EP0217568A2 - Vorrichtung zur Behandlung von Flüssigkeiten - Google Patents

Vorrichtung zur Behandlung von Flüssigkeiten Download PDF

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Publication number
EP0217568A2
EP0217568A2 EP86306956A EP86306956A EP0217568A2 EP 0217568 A2 EP0217568 A2 EP 0217568A2 EP 86306956 A EP86306956 A EP 86306956A EP 86306956 A EP86306956 A EP 86306956A EP 0217568 A2 EP0217568 A2 EP 0217568A2
Authority
EP
European Patent Office
Prior art keywords
module
housing
tubes
liquid
outlet port
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP86306956A
Other languages
English (en)
French (fr)
Other versions
EP0217568B1 (de
EP0217568A3 (en
Inventor
Richard Guy Gutman
Gwilym Handel Williams
Dennis Wood
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Sellafield Ltd
Original Assignee
British Nuclear Fuels PLC
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by British Nuclear Fuels PLC filed Critical British Nuclear Fuels PLC
Publication of EP0217568A2 publication Critical patent/EP0217568A2/de
Publication of EP0217568A3 publication Critical patent/EP0217568A3/en
Application granted granted Critical
Publication of EP0217568B1 publication Critical patent/EP0217568B1/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

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Classifications

    • GPHYSICS
    • G21NUCLEAR PHYSICS; NUCLEAR ENGINEERING
    • G21FPROTECTION AGAINST X-RADIATION, GAMMA RADIATION, CORPUSCULAR RADIATION OR PARTICLE BOMBARDMENT; TREATING RADIOACTIVELY CONTAMINATED MATERIAL; DECONTAMINATION ARRANGEMENTS THEREFOR
    • G21F9/00Treating radioactively contaminated material; Decontamination arrangements therefor
    • G21F9/04Treating liquids
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/11Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with bag, cage, hose, tube, sleeve or like filtering elements
    • B01D29/31Self-supporting filtering elements
    • B01D29/35Self-supporting filtering elements arranged for outward flow filtration
    • B01D29/356Self-supporting filtering elements arranged for outward flow filtration open-ended, the arrival of the mixture to be filtered and the discharge of the concentrated mixture are situated on both opposite sides of the filtering element
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D29/00Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor
    • B01D29/50Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition
    • B01D29/52Filters with filtering elements stationary during filtration, e.g. pressure or suction filters, not covered by groups B01D24/00 - B01D27/00; Filtering elements therefor with multiple filtering elements, characterised by their mutual disposition in parallel connection
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D63/00Apparatus in general for separation processes using semi-permeable membranes
    • B01D63/06Tubular membrane modules
    • B01D63/069Tubular membrane modules comprising a bundle of tubular membranes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2201/00Details relating to filtering apparatus
    • B01D2201/04Supports for the filtering elements
    • B01D2201/0407Perforated supports on both sides of the filtering element
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2201/00Details relating to filtering apparatus
    • B01D2201/04Supports for the filtering elements
    • B01D2201/0469Filter tubes connected to collector tubes
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2201/00Details relating to filtering apparatus
    • B01D2201/28Position of the filtering element
    • B01D2201/287Filtering elements with a vertical or inclined rotation or symmetry axis

