EP0654956A1 - Méthode de fabrication d'une couche chauffée électriquement - Google Patents
Méthode de fabrication d'une couche chauffée électriquement Download PDFInfo
- Publication number
- EP0654956A1 EP0654956A1 EP93810818A EP93810818A EP0654956A1 EP 0654956 A1 EP0654956 A1 EP 0654956A1 EP 93810818 A EP93810818 A EP 93810818A EP 93810818 A EP93810818 A EP 93810818A EP 0654956 A1 EP0654956 A1 EP 0654956A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- electric heating
- heating film
- manufacturing
- base material
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000005485 electric heating Methods 0.000 title claims abstract description 32
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 20
- 239000000463 material Substances 0.000 claims abstract description 33
- 239000000203 mixture Substances 0.000 claims abstract description 16
- 239000011344 liquid material Substances 0.000 claims abstract description 14
- 238000010438 heat treatment Methods 0.000 claims abstract description 7
- 150000002500 ions Chemical class 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims abstract description 6
- 239000012535 impurity Substances 0.000 claims abstract description 4
- 238000003756 stirring Methods 0.000 claims abstract description 4
- 229910044991 metal oxide Inorganic materials 0.000 claims abstract description 3
- 230000003213 activating effect Effects 0.000 claims abstract 2
- 238000005507 spraying Methods 0.000 claims abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 claims description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 235000019441 ethanol Nutrition 0.000 claims description 2
- 239000011521 glass Substances 0.000 claims description 2
- 235000011167 hydrochloric acid Nutrition 0.000 claims description 2
- 239000010445 mica Substances 0.000 claims description 2
- 229910052618 mica group Inorganic materials 0.000 claims description 2
- 229910052573 porcelain Inorganic materials 0.000 claims description 2
- 239000010453 quartz Substances 0.000 claims description 2
- 239000000470 constituent Substances 0.000 description 3
- 229910000410 antimony oxide Inorganic materials 0.000 description 2
- VTRUBDSFZJNXHI-UHFFFAOYSA-N oxoantimony Chemical compound [Sb]=O VTRUBDSFZJNXHI-UHFFFAOYSA-N 0.000 description 2
- NDVLTYZPCACLMA-UHFFFAOYSA-N silver oxide Chemical compound [O-2].[Ag+].[Ag+] NDVLTYZPCACLMA-UHFFFAOYSA-N 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- XOLBLPGZBRYERU-UHFFFAOYSA-N tin dioxide Chemical compound O=[Sn]=O XOLBLPGZBRYERU-UHFFFAOYSA-N 0.000 description 2
- 229910001887 tin oxide Inorganic materials 0.000 description 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- KZNMRPQBBZBTSW-UHFFFAOYSA-N [Au]=O Chemical compound [Au]=O KZNMRPQBBZBTSW-UHFFFAOYSA-N 0.000 description 1
- XHCLAFWTIXFWPH-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] Chemical compound [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] XHCLAFWTIXFWPH-UHFFFAOYSA-N 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- CXKCTMHTOKXKQT-UHFFFAOYSA-N cadmium oxide Inorganic materials [Cd]=O CXKCTMHTOKXKQT-UHFFFAOYSA-N 0.000 description 1
- CFEAAQFZALKQPA-UHFFFAOYSA-N cadmium(2+);oxygen(2-) Chemical compound [O-2].[Cd+2] CFEAAQFZALKQPA-UHFFFAOYSA-N 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- TXKMVPPZCYKFAC-UHFFFAOYSA-N disulfur monoxide Inorganic materials O=S=S TXKMVPPZCYKFAC-UHFFFAOYSA-N 0.000 description 1
- 238000001035 drying Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000003292 glue Substances 0.000 description 1
- 229910001922 gold oxide Inorganic materials 0.000 description 1
- BHEPBYXIRTUNPN-UHFFFAOYSA-N hydridophosphorus(.) (triplet) Chemical compound [PH] BHEPBYXIRTUNPN-UHFFFAOYSA-N 0.000 description 1
- 229910003437 indium oxide Inorganic materials 0.000 description 1
- PJXISJQVUVHSOJ-UHFFFAOYSA-N indium(iii) oxide Chemical compound [O-2].[O-2].[O-2].[In+3].[In+3] PJXISJQVUVHSOJ-UHFFFAOYSA-N 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 229910000476 molybdenum oxide Inorganic materials 0.000 description 1
- PQQKPALAQIIWST-UHFFFAOYSA-N oxomolybdenum Chemical compound [Mo]=O PQQKPALAQIIWST-UHFFFAOYSA-N 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 230000001737 promoting effect Effects 0.000 description 1
- 239000004065 semiconductor Substances 0.000 description 1
- 229910052814 silicon oxide Inorganic materials 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 229910001923 silver oxide Inorganic materials 0.000 description 1
- 239000008234 soft water Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- XTQHKBHJIVJGKJ-UHFFFAOYSA-N sulfur monoxide Chemical compound S=O XTQHKBHJIVJGKJ-UHFFFAOYSA-N 0.000 description 1
- 229910001935 vanadium oxide Inorganic materials 0.000 description 1
Images
Classifications
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/20—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater
- H05B3/22—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater non-flexible
- H05B3/26—Heating elements having extended surface area substantially in a two-dimensional plane, e.g. plate-heater non-flexible heating conductor mounted on insulating base
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B3/00—Ohmic-resistance heating
- H05B3/10—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor
- H05B3/12—Heating elements characterised by the composition or nature of the materials or by the arrangement of the conductor characterised by the composition or nature of the conductive material
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B2203/00—Aspects relating to Ohmic resistive heating covered by group H05B3/00
- H05B2203/013—Heaters using resistive films or coatings
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B2203/00—Aspects relating to Ohmic resistive heating covered by group H05B3/00
- H05B2203/017—Manufacturing methods or apparatus for heaters
-
- H—ELECTRICITY
- H05—ELECTRIC TECHNIQUES NOT OTHERWISE PROVIDED FOR
- H05B—ELECTRIC HEATING; ELECTRIC LIGHT SOURCES NOT OTHERWISE PROVIDED FOR; CIRCUIT ARRANGEMENTS FOR ELECTRIC LIGHT SOURCES, IN GENERAL
- H05B2203/00—Aspects relating to Ohmic resistive heating covered by group H05B3/00
- H05B2203/032—Heaters specially adapted for heating by radiation heating
Definitions
- This invention relates to a method of manufacturing an improved electric heating film.
