EP1082174A1 - Mahltrocknung von zellulose-derivaten, insbesondere methyl-zellulose - Google Patents
Mahltrocknung von zellulose-derivaten, insbesondere methyl-zelluloseInfo
- Publication number
- EP1082174A1 EP1082174A1 EP99924882A EP99924882A EP1082174A1 EP 1082174 A1 EP1082174 A1 EP 1082174A1 EP 99924882 A EP99924882 A EP 99924882A EP 99924882 A EP99924882 A EP 99924882A EP 1082174 A1 EP1082174 A1 EP 1082174A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- air
- product
- grinding
- vortex mill
- fed
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 229920002678 cellulose Polymers 0.000 title claims abstract description 17
- 239000001913 cellulose Substances 0.000 title claims abstract description 15
- 238000001035 drying Methods 0.000 title claims abstract description 14
- 229920000609 methyl cellulose Polymers 0.000 title description 5
- 239000001923 methylcellulose Substances 0.000 title description 5
- 238000000034 method Methods 0.000 claims abstract description 20
- 239000003570 air Substances 0.000 claims description 36
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 9
- 239000012080 ambient air Substances 0.000 claims description 4
- 238000003801 milling Methods 0.000 abstract 4
- 235000010980 cellulose Nutrition 0.000 description 13
- 235000010981 methylcellulose Nutrition 0.000 description 4
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- 238000002347 injection Methods 0.000 description 2
- 239000007924 injection Substances 0.000 description 2
- JTJMJGYZQZDUJJ-UHFFFAOYSA-N phencyclidine Chemical class C1CCCCN1C1(C=2C=CC=CC=2)CCCCC1 JTJMJGYZQZDUJJ-UHFFFAOYSA-N 0.000 description 2
- 238000007796 conventional method Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 238000013024 troubleshooting Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C13/00—Disintegrating by mills having rotary beater elements ; Hammer mills
- B02C13/14—Disintegrating by mills having rotary beater elements ; Hammer mills with vertical rotor shaft, e.g. combined with sifting devices
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/18—Adding fluid, other than for crushing or disintegrating by fluid energy
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C23/00—Auxiliary methods or auxiliary devices or accessories specially adapted for crushing or disintegrating not provided for in preceding groups or not specially adapted to apparatus covered by a single preceding group
- B02C23/18—Adding fluid, other than for crushing or disintegrating by fluid energy
- B02C23/24—Passing gas through crushing or disintegrating zone
- B02C23/26—Passing gas through crushing or disintegrating zone characterised by point of gas entry or exit or by gas flow path
Definitions
- Air whirling mills of the ULTRA-ROTOR type have been used successfully for many years for the grinding or simultaneous grinding and drying of cellulose derivatives.
- Air vortex mills of this type are known, for example, from EP-A-226 900 and from the "Grinding and Drying Plant” brochure from Altenburger Maschinen KG Jburgering & Co.
- Cellulose is usually produced and modified in reactors and then enters the next process step as wet cellulose pulp.
- a free-flowing powder of methyl cellulose was obtained in one step.
- the bulk density of the cellulose was always of great importance.
- the cellulose is conveyed in the wet state, moisture content typically 60-70%, but 80% is possible and more, as a wet product, into a cold air stream in the ULTRA-ROTOR.
- the hot air is first fed into the upper grinding zones and the product is then dried there.
- water can be injected in the lower area of the rotor. This further increases the bulk weight. The water injection ensures that the product remains sufficiently moist and cool during the grinding phase.
- Both fine celluloses, grain size 63 to 150 my, as well as coarser celluloses, grain size 200 to 800 my, intended for consumption, can be ground and dried with a high bulk density.
- FIGS. 1 to 3 each of which shows an air vortex mill 1 with its drive motor 2 in a highly schematic manner.
- the milled and / or dried product usually passes through such mills 1 from bottom to top. Because of the high flow velocities, the product stays in the mill for only a few seconds (e.g. 1 to 2 seconds).
- FIG. 1 shows an air vortex mill according to the prior art. Below the lower grinding stage (grinding stages are only shown in Figure 3) their inlet 3. The product leaves the mill through the outlet 4 located above the grinding stages. This outlet 4 is followed only by the devices shown in FIG. 3, usually cyclones, which serve to separate the product from the air flow.
- FIG. 2 shows an air vortex mill 1 in which the grinding and drying of cellulose derivatives is carried out by the method according to the invention.
- the product is fed to inlet 3 together with ambient air.
- the air vortex mill 1 is equipped with an inlet 5. It is located above the product inlet 3 and opens into the mill 1 at a height at which the crushing process takes place. Water can be injected via the inlet 5 in order to keep the product wet and cool during the comminution process.
- FIG. 3 shows an air vortex mill 1 with seven grinding stages 8. Ambient air and product are supplied to the inlet 3. As indicated by an arrow, product can also be added up to the level of the second grinding stage (inlet 7).
- the grinding process essentially takes place in the lower and middle region of the mill 1. As already mentioned, it is advisable to inject water at ambient temperature or cooler (e.g. 14 ° C) at the level of the grinding zones in which the crushing takes place, so that the product moisture does not drop below about 70%. In the illustrated embodiment, the injection takes place between the third and fifth grinding stage 8. Two water inlets 5, 5 'can also be provided.