Definitions

  • This invention relates to liquid treatment apparatus comprising one or more ducts through which a liquid is to be passed, each duct having a wall permeable to at least a component of the liquid, and particularly but not exclusively to ultrafiltration apparatus.
  • a known ultrafiltration apparatus described in British patent GB 1 468 928 (Union Carbide Corp.), comprises a plurality of parallel tubes arranged so that a liquid to be treated passes under pressure axially through the tubes.
  • the tubes are porous and permeable, being composed of bonded carbon particles and an essentially continuous coating of metal oxide particles on the inside surface of the tubes.
  • some of the liquid and low molecular weight dissolved phases pass through the walls of the tubes, while most of the higher molecular weight dissolved phases and any particulate matter are carried through the tubes in the liquid concentrate.
  • Such an apparatus may be used to separate pure water from an oil/water or oil/water/dirt emulsion. Equally it may be used to remove water from a sludge of particulate matter and water. For example it might be used to dewater a sludge containing low-level radioactive material, before immobilizing the sludge by the addition of cement.
  • known types of ultrafiltration apparatus are not suitable for use in situations where installation and removal of the apparatus must be performed remotely, or where the apparatus itself must be located within a shielded enclosure providing very limited access.
  • a liquid treatment apparatus comprising: a housing open at one end and defining at the other end an inlet port and an outlet port for a liquid undergoing treatment, and also defining an outlet port for a permeate liquid; a module insertable into the housing and comprising a plurality of parallel tubes, each tube having a wall permeable to at least a component of the liquid undergoing treatment, and means so that on insertion into the housing the module comes into sealing engagement with the inlet port and the outlet port, the tubes providing at least part of a path for the liquid undergoing treatment from the inlet port to the outlet port; and means for clamping the module to the housing at the open end of the housing.
  • the apparatus of the invention can readily be installed or dismantled remotely, as access to only one end of the housing (the open end) is needed, and furthermore the apparatus can be installed within a shielded enclosure with only the open end of the housing extending through a wall of the enclosure.
  • the module includes two header chambers at the insertable end of the module, one of which comes into communication with the inlet port and the other of which comes into communication with the outlet port on insertion of the module, each tube communicating with either one or other of the two header chambers at the insertable end, and a single header chamber at the other end of the module with which all the tubes communicate.
  • an ultrafiltration apparatus 10 for dewatering a radioactive sludge, the apparatus 10 being installed within a shielded enclosure 11.
  • the apparatus 10 includes a steel housing 12 of generally cylindrical shape with its longitudinal axis vertical, open at its top end and with an external flange 13 around the open end by which the housing 12 is supported through a hole in the roof 14 of the enclosure 11.
  • a lid 15 with a matching flange 16 covers the open end of the housing 12, and is clamped to it by bolts 17.
  • Near the top of the housing 12 is an outlet duct 18 for permeate water to leave the housing 12, while at the bottom of the housing 12 are an inlet port 20 and an outlet port 21 for the sludge to be treated.
  • the module 24 consists of a lower assembly 25, an upper assembly 26, two semicircular arrays of parallel ultrafiltration tubes 28 which extend between the lower assembly 25 and the upper assembly 26, and a perforated cylindrical protective steel sleeve 29 surrounding all the tubes 28. Only three tubes 28 of each array are shown.
  • Each tube 28 is of bonded carbon particles with an essentially continuous coating of metal oxide particles on its inside surface, the permeability being such that with a pressure difference of several atmospheres (for example 700 kPa) water from the sludge is caused to pass through the walls of the tubes 28.
  • the sludge flows upwardly in the tubes 28 of one array and flows back down in the tubes 28 of the other array.
  • the lower assembly 25 includes a lower portion 29 which defines two projecting stub pipes 30 and 31 which mate with the sludge inlet port 20 and outlet port 21 in the housing 12 respectively, O-rings 32 providing a leak-proof seal.
  • the stub pipes 30 and 31 open out into two semicircular headers, 34 and 35 respectively, separated by a diametral wall 36.
  • the tubes 28 are sealingly connected to the lower assembly 25 through corresponding holes 37 in a flat plate 38.
  • the seal is provided by a rubber gasket 40 (shown in Figure 2) sandwiched between the lower face of the flat plate 38 and two semicircular perforated sheets 41, one in each header 34 and 35.
  • the flat plate 38 is held to the lower portion 29 by bolts 42, and forms the top of the headers 34 and 35, so that each tube 28 communicates with either one or the other of the headers 34 and 35.
  • the gasket 40 also defines collars 44 which fit around the open ends of the tubes 28, between each tube 28 and the wall of the corresponding hole 37.
  • the perforated sheets 41 are clamped to the flat plate 38 by bolts 45, and the holes through the sheets 41 align with those through the plate 38.
  • the gasket 40 also provides a seal between the wall 36 and the plate 38.
  • the upper assembly 26 comprises a flat plate 48 and a cap portion 49, held together by bolts 50, and together defining a common header 52 for all the tubes 28.
  • the tubes 28 are sealingly connected to the upper assembly 26 through corresponding holes in the plate 48, the seal being provided in a similar way to that described above by a rubber gasket (not shown) sandwiched between the upper face of the plate 48 and a thin perforated sheet 54, the gasket also defining a collar (not shown) around the top end of each tube 28.
  • the cap portion 49 is provided with a bracket 55 so that the assembled module 24 can be inserted into or lifted out of the housing 12, after removal of the lid 15.
  • the flat plate 48 is of greater diameter than the rest of the module 24, and has a number of peripheral unthreaded holes through which bolts 56 can be inserted to engage in threaded holes in an internal flange 58 on the housing 12, so as to clamp the module 24 into the housing 12.
  • a radioactive sludge is pumped into the inlet port 20 at a pressure of for example 500 kPa, and flows through the module 24, passing into the header 34, up one array of tubes 28 to the header 52, back down the other array of tubes 28 to the header 35, and so out of the outlet port 21.
  • the emerging sludge is more concentrated than the inflowing sludge, as during its passage through the tubes 28 some of the water passes through the permeable walls of the tubes 28 into the housing 12, to flow out of the outlet duct 18, where the pressure is typically about atmospheric.
  • module 24 has two semicircular arrays of tubes 28 and two semicircular headers 34 and 35'in the lower assembly 25, an alternative module might have differently shaped arrays of tubes 28 and so differently shaped headers.
  • a module (not shown) might have a central circular header and a concentric annular header.
  • a module might incorporate sealing means other than the O-rings 32 described above for sealing the sludge inlet and outlet ports of the housing to the module, as long as the seals can withstand a pressure difference of several atmospheres.
  • the bolts 56 enable the force with which the module 24 is urged into engagement with the sludge inlet and outlet ports to be adjusted.

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Engineering & Computer Science (AREA)
  • General Engineering & Computer Science (AREA)
  • High Energy & Nuclear Physics (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)
EP86306956A 1985-09-24 1986-09-10 Vorrichtung zur Behandlung von Flüssigkeiten Expired - Lifetime EP0217568B1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
GB8523549 1985-09-24
GB858523549A GB8523549D0 (en) 1985-09-24 1985-09-24 Liquid treatment apparatus

Publications (3)

Publication Number Publication Date
EP0217568A2 true EP0217568A2 (de) 1987-04-08
EP0217568A3 EP0217568A3 (en) 1987-06-16
EP0217568B1 EP0217568B1 (de) 1990-03-21

Family

ID=10585644

Family Applications (1)

Application Number Title Priority Date Filing Date
EP86306956A Expired - Lifetime EP0217568B1 (de) 1985-09-24 1986-09-10 Vorrichtung zur Behandlung von Flüssigkeiten

Country Status (4)

Country Link
EP (1) EP0217568B1 (de)
JP (1) JP2593853B2 (de)
DE (1) DE3669664D1 (de)
GB (3) GB8523549D0 (de)

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0343895A2 (de) * 1988-05-27 1989-11-29 Zenon Environmental Inc. Röhrenmembranmodul
WO1995022397A1 (en) * 1994-02-21 1995-08-24 Peter Stubtoft Assembly for processing an aqueous fluid by reverse osmosis
WO1998036824A1 (de) * 1997-02-21 1998-08-27 Nunner Gmbh Vorrichtung zur querstromfiltration von flüssigkeiten
WO2001096003A1 (fr) * 2000-06-14 2001-12-20 Societe Industrielle De La Vallee De L'aigues S.I.V.A. Dispositif de filtration integrant une boucle de circulation
EP1302227A1 (de) * 2001-10-11 2003-04-16 Filtrox AG Filtrationseinheit
EP1302228A1 (de) * 2001-10-11 2003-04-16 Filtrox AG Filtrationseinheit
CN1907536B (zh) * 2005-07-29 2010-08-18 山谷水工业公司 包括回路与循环泵的过滤装置
US8240482B2 (en) 2006-07-17 2012-08-14 Societe Industrielle De La Vallee De L'aigues S.I.V.A. Tangential filtration device

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0732866B2 (ja) * 1992-03-30 1995-04-12 株式会社クボタ 濾過膜モジュール
JP2011131148A (ja) * 2009-12-24 2011-07-07 Kyocera Corp 分離膜装置

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1259400A (fr) * 1960-03-01 1961-04-28 Commissariat Energie Atomique Dispositif démontable pour la filtration ou le traitement de fluides radioactifs
US3722694A (en) * 1970-06-10 1973-03-27 Romicon Inc Filtration device
FR2234912A1 (de) * 1973-06-27 1975-01-24 Rhone Poulenc Sa
FR2407012A1 (fr) * 1977-10-27 1979-05-25 Wafilin Bv Appareil pour filtration sur membrane assurant une meilleure elimination des sels
EP0203862A1 (de) * 1985-05-29 1986-12-03 Framatome Ultrafiltrationsvorrichtung für eine unter Druck stehende Flüssigkeit bei hoher Temperatur

Family Cites Families (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5348853Y2 (de) * 1975-02-25 1978-11-22
JPS5811362Y2 (ja) * 1980-10-30 1983-03-03 日東電工株式会社 管状膜分離装置

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR1259400A (fr) * 1960-03-01 1961-04-28 Commissariat Energie Atomique Dispositif démontable pour la filtration ou le traitement de fluides radioactifs
US3722694A (en) * 1970-06-10 1973-03-27 Romicon Inc Filtration device
FR2234912A1 (de) * 1973-06-27 1975-01-24 Rhone Poulenc Sa
FR2407012A1 (fr) * 1977-10-27 1979-05-25 Wafilin Bv Appareil pour filtration sur membrane assurant une meilleure elimination des sels
EP0203862A1 (de) * 1985-05-29 1986-12-03 Framatome Ultrafiltrationsvorrichtung für eine unter Druck stehende Flüssigkeit bei hoher Temperatur

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0343895A2 (de) * 1988-05-27 1989-11-29 Zenon Environmental Inc. Röhrenmembranmodul
EP0343895A3 (en) * 1988-05-27 1990-01-31 Zenon Environmental Inc. Tubular membrane module
AU618597B2 (en) * 1988-05-27 1992-01-02 Zenon Environmental Inc. Tubular module
WO1995022397A1 (en) * 1994-02-21 1995-08-24 Peter Stubtoft Assembly for processing an aqueous fluid by reverse osmosis
WO1998036824A1 (de) * 1997-02-21 1998-08-27 Nunner Gmbh Vorrichtung zur querstromfiltration von flüssigkeiten
WO2001096003A1 (fr) * 2000-06-14 2001-12-20 Societe Industrielle De La Vallee De L'aigues S.I.V.A. Dispositif de filtration integrant une boucle de circulation
FR2810256A1 (fr) * 2000-06-14 2001-12-21 Vallee De L Aigues S I V A Soc Dispositif de filtration integrant une boucle de circulation
US7192522B2 (en) 2000-06-14 2007-03-20 Societe Industrielle De La Vallee De L'aigues S.I.V.A. Filtering device incorporating a circulation loop
EP1302227A1 (de) * 2001-10-11 2003-04-16 Filtrox AG Filtrationseinheit
EP1302228A1 (de) * 2001-10-11 2003-04-16 Filtrox AG Filtrationseinheit
CN1907536B (zh) * 2005-07-29 2010-08-18 山谷水工业公司 包括回路与循环泵的过滤装置
US8240482B2 (en) 2006-07-17 2012-08-14 Societe Industrielle De La Vallee De L'aigues S.I.V.A. Tangential filtration device

Also Published As

Publication number Publication date
GB8621813D0 (en) 1986-10-15
JP2593853B2 (ja) 1997-03-26
GB2180775B (en) 1989-01-05
GB8527639D0 (en) 1985-12-11
DE3669664D1 (de) 1990-04-26
GB2180775A (en) 1987-04-08
GB8523549D0 (en) 1985-10-30
EP0217568B1 (de) 1990-03-21
JPS6271504A (ja) 1987-04-02
EP0217568A3 (en) 1987-06-16

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