EP0695813A3 - Process for carburizing carburisable work pieces under the action of plasma-pulses - Google Patents

Process for carburizing carburisable work pieces under the action of plasma-pulses Download PDF

Info

Publication number
EP0695813A3
EP0695813A3 EP95109082A EP95109082A EP0695813A3 EP 0695813 A3 EP0695813 A3 EP 0695813A3 EP 95109082 A EP95109082 A EP 95109082A EP 95109082 A EP95109082 A EP 95109082A EP 0695813 A3 EP0695813 A3 EP 0695813A3
Authority
EP
European Patent Office
Prior art keywords
carburisable
carburizing
pulses
plasma
action
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP95109082A
Other languages
German (de)
French (fr)
Other versions
EP0695813A2 (en
EP0695813B1 (en
Inventor
Frank Dr Schnatbaum
Albrecht Dr Melber
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ALD Vacuum Technologies GmbH
Original Assignee
ALD Vacuum Technologies GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ALD Vacuum Technologies GmbH filed Critical ALD Vacuum Technologies GmbH
Publication of EP0695813A2 publication Critical patent/EP0695813A2/en
Publication of EP0695813A3 publication Critical patent/EP0695813A3/en
Application granted granted Critical
Publication of EP0695813B1 publication Critical patent/EP0695813B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C23COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23CCOATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C8/00Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals
    • C23C8/06Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases
    • C23C8/36Solid state diffusion of only non-metal elements into metallic material surfaces; Chemical surface treatment of metallic material by reaction of the surface with a reactive gas, leaving reaction products of surface material in the coating, e.g. conversion coatings, passivation of metals using gases using ionised gases, e.g. ionitriding
    • C23C8/38Treatment of ferrous surfaces

Abstract

Workpieces of carburizable materials, especially steels, are carburized by means of a pulsed plasma discharge in a carbon-containing atmosphere at pressures of 0.1-30 mbars and at pulsed voltages of 200-2,000 V, preferably of 300-1,000 V. A continuously applied baseline voltage, which is below the breakdown voltage, is superimposed on the pulsed voltage. The baseline voltage is preferably a direct-current voltage, which is in the range of 10-150 V, preferably of 20-100 V.
EP95109082A 1994-08-06 1995-06-13 Process for carburizing carburisable work pieces under the action of plasma-pulses Expired - Lifetime EP0695813B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
DE4427902 1994-08-06
DE4427902A DE4427902C1 (en) 1994-08-06 1994-08-06 Method for carburising components made from carburisable materials by means of a plasma discharge operated in a pulsed fashion

Publications (3)

Publication Number Publication Date
EP0695813A2 EP0695813A2 (en) 1996-02-07
EP0695813A3 true EP0695813A3 (en) 1997-02-12
EP0695813B1 EP0695813B1 (en) 1999-09-08

Family

ID=6525098

Family Applications (1)

Application Number Title Priority Date Filing Date
EP95109082A Expired - Lifetime EP0695813B1 (en) 1994-08-06 1995-06-13 Process for carburizing carburisable work pieces under the action of plasma-pulses

Country Status (5)

Country Link
US (1) US5558725A (en)
EP (1) EP0695813B1 (en)
JP (1) JPH08170162A (en)
AT (1) ATE184329T1 (en)
DE (2) DE4427902C1 (en)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE19547131A1 (en) 1995-12-16 1997-06-19 Ipsen Ind Int Gmbh Process for plasma carburizing metallic workpieces
WO1999031291A2 (en) * 1997-12-15 1999-06-24 Volkswagen Aktiengesellschaft Plasma boronizing
GB2336603A (en) * 1998-04-23 1999-10-27 Metaltech Limited A method and apparatus for plasma boronising
IT1309928B1 (en) * 1999-12-01 2002-02-05 Bundy S P A PIPE FOR PRESSURE FLUID SUPPLY SYSTEMS, IN PARTICULAR FOR FUEL SUPPLY IN DIESEL ENGINES,
DE10021583A1 (en) * 2000-05-04 2001-11-15 Ald Vacuum Techn Ag Assembly to carburize and harden steel workpiece charges has structured pressures in the transport tunnel and heating chambers and carburizing and quenching chambers to reduce energy costs
JP4744019B2 (en) * 2000-07-12 2011-08-10 大阪府 Method for surface treatment of titanium metal
DE10109565B4 (en) 2001-02-28 2005-10-20 Vacuheat Gmbh Method and device for partial thermochemical vacuum treatment of metallic workpieces
KR100614288B1 (en) * 2005-01-17 2006-08-21 한국에너지기술연구원 The process control technology of low-pressure carburizing with pulse injection of gas
DE102013006589A1 (en) * 2013-04-17 2014-10-23 Ald Vacuum Technologies Gmbh Method and device for the thermochemical hardening of workpieces
JP7421373B2 (en) * 2020-03-02 2024-01-24 日立Astemo株式会社 Carburizing method and base material to be treated

