FR2358377A1 - PROCESS FOR PREPARING AN UNSATURED DOUBLE ALKENIC BONDED ESTER - Google Patents
PROCESS FOR PREPARING AN UNSATURED DOUBLE ALKENIC BONDED ESTERInfo
- Publication number
- FR2358377A1 FR2358377A1 FR7721283A FR7721283A FR2358377A1 FR 2358377 A1 FR2358377 A1 FR 2358377A1 FR 7721283 A FR7721283 A FR 7721283A FR 7721283 A FR7721283 A FR 7721283A FR 2358377 A1 FR2358377 A1 FR 2358377A1
- Authority
- FR
- France
- Prior art keywords
- preparing
- alkenic
- unsatured
- double
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Macromonomer-Based Addition Polymer (AREA)
- Polyesters Or Polycarbonates (AREA)
Abstract
L'invention concerne la préparation d'esters. Il s'agit d'un procédé pour préparer un ester insaturé à double liaison alcénique, en faisant réagir de l'acide acrylique et/ou de l'acide méthacrylique avec un composé hydroxy à au moins un groupement hydroxyle primaire, en présence d'un catalyseur d'estérification acide et d'un solvant organique immiscible à l'eau. En fin de la réaction d'estérification, on ajoute un composé de lithium au mélange d'estérification et on soumet le mélange à une distillation. Les esters insaturés obtenus peuvent être utilisés pour la préparation de liants durcissables au rayonnement pour encres d'imprimerie, laques, colles et caoutchoucs et dans les industries papetière et textile.The invention relates to the preparation of esters. This is a process for preparing an unsaturated ester with an alkenic double bond, by reacting acrylic acid and / or methacrylic acid with a hydroxy compound having at least one primary hydroxyl group, in the presence of an acid esterification catalyst and a water-immiscible organic solvent. At the end of the esterification reaction, a lithium compound is added to the esterification mixture and the mixture is subjected to distillation. The unsaturated esters obtained can be used for the preparation of radiation-curable binders for printing inks, lacquers, glues and rubbers and in the paper and textile industries.
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
NL7607719A NL7607719A (en) | 1976-07-13 | 1976-07-13 | PROCESS FOR THE PREPARATION OF AN ALKENIC UNSATURATED ESTER. |
Publications (1)
Publication Number | Publication Date |
---|---|
FR2358377A1 true FR2358377A1 (en) | 1978-02-10 |
Family
ID=19826586
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
FR7721283A Withdrawn FR2358377A1 (en) | 1976-07-13 | 1977-07-11 | PROCESS FOR PREPARING AN UNSATURED DOUBLE ALKENIC BONDED ESTER |
Country Status (10)
Country | Link |
---|---|
JP (1) | JPS539712A (en) |
AU (1) | AU508332B2 (en) |
BE (1) | BE856672A (en) |
CA (1) | CA1089874A (en) |
DE (1) | DE2731085C3 (en) |
ES (1) | ES460660A1 (en) |
FR (1) | FR2358377A1 (en) |
GB (1) | GB1535657A (en) |
IT (1) | IT1080673B (en) |
NL (1) | NL7607719A (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0376089A1 (en) * | 1988-12-24 | 1990-07-04 | Henkel Kommanditgesellschaft auf Aktien | Process for the dry neutralization of organic liquid phases |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPH0764790B2 (en) * | 1987-03-24 | 1995-07-12 | 株式会社クラレ | 2-Methyl-1,8-octanedioldi (meth) acrylate |
DE3939163A1 (en) * | 1989-11-27 | 1991-05-29 | Henkel Kgaa | Purificn. of volatile organic cpds. with olefinic double bonds |
JPH01265169A (en) * | 1989-02-22 | 1989-10-23 | Tokyo Electric Power Co Inc:The | Electronic watthour meter |
JPH0358955A (en) * | 1989-07-27 | 1991-03-14 | Nippon Kayaku Co Ltd | Diacrylic ester, resin composition and printing ink composition |
JPH0366643A (en) * | 1989-08-03 | 1991-03-22 | Dai Ichi Kogyo Seiyaku Co Ltd | Diluent for radiation curing resin |
DE19929258A1 (en) * | 1999-06-25 | 2000-12-28 | Basf Ag | Process for the preparation of (meth) acrylic acid esters |
TWI278448B (en) * | 2000-01-27 | 2007-04-11 | Univ Kanagawa | Unsaturated monocarboxylic ester compound, process for producing the same, and composition curable with actinic energy ray |
AU2002228453A1 (en) | 2001-01-11 | 2002-07-24 | DSM IP Assests N.V. | Process for the preparation of esters of (meth)acrylic acid |
CN100445261C (en) * | 2005-05-24 | 2008-12-24 | 上海华谊丙烯酸有限公司 | Synthesis process of (methyl) cyclohexyl acrylate |
DE102014202963A1 (en) * | 2014-02-18 | 2015-08-20 | Basf Se | Process for the preparation of (meth) acrylic esters of polyalkoxy-containing alcohols |
Family Cites Families (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JPS5249449B2 (en) * | 1973-05-21 | 1977-12-17 |
-
1976
- 1976-07-13 NL NL7607719A patent/NL7607719A/en not_active Application Discontinuation
-
1977
- 1977-06-27 IT IT2509977A patent/IT1080673B/en active
- 1977-06-29 AU AU26574/77A patent/AU508332B2/en not_active Expired
- 1977-06-29 JP JP7771277A patent/JPS539712A/en active Granted
- 1977-07-06 GB GB2837977A patent/GB1535657A/en not_active Expired
- 1977-07-09 DE DE19772731085 patent/DE2731085C3/en not_active Expired
- 1977-07-11 FR FR7721283A patent/FR2358377A1/en not_active Withdrawn
- 1977-07-11 CA CA282,399A patent/CA1089874A/en not_active Expired
- 1977-07-11 BE BE179227A patent/BE856672A/en not_active IP Right Cessation
- 1977-07-12 ES ES460660A patent/ES460660A1/en not_active Expired
Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
EP0376089A1 (en) * | 1988-12-24 | 1990-07-04 | Henkel Kommanditgesellschaft auf Aktien | Process for the dry neutralization of organic liquid phases |
WO1990007484A1 (en) * | 1988-12-24 | 1990-07-12 | Henkel Kommanditgesellschaft Auf Aktien | Improved dry neutralization process for liquid organic phases |
Also Published As
Publication number | Publication date |
---|---|
NL7607719A (en) | 1978-01-17 |
ES460660A1 (en) | 1978-05-16 |
GB1535657A (en) | 1978-12-13 |
AU508332B2 (en) | 1980-03-20 |
DE2731085C3 (en) | 1982-04-15 |
AU2657477A (en) | 1979-01-04 |
CA1089874A (en) | 1980-11-18 |
JPS5748057B2 (en) | 1982-10-14 |
DE2731085A1 (en) | 1978-01-26 |
JPS539712A (en) | 1978-01-28 |
DE2731085B2 (en) | 1981-07-23 |
BE856672A (en) | 1977-10-31 |
IT1080673B (en) | 1985-05-16 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
ST | Notification of lapse |