ES356415A1 - Preparation of di(Aminophenyl) Methane - Google Patents
Preparation of di(Aminophenyl) MethaneInfo
- Publication number
- ES356415A1 ES356415A1 ES356415A ES356415A ES356415A1 ES 356415 A1 ES356415 A1 ES 356415A1 ES 356415 A ES356415 A ES 356415A ES 356415 A ES356415 A ES 356415A ES 356415 A1 ES356415 A1 ES 356415A1
- Authority
- ES
- Spain
- Prior art keywords
- aniline
- aminophenyl
- methane
- range
- temperature
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B41—PRINTING; LINING MACHINES; TYPEWRITERS; STAMPS
- B41J—TYPEWRITERS; SELECTIVE PRINTING MECHANISMS, i.e. MECHANISMS PRINTING OTHERWISE THAN FROM A FORME; CORRECTION OF TYPOGRAPHICAL ERRORS
- B41J2/00—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed
- B41J2/485—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by the process of building-up characters or image elements applicable to two or more kinds of printing or marking processes
- B41J2/495—Typewriters or selective printing mechanisms characterised by the printing or marking process for which they are designed characterised by the process of building-up characters or image elements applicable to two or more kinds of printing or marking processes by selective printing from a rotating helical member
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C265/00—Derivatives of isocyanic acid
- C07C265/12—Derivatives of isocyanic acid having isocyanate groups bound to carbon atoms of six-membered aromatic rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Polyurethanes Or Polyureas (AREA)
- Compositions Of Macromolecular Compounds (AREA)
- Epoxy Resins (AREA)
Abstract
Di-(aminophenyl)-methane having a high content of the p,p1-isomer is obtained by condensing aniline and formaldehyde in the presence of hydrochloric acid at a temperature within the range of 0 to 60 C., there being at least 3 moles of water/mole of aniline, the molar ratio of aniline to formaldehyde being substantially within the range of 3 : 1 to 2 : 1 and the molar proportion of acid to aniline being not greater than 1.0, and maintaining the reaction mixture within said temperature range throughout the mixing operation and thereafter at least until the presence of > N-CH 2 -N < bonds can no longer be detected in the reaction mixture and subsequently maintaining the reaction temperature substantially within the range of 0 to 100 C. until the formation of di- (aminophenyl)-methane is complete. Examples are given which illustrate this process.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US65862067A | 1967-08-07 | 1967-08-07 | |
US67915267A | 1967-10-30 | 1967-10-30 |
Publications (1)
Publication Number | Publication Date |
---|---|
ES356415A1 true ES356415A1 (en) | 1970-01-01 |
Family
ID=27097664
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
ES356415A Expired ES356415A1 (en) | 1967-08-07 | 1968-07-23 | Preparation of di(Aminophenyl) Methane |
Country Status (8)
Country | Link |
---|---|
JP (1) | JPS4832104B1 (en) |
BE (1) | BE719163A (en) |
DE (1) | DE1793137A1 (en) |
ES (1) | ES356415A1 (en) |
FR (1) | FR1603607A (en) |
GB (1) | GB1181763A (en) |
NL (1) | NL151065B (en) |
SE (1) | SE367622B (en) |
Families Citing this family (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BE645447A (en) * | 1963-03-20 | |||
DE2238920C3 (en) * | 1972-08-08 | 1984-09-27 | Bayer Ag, 5090 Leverkusen | Process for the production of polyamines |
JPH02285513A (en) * | 1989-04-26 | 1990-11-22 | Dainippon Printing Co Ltd | Recording medium |
US5310769A (en) * | 1992-05-01 | 1994-05-10 | Bayer Aktiengesellschaft | Process for the production of polyamine mixtures of the polyamino-polyaryl-polymethylene series |
CN102443308A (en) * | 2010-10-15 | 2012-05-09 | 上海维度化工科技有限公司 | Preparation method for epoxy floor paint curing agents |
JP6264947B2 (en) * | 2014-03-03 | 2018-01-24 | 東ソー株式会社 | Process for producing a mixture of diphenylmethanediamine and polyphenylenepolymethylenepolyamine |
-
1968
- 1968-07-23 ES ES356415A patent/ES356415A1/en not_active Expired
- 1968-08-01 GB GB3678568A patent/GB1181763A/en not_active Expired
- 1968-08-01 JP JP43054021A patent/JPS4832104B1/ja active Pending
- 1968-08-06 SE SE1059168A patent/SE367622B/xx unknown
- 1968-08-06 FR FR1603607D patent/FR1603607A/en not_active Expired
- 1968-08-07 NL NL6811215A patent/NL151065B/en not_active IP Right Cessation
- 1968-08-07 BE BE719163D patent/BE719163A/en not_active IP Right Cessation
- 1968-08-07 DE DE19681793137 patent/DE1793137A1/en active Pending
Also Published As
Publication number | Publication date |
---|---|
SE367622B (en) | 1974-06-04 |
GB1181763A (en) | 1970-02-18 |
DE1793137A1 (en) | 1972-03-09 |
JPS4832104B1 (en) | 1973-10-04 |
NL6811215A (en) | 1969-02-11 |
NL151065B (en) | 1976-10-15 |
BE719163A (en) | 1969-02-07 |
FR1603607A (en) | 1971-05-10 |
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