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2946708A (en) * 1950-11-09 1960-07-26 Berghaus Elektrophysik Anst Nitriding with electric glow discharge
DE2842407A1 (en) * 1978-09-29 1980-04-03 Norbert Stauder Surface treatment of workpiece in sealed chamber by glow discharge - where ionisation plasma burner is used to reinforce ionised gas in chamber, e.g. for nitriding or carburising steel
US4406765A (en) * 1980-01-28 1983-09-27 Fuji Photo Film Co., Ltd. Apparatus and process for production of amorphous semiconductor
JPH02125856A (en) * 1988-11-04 1990-05-14 Shindengen Electric Mfg Co Ltd Device for thermochemically treating metal of the like
DE4003623A1 (en) * 1990-02-07 1991-08-08 Kloeckner Ionon METHOD FOR CONTROLLING A PLANT TREATMENT SYSTEM FOR WORKPIECES
DE4238993C1 (en) * 1992-01-20 1993-07-01 Leybold Durferrit Gmbh, 5000 Koeln, De
FR2708624A1 (en) * 1993-07-30 1995-02-10 Neuville Stephane Process for deposition of a protective coating based on amorphous diamond pseudocarbon or on modified silicon carbide

Family Cites Families (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE601847C (en) * 1933-04-01 1934-08-25 Siemens Schuckertwerke Akt Ges Method for introducing a substance into a metal
FR2501727A1 (en) * 1981-03-13 1982-09-17 Vide Traitement PROCESS FOR THE THERMOCHEMICAL TREATMENT OF METALS BY ION BOMBING
US5127967A (en) * 1987-09-04 1992-07-07 Surface Combustion, Inc. Ion carburizing
US5383980A (en) * 1992-01-20 1995-01-24 Leybold Durferrit Gmbh Process for hardening workpieces in a pulsed plasma discharge

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2946708A (en) * 1950-11-09 1960-07-26 Berghaus Elektrophysik Anst Nitriding with electric glow discharge
DE2842407A1 (en) * 1978-09-29 1980-04-03 Norbert Stauder Surface treatment of workpiece in sealed chamber by glow discharge - where ionisation plasma burner is used to reinforce ionised gas in chamber, e.g. for nitriding or carburising steel
US4406765A (en) * 1980-01-28 1983-09-27 Fuji Photo Film Co., Ltd. Apparatus and process for production of amorphous semiconductor
JPH02125856A (en) * 1988-11-04 1990-05-14 Shindengen Electric Mfg Co Ltd Device for thermochemically treating metal of the like
DE4003623A1 (en) * 1990-02-07 1991-08-08 Kloeckner Ionon METHOD FOR CONTROLLING A PLANT TREATMENT SYSTEM FOR WORKPIECES
DE4238993C1 (en) * 1992-01-20 1993-07-01 Leybold Durferrit Gmbh, 5000 Koeln, De
FR2708624A1 (en) * 1993-07-30 1995-02-10 Neuville Stephane Process for deposition of a protective coating based on amorphous diamond pseudocarbon or on modified silicon carbide

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
PATENT ABSTRACTS OF JAPAN vol. 14, no. 342 (C - 0743) 24 July 1990 (1990-07-24) *

Also Published As

Publication number Publication date
DE59506771D1 (en) 1999-10-14
US5558725A (en) 1996-09-24
EP0695813A2 (en) 1996-02-07
EP0695813B1 (en) 1999-09-08
JPH08170162A (en) 1996-07-02
ATE184329T1 (en) 1999-09-15
DE4427902C1 (en) 1995-03-30

Similar Documents

Publication Publication Date Title
EP0695813A3 (en) Process for carburizing carburisable work pieces under the action of plasma-pulses
AU8101098A (en) Device and method for cleaning or drying work pieces
ES2163561T3 (en) PROCEDURE TO INCREASE THE HUMECTABILITY OF ITEM SURFACES.
ATE302019T1 (en) METHOD AND COMPOSITIONS FOR OPTIMIZING OXYGEN TRANSPORT IN CELL-FREE SYSTEMS
EP1702734A3 (en) Method and apparatus for fluid jet formation
DE59701121D1 (en) METHOD FOR COATING OR WELDING EASILY OXIDIZABLE MATERIALS AND PLASMA BURNER THEREFOR
DE69009603T2 (en) Process for the pretreatment of metallic workpieces and the nitriding hardening of steel.
GB9715180D0 (en) Process for the treatment of austenitic stainless steel articles
EP0933440A4 (en) Case hardened steel excellent in the prevention of coarsening of particles during carburizing thereof, method of manufacturing the same, and raw shaped material for carburized parts
MY116621A (en) Method and apparatus for grinding brittle materials
PL338794A1 (en) Blood plasma for versatile application
HUP9801540A1 (en) Process for manufacturing a carburized or carbonitrided steel component, and steel for the manufacturing of this component
ZA200000523B (en) Process for the treatment of steel work gases.
ES2144868T3 (en) SURFACE TREATMENT METHOD BY DRY WAY AND DEVICE FOR THE APPLICATION OF AN ASI METHOD.
GB2320713A (en) Process for the destruction of chemical agents and munitions
AU5083300A (en) Method of and apparatus for removing material
DE59908093D1 (en) Method and device for fine machining of essentially cylindrical workpiece surfaces
DE59205356D1 (en) Process for hardening workpieces in a pulse plasma discharge
ES2181906T3 (en) INSTALLATION FOR FINISHING PARTS SURFACES.
UA8625A1 (en) Method for thermo-chemical treatment of articles
Gotz Hardening Without Rework
Pop et al. The superficial microalloying of tool steel by an electrical discharge method
Melber et al. Method of Hardening Workpieces in a Pulsed Plasma Discharge
RU98117499A (en) METHOD FOR ANTIFRICTION CHEMICAL AND THERMAL TREATMENT OF INSTRUMENTAL STEELS
Li et al. Vacuum ion surface alloying in alternating current field and its application for hacksaw blade