- the warm or hot air - e.g. with a temperature of 1 80 to 220 ° C - is only supplied at the level of the upper stages (in the illustrated embodiment at the level of the sixth stage).
- the drying of the product takes place in this area.
- a residual moisture of less than 5% H20 is aimed for. If this is not achieved in the top two stages, there is the possibility, on the one hand, of increasing the number of stages of the air vortex mill.
- the residual moisture can be set to the desired level in a dryer of any kind connected to the outlet 4.
- a dryer 9 connected to the outlet 4 is shown schematically. This is followed by a cyclone system 10 known per se for separating product and air.
Landscapes
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Polysaccharides And Polysaccharide Derivatives (AREA)
- Crushing And Grinding (AREA)
Abstract
Description
Claims
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19823563A DE19823563A1 (de) | 1998-05-27 | 1998-05-27 | Mahltrocknung von Zellulose-Derivaten, insbesondere Methl-Zellulose |
DE19823563 | 1998-05-27 | ||
PCT/EP1999/003077 WO1999061157A1 (de) | 1998-05-27 | 1999-05-05 | Mahltrocknung von zellulose-derivaten, insbesondere methyl-zellulose |
Publications (2)
Publication Number | Publication Date |
---|---|
EP1082174A1 true EP1082174A1 (de) | 2001-03-14 |
EP1082174B1 EP1082174B1 (de) | 2002-02-13 |
Family
ID=7869001
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP99924882A Expired - Lifetime EP1082174B1 (de) | 1998-05-27 | 1999-05-05 | Mahltrocknung von zellulose-derivaten, insbesondere methyl-zellulose |
Country Status (3)
Country | Link |
---|---|
EP (1) | EP1082174B1 (de) |
DE (2) | DE19823563A1 (de) |
WO (1) | WO1999061157A1 (de) |
Families Citing this family (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE20021758U1 (de) * | 2000-12-22 | 2002-05-08 | Sniehotta, Michael, Dipl.-Ing., Dipl.-Geol., 45699 Herten | Prallmühle mit Schlagwerkzeugen an einem motorgetriebenen Rotor |
DE102005032248B4 (de) * | 2005-07-09 | 2009-04-23 | Tronox Pigments Gmbh | Titandioxidpigmentherstellung unter Verwendung einer Luftwirbelmühle |
DE102006006096A1 (de) * | 2006-02-10 | 2007-08-16 | Altenburger Maschinen Jäckering GmbH | Vorrichtung und Verfahren zur Einspeisung von feuchten und/oder klebrigen Produkten, insbesondere Zellulose, in einer Luftwirbelmühle |
DE102006033791A1 (de) * | 2006-07-19 | 2008-01-24 | Prokon Nord Energiesysteme Gmbh | Verbesserte Verfahren zur Herstellung von Ethanol, Gluten und und Kleie aus Getreide |
DE102010009894A1 (de) | 2010-03-02 | 2011-09-08 | Rolf Schatz | Rotor-Mahlwerkzeug für Rotorprallmühlen |
DE102014015964A1 (de) | 2014-10-31 | 2016-06-16 | Pallmann Maschinenfabrik Gmbh & Co. Kg | Vorrichtung und Verfahren zum Bearbeiten von Aufgabegut |
DE102022132971A1 (de) | 2022-12-12 | 2024-06-13 | PWA recycling concept GmbH | Vorrichtung zum Zerkleinern und/oder Aufbereiten von Material, Anordnung und Verfahren |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE3543370A1 (de) * | 1985-12-07 | 1987-06-11 | Jackering Altenburger Masch | Muehle mit mehreren mahlstufen |
DE3811910C2 (de) * | 1988-04-09 | 1997-04-10 | Mahltechnik Goergens Gmbh | Mühle und Verfahren zum gleichzeitigen Mahlen und Trocknen eines feuchten Produkts |
DE3839831A1 (de) * | 1988-11-25 | 1990-05-31 | Hoechst Ag | Verfahren und vorrichtung zur produktschonenden mahlung und gleichzeitigen trocknung von feuchten celluloseethern |
DE19641781A1 (de) * | 1996-10-10 | 1998-04-16 | Clariant Gmbh | Verfahren und Vorrichtung zum gleichzeitigen Mahlen und Trocknen eines feuchten Celluloseether enthaltenden Mahlgutes |
-
1998
- 1998-05-27 DE DE19823563A patent/DE19823563A1/de not_active Withdrawn
-
1999
- 1999-05-05 EP EP99924882A patent/EP1082174B1/de not_active Expired - Lifetime
- 1999-05-05 WO PCT/EP1999/003077 patent/WO1999061157A1/de active IP Right Grant
- 1999-05-05 DE DE59900869T patent/DE59900869D1/de not_active Expired - Lifetime
Non-Patent Citations (1)
Title |
---|
See references of WO9961157A1 * |
Also Published As
Publication number | Publication date |
---|---|
WO1999061157A1 (de) | 1999-12-02 |
DE59900869D1 (de) | 2002-03-21 |
EP1082174B1 (de) | 2002-02-13 |
DE19823563A1 (de) | 1999-12-02 |
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