- the method of manufacturing an electric heating film according to the present invention mainly comprises steps of preparing a mixture 10 by mixing a plurality of compounds, mixing the mixture with medium materials to form a liquid material, cleaning and drying the base material, atomizing the liquid material, and coating the base material 12.
- the steps of the manufacturing method will be described in detail hereinafter.
- Tin oxide is the easiest to obtain and lowest in cost and so it is used as the main material.
- oxides are non-conductive substances and will become semi-conductors when incorporated of certain impurities.
- impurities in weight has been added into the oxides so as to modify the resistivity of the mixture thereby controlling the heat evolved from the mixture.
- the medium material may be water, methyl alcohol, ethyl alcohol, hydrochloric acid, ethylamine, ...etc.
- the mixture and the medium material are stirred well to form a liquid material which is then filtered so as to remove the undesired matter therein.
- the base material 12 is to coated with the electric heating film according to the present invention.
- the base material 12 may be in the shape of a tube, a panel, or a beehive 21 shown in FIG. 3.
- the base material 12 may be conveniently made of quartz, glass, porcelain, mica or similar material with high temperature resistance and low expansion coefficient.
- the base material 12 must be inspected, washed with clean soft water and dilute hydrochloric acid, and dried before use.
- the base material into a heating furnace (not shown) and heated to 400-800 degrees centigrade for 5-10 minutes so as to activate the surface of the base material. Then, mix the liquid material with air at a certain proportion and spray them into the heating furnace by means of a compressor at an air pressure of 2.0 kg/cm3 hence atomizing and dissolving the liquid material into ions. Thereafter, let the ions be accumulated and evenly coated on the base material 12 to a thickness of 3-300 ⁇ thereby providing the base material 12 with a layer of electric heating film according to the present invention. Thereafter, the base material in the shape of a beehive is coated with a layer of silver glue 21 with a temperature resistance of higher than 850 degrees centigrade and a resistance lesser than 0.3 ohm.
- the general time for atomizing the liquid material is about 10-30 minutes and depends on the thickness of the film designed to be coated on the base material and the power of the heating furnace.
- the electric heating film coated on the base material 12 is very thin, the electric current consumed is very small and the heat energy is transmitted from inside to outside, the temperature difference between the inside and outside will be small and it is unnecessary to worry about explosion.
- the temperature evolved from the electric heating film can reach 700 degrees centigrade. Further, no obvious flame will be produced when the temperature is lower 500 degrees centigrade.
- the electric heating will consume less than 70 per cent of electricity required by the prior art.
- FIG. 5 illustrates the relationship between the power and the temperature of the present invention.
- the power consumption of the present invention is much lower than that required by the prior art.
- FIG. 6 shows the relationship between the refractive index and the wave length of the present invention.
- the heat energy of the present invention includes far infrared energy and radiating energy and 80% of the heat energy comes from the far infrared energy.
