and precipitating said polymer with a water soluble salt of a polybasic acid |
FR2287459A1 (en) * | 1974-10-11 | 1976-05-07 | Goldschmidt Ag Th | PROCESS FOR PREPARING SOLUTIONS OF CURABLE UREA AND FORMALDEHYDE RESINS |
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0498301A2 (en) * | 1991-02-07 | 1992-08-12 | H.B. FULLER LICENSING & FINANCING, INC. | Process for preparing a watersoluble (form)aldehyde resin and adhesive composition containing the same |
EP0498301A3 (en) * | 1991-02-07 | 1992-11-25 | H.B. Fuller Licensing & Financing, Inc. | Process for preparing a watersoluble (form)aldehyde resin and adhesive composition containing the same |
Also Published As
Publication number | Publication date |
---|---|
MX149039A (en) | 1983-08-10 |
GB2003897A (en) | 1979-03-21 |
FR2399449B1 (en) | 1981-07-10 |
DE2734638C2 (en) | 1982-12-30 |
ES472102A1 (en) | 1979-02-16 |
DE2734638A1 (en) | 1979-02-15 |
YU173078A (en) | 1982-06-30 |
YU39425B (en) | 1984-12-31 |
SE433614B (en) | 1984-06-04 |
BE869436A (en) | 1978-12-01 |
SE7808100L (en) | 1979-02-02 |
AU3845078A (en) | 1980-01-31 |
GB2003897B (en) | 1982-01-27 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |