EP0247702B1 - Cigarettes - Google Patents

Cigarettes Download PDF

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Publication number
EP0247702B1
EP0247702B1 EP87201198A EP87201198A EP0247702B1 EP 0247702 B1 EP0247702 B1 EP 0247702B1 EP 87201198 A EP87201198 A EP 87201198A EP 87201198 A EP87201198 A EP 87201198A EP 0247702 B1 EP0247702 B1 EP 0247702B1
Authority
EP
European Patent Office
Prior art keywords
tipping paper
mouth end
layer
sleeve
rod
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
EP87201198A
Other languages
German (de)
French (fr)
Other versions
EP0247702A2 (en
EP0247702A3 (en
Inventor
Reginald Wayne Newsome
Walter Allen Nichols
Willard Anthony Geiszler
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Philip Morris Products Inc
Original Assignee
Philip Morris Products Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Philip Morris Products Inc filed Critical Philip Morris Products Inc
Priority to AT87201198T priority Critical patent/ATE87185T1/en
Publication of EP0247702A2 publication Critical patent/EP0247702A2/en
Publication of EP0247702A3 publication Critical patent/EP0247702A3/en
Application granted granted Critical
Publication of EP0247702B1 publication Critical patent/EP0247702B1/en
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24DCIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D3/00Tobacco smoke filters, e.g. filter-tips, filtering inserts; Filters specially adapted for simulated smoking devices; Mouthpieces for cigars or cigarettes
    • A24D3/04Tobacco smoke filters characterised by their shape or structure
    • A24D3/041Tobacco smoke filters characterised by their shape or structure with adjustable means for modifying the degree of filtration of the filter

Definitions

  • the present invention relates to cigarettes. More particularly, the present invention relates to cigarettes which are adjustable to provide a wide range of air dilution values.
  • the sleeve or filter plug may be removed from the cigarette by the smoker and not readily replaced, and that when dilution is desired, thus requiring some degree of registry between the two sets of openings, this registry may be inadvertently destroyed by a slight axial movement of the sleeve or plug. Accordingly, the dilution, once set by the smoker, is not ensured of any degree of consistency.
  • Yet another problem associated with a number of these prior devices is that they have not been readily adaptable to a high rate of production on cigarette making machinery of conventional design.
  • US-A-3 359 988 discloses a filter cigarette, the filter of which is divided longitudinally into two channels, one uniquely for air and the other uniquely for smoke. Ingress of air to the air channel is controlled by movement of a circumferential band around the filter, the band having a hole in it which is moved into and out of registry with holes in the external wall of the air channel.
  • a smoking article comprising a rod of combustible smoking material and a mouth end region open to permit the passage of air and smoke, the mouth end region having a peripheral area thereof adapted for the passage of air therethrough, and being circumscribed by a substantially air impermeable sheet material, such as GB.A-706624 shows. It is further characterised in that the sheet material comprises a first band permanently fixed to the mouth end of the smoking article and a second band abutting the first band and movable on the smoking article relative to the said peripheral area to admit varying amounts of air to the mouth end region to dilute the smoke therein.
  • the assembly comprises a tobacco rod, an integral, axially aligned, wrapped filter plug and two circumscribing layers of tipping paper.
  • the filter is wrapped in an air permeable plug wrap.
  • the tobacco rod and filter plug are joined together by a first circumscribing layer of air permeable tipping paper which extends from the mouth end of the filter plug to a position on the tobacco rod adjacent the rod end of the filter plug.
  • the second layer of tipping paper is air impermeable, circumscribes the first layer of tipping paper, and extends from the mouth end of the filter to the rod end of the first layer of tipping paper.
  • the second layer has a circumferentially extending row of closely spaced perforations intermediate its two ends.
  • the mouth end portion of the second layer is attached to the underlying first layer of tipping paper.
  • the rod end portion of the second layer is freed by rotating this portion about the axis of the cigarette to break the perforations, thus forming a sleeve which can move axially between the mouth end portion of the second layer and positions along the tobacco rod.
  • the mouth end portion of the second layer prevents the sleeve from being removed from the mouth end of the cigarette.
  • a cigarette comprises a tobacco rod 201 which is axially aligned with and joined in end-to-end abutting relation to a conventional, substantially cylindrical filter plug 202, which may be a cellulose acetate filter or the like.
  • the filter plug is wrapped in an air permeable plug wrap 203.
  • the wrapped filter plug is joined to the tobacco rod 201 by a circumscribing first layer of tipping paper 204 which extends from the mouth end of the filter plug to a position on the tobacco rod adjacent the rod end of the filter plug.
  • Tipping paper 204 is air permeable and is attached, preferably by a circumferentially extending band of adhesive on its inner surface, to the outer surfaces of the tobacco rod and the filter plug wrap with the band centered on either side of their line of abutment 205.
  • a second layer of tipping paper 206 circumscribes the first layer of tipping paper and extends from the mouth end of the filter substantially to the rod end of the filter.
  • This second layer is divided into a mouth end sleeve 207 and a rod end sleeve 208 by a circumferentially extending row of closely spaced perforations 210.
  • the mouth end sleeve 207 is attached to the tipping paper 204 adjacent the mouth end, preferably by a band of adhesive 209 on its inner surface.
  • the rod end sleeve 208 is not attached to the underlying layer of tipping paper 204.
  • the second layer of tipping paper 206 is substantially air impermeable and the rod end sleeve 208 is detachable along the line of perforations 210.
  • the cigarette has a set of air dilution values which, if the smoker prefers, can be varied by rotating the rod end sleeve 208 to detach it from the mouth end sleeve 207 and then axially moving sleeve 208 towards the coal end of the tobacco rod, thereby exposing the underlying air permeable tipping paper 204.
  • This axial movement permits varying degrees of air to enter the filter, thereby diluting the smoke and changing the air dilution value of the cigarette.
  • This axially slidable sleeve 208 is retained against removal from the mouth end of the cigarette by the attached mouth end sleeve 207.
  • the plug wrap and the first layer of tipping paper may also be substantially air impermeable and may contain a plurality of openings therethrough which are exposed when the sleeve 208 is detached and moved axially towards the coal end of the cigarette.
  • the filter cigarette of the present invention may be readily produced on conventional cigarette making equipment and apparatus with a minimum of modifications. Forming and cutting the cigarette rod and the filter plug to length are done conventionally. Also, bringing the filter plug into axial alignment with the cigarette rod and the overwrapping with the first layer of tipping paper is accomplished in the same manner as in conventional cigarettes except that the adhesive applicator is adapted to provide only a band of adhesive on the portion of the first layer of tipping paper which overlaps and joins the plug wrap to the tobacco rod. The same machine for applying the first layer of tipping paper with the glue applicator adapted to provide a band of glue corresponding to the mouth end sleeve portion of the second layer of tipping paper.
  • the row of perforations in the second layer of tipping paper may be made, preferably prior to application, by any conventional means such as laser perforation, electrostatic perforation, or mechanical perforation using points or knives. It is preferred to employ a laser perforation device in order to make the perforations extremely small.
  • the tipping paper is fed through a perforating zone where it is exposed to a laser light beam focused laterally of the width of the travelling tipping paper so as to define the desired width of the detachable sleeve portion of the second layer of tipping paper.
  • the power settings and focusing of the laser beam and the rate of feed of the tipping paper are selected so as to all but part of the paper along the "break away" line 210 shown in Figs. 1 and 2.
  • the attachment which rains is selected to retain enough strength to hold the sleeves together during assembly but permits the detachable sleeve to be readily detached by the smoker without tearing the tipping paper other than between the perforations.
  • a laser system is employed to make about 40 perforations per centimetre (about 100 perforations per inch) in the paper along the line 210.

Landscapes

  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)
  • Manufacturing Of Cigar And Cigarette Tobacco (AREA)
  • Adornments (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Vending Machines For Individual Products (AREA)
  • Processes Of Treating Macromolecular Substances (AREA)

Abstract

A cigarette is provided which comprises a wrapped filter plug 202,203 aligned in end-to-end abutting relationship with a substantially cylindrical tobacco rod 201. The filter plug and tobacco rod are circumscribed and joined by a substantially air permeable first layer of tipping paper 204. Circumscribing the first layer of tipping paper is a second layer of substantially air impermeable tipping paper 206. The second layer has a circumferentially extending row of closely spaced perforations 210 intermediate the two ends of the second layer which divides it into a mouth-end sleeve 207 attached to the first layer at the mouth end of the cigarette and a second rod-end sleeve 208 detachable from the mouth end sleeve by rotating the sleeve relative to the first sleeve so that it can move axially between the mouth-end sleeve and positions along the tobacco rod allowing air to enter the filter through the exposed portions of the air permeable layers.

Description

  • The present invention relates to cigarettes. More particularly, the present invention relates to cigarettes which are adjustable to provide a wide range of air dilution values.
  • Various mechanisms have been disclosed in heretofore issued patents which provide for adjustment of the air dilution value of a filter cigarette, but these mechanisms are not without certain disadvantages. While many complicated mechanisms have been disclosed, the simpler mechanisms generally involve making one or more openings through a substantially air impermeable filter plug wrap and the overlying, substantially air impermeable, tipping paper and one or more corresponding openings in a sleeve which is placed over the tipping paper and which is then either rotated or moved axially to select the degree to which the two sets of openings are in registry. In another embodiment found in the art, the filter is not glued to the tipping paper and thus may be moved axially within the cylinder formed by the tipping paper. Openings are made in the filter plug wrap and corresponding openings are made in the tipping paper. The air dilution value is adjusted by axially moving the filter plug within the tipping paper to adjust the degree to which the two sets of openings are in registry.
  • Among the problems associated with such mechanisms are that the sleeve or filter plug may be removed from the cigarette by the smoker and not readily replaced, and that when dilution is desired, thus requiring some degree of registry between the two sets of openings, this registry may be inadvertently destroyed by a slight axial movement of the sleeve or plug. Accordingly, the dilution, once set by the smoker, is not ensured of any degree of consistency. Yet another problem associated with a number of these prior devices is that they have not been readily adaptable to a high rate of production on cigarette making machinery of conventional design.
  • US-A-3 359 988 discloses a filter cigarette, the filter of which is divided longitudinally into two channels, one uniquely for air and the other uniquely for smoke. Ingress of air to the air channel is controlled by movement of a circumferential band around the filter, the band having a hole in it which is moved into and out of registry with holes in the external wall of the air channel.
  • Another solution to this problem is the subject of European Patent Application No. 83 304 257 (published no. EP-A-0 100 215), from which this application has been divided.
  • In accordance with the present invention there is provided a smoking article comprising a rod of combustible smoking material and a mouth end region open to permit the passage of air and smoke, the mouth end region having a peripheral area thereof adapted for the passage of air therethrough, and being circumscribed by a substantially air impermeable sheet material, such as GB.A-706624 shows. It is further characterised in that the sheet material comprises a first band permanently fixed to the mouth end of the smoking article and a second band abutting the first band and movable on the smoking article relative to the said peripheral area to admit varying amounts of air to the mouth end region to dilute the smoke therein.
  • In a preferred embodiment of the invention, the assembly comprises a tobacco rod, an integral, axially aligned, wrapped filter plug and two circumscribing layers of tipping paper. The filter is wrapped in an air permeable plug wrap. The tobacco rod and filter plug are joined together by a first circumscribing layer of air permeable tipping paper which extends from the mouth end of the filter plug to a position on the tobacco rod adjacent the rod end of the filter plug. The second layer of tipping paper is air impermeable, circumscribes the first layer of tipping paper, and extends from the mouth end of the filter to the rod end of the first layer of tipping paper. The second layer has a circumferentially extending row of closely spaced perforations intermediate its two ends. The mouth end portion of the second layer is attached to the underlying first layer of tipping paper. The rod end portion of the second layer is freed by rotating this portion about the axis of the cigarette to break the perforations, thus forming a sleeve which can move axially between the mouth end portion of the second layer and positions along the tobacco rod. The mouth end portion of the second layer prevents the sleeve from being removed from the mouth end of the cigarette.
  • The cigarettes of the present invention may be manufactured employing conventional equipment with only minor modifications and a method of manufacturing such cigarettes forms another aspect of the present invention. The invention will be further described, by way of example, with reference to the drawings, in which:
    • Fig. 1 is an enlarged partially fragmentary perspective view, taken from the mouth end, of a filter cigarette according to a preferred embodiment of the present invention;
    • Fig. 2 is an enlarged perspective view, taken from the mouth end, of the assembled cigarette of Fig. 1; and
    • Fig. 3 is a perspective view, also taken from the mouth end, of a filter cigarette of Figs. 1 and 2 showing the axially movable band detached form the mouth end band.
  • As shown in Figs. 1, 2 and 3, according to a preferred embodiment of the invention a cigarette comprises a tobacco rod 201 which is axially aligned with and joined in end-to-end abutting relation to a conventional, substantially cylindrical filter plug 202, which may be a cellulose acetate filter or the like. The filter plug is wrapped in an air permeable plug wrap 203. The wrapped filter plug is joined to the tobacco rod 201 by a circumscribing first layer of tipping paper 204 which extends from the mouth end of the filter plug to a position on the tobacco rod adjacent the rod end of the filter plug. Tipping paper 204 is air permeable and is attached, preferably by a circumferentially extending band of adhesive on its inner surface, to the outer surfaces of the tobacco rod and the filter plug wrap with the band centered on either side of their line of abutment 205.
  • A second layer of tipping paper 206 circumscribes the first layer of tipping paper and extends from the mouth end of the filter substantially to the rod end of the filter. This second layer is divided into a mouth end sleeve 207 and a rod end sleeve 208 by a circumferentially extending row of closely spaced perforations 210. The mouth end sleeve 207 is attached to the tipping paper 204 adjacent the mouth end, preferably by a band of adhesive 209 on its inner surface. The rod end sleeve 208 is not attached to the underlying layer of tipping paper 204.
  • The second layer of tipping paper 206 is substantially air impermeable and the rod end sleeve 208 is detachable along the line of perforations 210. In its attached form, the cigarette has a set of air dilution values which, if the smoker prefers, can be varied by rotating the rod end sleeve 208 to detach it from the mouth end sleeve 207 and then axially moving sleeve 208 towards the coal end of the tobacco rod, thereby exposing the underlying air permeable tipping paper 204. This axial movement permits varying degrees of air to enter the filter, thereby diluting the smoke and changing the air dilution value of the cigarette. This axially slidable sleeve 208 is retained against removal from the mouth end of the cigarette by the attached mouth end sleeve 207.
  • In an alternative embodiment, the plug wrap and the first layer of tipping paper may also be substantially air impermeable and may contain a plurality of openings therethrough which are exposed when the sleeve 208 is detached and moved axially towards the coal end of the cigarette.
  • The filter cigarette of the present invention may be readily produced on conventional cigarette making equipment and apparatus with a minimum of modifications. Forming and cutting the cigarette rod and the filter plug to length are done conventionally. Also, bringing the filter plug into axial alignment with the cigarette rod and the overwrapping with the first layer of tipping paper is accomplished in the same manner as in conventional cigarettes except that the adhesive applicator is adapted to provide only a band of adhesive on the portion of the first layer of tipping paper which overlaps and joins the plug wrap to the tobacco rod. The same machine for applying the first layer of tipping paper with the glue applicator adapted to provide a band of glue corresponding to the mouth end sleeve portion of the second layer of tipping paper.
  • The row of perforations in the second layer of tipping paper may be made, preferably prior to application, by any conventional means such as laser perforation, electrostatic perforation, or mechanical perforation using points or knives. It is preferred to employ a laser perforation device in order to make the perforations extremely small. In practice, the tipping paper is fed through a perforating zone where it is exposed to a laser light beam focused laterally of the width of the travelling tipping paper so as to define the desired width of the detachable sleeve portion of the second layer of tipping paper. The power settings and focusing of the laser beam and the rate of feed of the tipping paper are selected so as to all but part of the paper along the "break away" line 210 shown in Figs. 1 and 2. The attachment which rains is selected to retain enough strength to hold the sleeves together during assembly but permits the detachable sleeve to be readily detached by the smoker without tearing the tipping paper other than between the perforations. Preferably, a laser system is employed to make about 40 perforations per centimetre (about 100 perforations per inch) in the paper along the line 210.

Claims (2)

  1. A smoking article comprising a rod of combustible smoking material (201) and a mouth end region open to permit the passage of air and smoke, the mouth end region having a peripheral area thereof adapted for the passage of air therethrough, and being circumscribed by a substantially air impermeable sheet material (206) characterised in that the sheet material comprises a first band (207) permanently fixed to the mouth end of the smoking article and a second band (208) abutting the first band and movable on the smoking article relative to the said peripheral area to admit varying amounts of air to the mouth end region to dilute the smoke therein.
  2. A smoking article according to claim 1, further characterised in that the mouth end region comprises a filter plug (202) abutting the said rod (201), the filter plug being circumscribed by a substantially air permeable wrapping (203), a first, substantially air permeable tipping paper (204) and a second substantially air impermeable tipping paper (206), the first tipping paper extending from the mouth end of the filter plug to a position on the rod adjacent the rod end of the filter plug, and the second tipping paper extending substantially from the mouth end to the rod end of the filter, the second tipping paper being divided into a mouth end sleeve (207) fixed to the first tipping paper and a rod end sleeve (208) axially movable over the first tipping paper to expose a varying extent of the air permeable first tipping paper.
EP87201198A 1982-07-23 1983-07-22 Cigarettes Expired - Lifetime EP0247702B1 (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
AT87201198T ATE87185T1 (en) 1982-07-23 1983-07-22 CIGARETTES.

Applications Claiming Priority (6)

Application Number Priority Date Filing Date Title
US40138082A 1982-07-23 1982-07-23
US42939382A 1982-09-30 1982-09-30
US42935482A 1982-09-30 1982-09-30
US429393 1982-09-30
US429354 1982-09-30
US401380 1999-09-22

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
EP83304257.5 Division 1983-07-22

Publications (3)

Publication Number Publication Date
EP0247702A2 EP0247702A2 (en) 1987-12-02
EP0247702A3 EP0247702A3 (en) 1988-12-21
EP0247702B1 true EP0247702B1 (en) 1993-03-24

Family

ID=27410451

Family Applications (2)

Application Number Title Priority Date Filing Date
EP87201198A Expired - Lifetime EP0247702B1 (en) 1982-07-23 1983-07-22 Cigarettes
EP83304257A Expired EP0100215B1 (en) 1982-07-23 1983-07-22 Cigarettes and methods of manufacture

Family Applications After (1)

Application Number Title Priority Date Filing Date
EP83304257A Expired EP0100215B1 (en) 1982-07-23 1983-07-22 Cigarettes and methods of manufacture

Country Status (7)

Country Link
EP (2) EP0247702B1 (en)
JP (2) JPS59501443A (en)
AT (1) ATE38465T1 (en)
AU (1) AU559188B2 (en)
CA (1) CA1210297A (en)
DE (2) DE3378400D1 (en)
WO (1) WO1984000478A1 (en)

Families Citing this family (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4648413A (en) * 1984-03-07 1987-03-10 Saintsing Barry L Adjustable-delivery cigarette
US4576187A (en) * 1984-10-22 1986-03-18 R. J. Reynolds Tobacco Company Variable air dilution cigarette filter
US4817638A (en) * 1985-08-01 1989-04-04 Philip Morris Incorporated Apparatus for adjusting a cigarette having variable smoking characteristics
GB8531659D0 (en) * 1985-12-23 1986-02-05 British American Tobacco Co Smoking articles
GB9400985D0 (en) * 1994-01-19 1994-03-16 Rothmans International Ltd Filtered smoking article
EP1754419A1 (en) * 2005-08-15 2007-02-21 Philip Morris Products S.A. Liquid release device for a smoking article
US7789089B2 (en) * 2006-08-04 2010-09-07 R. J. Reynolds Tobacco Company Filtered cigarette possessing tipping material
CN101016709B (en) * 2007-02-15 2010-05-19 云南瑞升烟草技术(集团)有限公司 Fast adjusting tipping paper
GB0724408D0 (en) * 2007-12-14 2008-01-30 British American Tobacco Co Recessed ventilation for smoking articles
EP2368448A1 (en) * 2010-03-26 2011-09-28 Philip Morris Products S.A. Smoking article with variable ventilation
GB201104232D0 (en) 2011-03-14 2011-04-27 British American Tobacco Co Smoking article and method of manufacturing a smoking article
GB201116629D0 (en) * 2011-09-27 2011-11-09 British American Tobacco Co Smoking articles and methods of manufacturing smoking articles
GB201217894D0 (en) * 2012-10-05 2012-11-21 British American Tobacco Co A smoking article
ITBO20120585A1 (en) 2012-10-26 2014-04-27 Gd Spa MACHINE FOR REALIZING CIGARETTES WITH ADJUSTABLE VENTILATION.
ITBO20120584A1 (en) 2012-10-26 2014-04-27 Gd Spa MACHINE FOR REALIZING CIGARETTES WITH ADJUSTABLE VENTILATION.
JP6283697B2 (en) * 2013-03-13 2018-02-21 ジェイティー インターナショナル エス.エイ. Cigarette with variable airflow filter
KR101819814B1 (en) * 2013-07-03 2018-01-17 니뽄 다바코 산교 가부시키가이샤 Filter for cigarette and cigarette with filter
WO2015014610A1 (en) * 2013-07-29 2015-02-05 Jt International Sa Filter element for a smoking article
JP6103676B2 (en) * 2014-03-28 2017-03-29 日本たばこ産業株式会社 Filter cigarette manufacturing machine, manufacturing method thereof, and filter cigarette

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB706624A (en) * 1949-12-06 1954-03-31 Elie Prodromos Aghnides Improvements in or relating to cigarettes
US3359988A (en) * 1965-04-21 1967-12-26 Osborne M Thomson Filter cigarette
US3428050A (en) * 1967-02-21 1969-02-18 Walter R Kandel Filter cigarette of adjustable filter capacity
US3503406A (en) * 1968-10-28 1970-03-31 Lawrence Murry Riegel Cigarettes
US3512537A (en) * 1968-11-27 1970-05-19 U S Remedy Corp Adjustable aerated cigarette
CA913486A (en) * 1970-05-25 1972-10-31 Plourde Jacques Selective air dosing means for cigarettes
US3695274A (en) * 1970-11-30 1972-10-03 Brown & Williamson Tobacco Piston type cigarette filter
GB1400278A (en) * 1972-06-06 1975-07-16 British American Tobacco Co Smoking articles
US4232574A (en) * 1977-08-19 1980-11-11 Liggett Group Inc. Apparatus and method for providing a cigarette filter with an aeration groove
US4340074A (en) * 1979-11-07 1982-07-20 Brown & Williamson Tobacco Corporation Cigarette material having non-lipsticking properties
JPS59501813A (en) * 1982-09-30 1984-11-01 フィリップ・モーリス・プロダクツ・インコーポレイテッド Adjustable filter cigarette and its manufacturing method

Also Published As

Publication number Publication date
AU559188B2 (en) 1987-02-26
JPH01273575A (en) 1989-11-01
EP0247702A2 (en) 1987-12-02
DE100215T1 (en) 1984-09-27
AU1725983A (en) 1984-02-16
EP0100215A3 (en) 1985-10-09
EP0100215A2 (en) 1984-02-08
DE3378400D1 (en) 1988-12-15
WO1984000478A1 (en) 1984-02-16
ATE38465T1 (en) 1988-11-15
JPH0228318B2 (en) 1990-06-22
EP0247702A3 (en) 1988-12-21
EP0100215B1 (en) 1988-11-09
CA1210297A (en) 1986-08-26
JPS59501443A (en) 1984-08-16
JPH0262228B2 (en) 1990-12-25

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