Landscapes
- Resistance Heating (AREA)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP93810818A EP0654956A1 (fr) | 1993-11-24 | 1993-11-24 | Méthode de fabrication d'une couche chauffée électriquement |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
EP93810818A EP0654956A1 (fr) | 1993-11-24 | 1993-11-24 | Méthode de fabrication d'une couche chauffée électriquement |
Publications (1)
Publication Number | Publication Date |
---|---|
EP0654956A1 true EP0654956A1 (fr) | 1995-05-24 |
Family
ID=8215074
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
EP93810818A Withdrawn EP0654956A1 (fr) | 1993-11-24 | 1993-11-24 | Méthode de fabrication d'une couche chauffée électriquement |
Country Status (1)
Country | Link |
---|---|
EP (1) | EP0654956A1 (fr) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001043506A1 (fr) * | 1999-12-10 | 2001-06-14 | Bdsb Holdings Limited | Procede de fabrication d'elements chauffants a resistance electrique composes d'oxydes metalliques semi-conducteurs et elements a resistance ainsi fabriques |
WO2005055662A1 (fr) * | 2003-12-02 | 2005-06-16 | Jian Chen | Film chauffant electrique inorganique multifonction, a haute efficacite, resistant aux temperatures elevees, et son procede de production |
EP1681905A1 (fr) * | 2005-01-17 | 2006-07-19 | Cheng-Ping Lin | Méthode de fabrication d'un film électrique chauffant à semiconducteur |
CN102291860A (zh) * | 2011-04-25 | 2011-12-21 | 马秀芝 | 一种自限温氧化物电热膜的制造方法 |
CN102843793A (zh) * | 2011-06-24 | 2012-12-26 | 北京万众光通科技发展有限公司 | 一种电热转换体涂层配方及使用方法 |
CN102925880A (zh) * | 2012-11-16 | 2013-02-13 | 宁波祈禧电器有限公司 | 一种氧化锡锑透明电热膜的制备方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE908882C (de) * | 1946-05-02 | 1954-04-12 | Corning Glass Works | Elektrischer Widerstand und Verfahren zu seiner Herstellung |
DE2121319A1 (de) * | 1971-04-30 | 1973-01-18 | Rocholl Martin Ggottfried Dipl | Verfahren zum beschichten von glasscheiben mit einem optisch transparenten flaechenheizleiter |
EP0208808A1 (fr) * | 1985-07-11 | 1987-01-21 | Zhu Hanxiong | Résistance imprimée, sa méthode de fabrication et son application |
EP0280362A2 (fr) * | 1987-02-21 | 1988-08-31 | Philips Patentverwaltung GmbH | Elément chauffant en couche mince |
EP0302589A1 (fr) * | 1987-06-27 | 1989-02-08 | Jeffery Boardman | Procédé pour fabriquer des éléments de chauffage électriques et éléments de chauffage électriques fabriqués d'après ce procédé |
FR2640803A1 (fr) * | 1988-12-15 | 1990-06-22 | Neiman Sa | Resistance en ceramique a haute temperature |
-
1993
- 1993-11-24 EP EP93810818A patent/EP0654956A1/fr not_active Withdrawn
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE908882C (de) * | 1946-05-02 | 1954-04-12 | Corning Glass Works | Elektrischer Widerstand und Verfahren zu seiner Herstellung |
DE2121319A1 (de) * | 1971-04-30 | 1973-01-18 | Rocholl Martin Ggottfried Dipl | Verfahren zum beschichten von glasscheiben mit einem optisch transparenten flaechenheizleiter |
EP0208808A1 (fr) * | 1985-07-11 | 1987-01-21 | Zhu Hanxiong | Résistance imprimée, sa méthode de fabrication et son application |
EP0280362A2 (fr) * | 1987-02-21 | 1988-08-31 | Philips Patentverwaltung GmbH | Elément chauffant en couche mince |
EP0302589A1 (fr) * | 1987-06-27 | 1989-02-08 | Jeffery Boardman | Procédé pour fabriquer des éléments de chauffage électriques et éléments de chauffage électriques fabriqués d'après ce procédé |
FR2640803A1 (fr) * | 1988-12-15 | 1990-06-22 | Neiman Sa | Resistance en ceramique a haute temperature |
Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2001043506A1 (fr) * | 1999-12-10 | 2001-06-14 | Bdsb Holdings Limited | Procede de fabrication d'elements chauffants a resistance electrique composes d'oxydes metalliques semi-conducteurs et elements a resistance ainsi fabriques |
WO2005055662A1 (fr) * | 2003-12-02 | 2005-06-16 | Jian Chen | Film chauffant electrique inorganique multifonction, a haute efficacite, resistant aux temperatures elevees, et son procede de production |
CN100426936C (zh) * | 2003-12-02 | 2008-10-15 | 北京明盛电通能源新技术有限公司 | 一种耐高温无机电热膜及其制作方法 |
EP1681905A1 (fr) * | 2005-01-17 | 2006-07-19 | Cheng-Ping Lin | Méthode de fabrication d'un film électrique chauffant à semiconducteur |
CN102291860A (zh) * | 2011-04-25 | 2011-12-21 | 马秀芝 | 一种自限温氧化物电热膜的制造方法 |
CN102291860B (zh) * | 2011-04-25 | 2013-02-27 | 许子燕 | 一种自限温氧化物电热膜的制造方法 |
CN102843793A (zh) * | 2011-06-24 | 2012-12-26 | 北京万众光通科技发展有限公司 | 一种电热转换体涂层配方及使用方法 |
CN102843793B (zh) * | 2011-06-24 | 2015-05-20 | 北京万众光通科技发展有限公司 | 一种电热转换体涂层及使用方法 |
CN102925880A (zh) * | 2012-11-16 | 2013-02-13 | 宁波祈禧电器有限公司 | 一种氧化锡锑透明电热膜的制备方法 |
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Legal Events
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PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
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AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): AT BE CH DE DK ES FR GB IT LI NL SE |
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18D | Application deemed to be withdrawn |
Effective date: 19951125 |