Legal Events

Date Code Title Description
PUAI Public reference made under article 153(3) epc to a published international application that has entered the european phase

Free format text: ORIGINAL CODE: 0009012

AK Designated contracting states

Kind code of ref document: A2

Designated state(s): AT CH DE FR GB IT LI SE

PUAL Search report despatched

Free format text: ORIGINAL CODE: 0009013

AK Designated contracting states

Kind code of ref document: A3

Designated state(s): AT CH DE FR GB IT LI SE

17P Request for examination filed

Effective date: 19970510

GRAG Despatch of communication of intention to grant

Free format text: ORIGINAL CODE: EPIDOS AGRA

17Q First examination report despatched

Effective date: 19981023

GRAG Despatch of communication of intention to grant

Free format text: ORIGINAL CODE: EPIDOS AGRA

GRAH Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOS IGRA

GRAH Despatch of communication of intention to grant a patent

Free format text: ORIGINAL CODE: EPIDOS IGRA

GRAA (expected) grant

Free format text: ORIGINAL CODE: 0009210

ITF It: translation for a ep patent filed

Owner name: BARZANO' E ZANARDO MILANO S.P.A.

AK Designated contracting states

Kind code of ref document: B1

Designated state(s): AT CH DE FR GB IT LI SE

REF Corresponds to:

Ref document number: 184329

Country of ref document: AT

Date of ref document: 19990915

Kind code of ref document: T

REG Reference to a national code

Ref country code: CH

Ref legal event code: NV

Representative=s name: KEMENY AG PATENTANWALTBUERO

Ref country code: CH

Ref legal event code: EP

GBT Gb: translation of ep patent filed (gb section 77(6)(a)/1977)

Effective date: 19990910

REF Corresponds to:

Ref document number: 59506771

Country of ref document: DE

Date of ref document: 19991014

ET Fr: translation filed
RAP2 Party data changed (patent owner data changed or rights of a patent transferred)

Owner name: ALD VACUUM TECHNOLOGIES AG

PLBE No opposition filed within time limit

Free format text: ORIGINAL CODE: 0009261

REG Reference to a national code

Ref country code: FR

Ref legal event code: CJ

STAA Information on the status of an ep patent application or granted ep patent

Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT

26N No opposition filed
REG Reference to a national code

Ref country code: GB

Ref legal event code: IF02

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: FR

Payment date: 20050512

Year of fee payment: 11

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: GB

Payment date: 20050516

Year of fee payment: 11

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: SE

Payment date: 20050519

Year of fee payment: 11

Ref country code: CH

Payment date: 20050519

Year of fee payment: 11

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: GB

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20060613

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: SE

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20060614

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: LI

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20060630

Ref country code: CH

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20060630

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: IT

Payment date: 20060630

Year of fee payment: 12

REG Reference to a national code

Ref country code: CH

Ref legal event code: PL

EUG Se: european patent has lapsed
GBPC Gb: european patent ceased through non-payment of renewal fee

Effective date: 20060613

REG Reference to a national code

Ref country code: FR

Ref legal event code: ST

Effective date: 20070228

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: FR

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20060630

PG25 Lapsed in a contracting state [announced via postgrant information from national office to epo]

Ref country code: IT

Free format text: LAPSE BECAUSE OF NON-PAYMENT OF DUE FEES

Effective date: 20070613

PGFP Annual fee paid to national office [announced via postgrant information from national office to epo]

Ref country code: AT

Payment date: 20140611

Year of fee payment: 20

Ref country code: DE

Payment date: 20140619

Year of fee payment: 20

REG Reference to a national code

Ref country code: DE

Ref legal event code: R071

Ref document number: 59506771

Country of ref document: DE

REG Reference to a national code

Ref country code: AT

Ref legal event code: MK07

Ref document number: 184329

Country of ref document: AT

Kind code of ref document: T

Effective date: 20150613