EP0184740A3 - Process for the preparation of methyl esters of fatty acids - Google Patents

Process for the preparation of methyl esters of fatty acids Download PDF

Info

Publication number: EP0184740A3
Authority: EP; European Patent Office
Prior art keywords: fatty acids; methanol; oil phase; alkanol; reaction
Prior art date: 1984-12-08
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.): Granted

Application number

EP85115217A

Other languages

English (en)

Other versions

EP0184740A2 (de

EP0184740B1 (de

Inventor

Herbert Dr. Lepper

Lothar Friesenhagen

Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)

Henkel AG and Co KGaA

Original Assignee

Henkel AG and Co KGaA

Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)

1984-12-08

Filing date

1985-11-30

Publication date

1987-09-09

1985-11-30 Application filed by Henkel AG and Co KGaA filed Critical Henkel AG and Co KGaA

1985-11-30 Priority to AT85115217T priority Critical patent/ATE61332T1/de

1986-06-18 Publication of EP0184740A2 publication Critical patent/EP0184740A2/de

1987-09-09 Publication of EP0184740A3 publication Critical patent/EP0184740A3/de

1991-03-06 Application granted granted Critical

1991-03-06 Publication of EP0184740B1 publication Critical patent/EP0184740B1/de

2005-11-30 Anticipated expiration legal-status Critical

Status Expired - Lifetime legal-status Critical Current

Links

Classifications

- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/003—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fatty acids with alcohols
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11C—FATTY ACIDS FROM FATS, OILS OR WAXES; CANDLES; FATS, OILS OR FATTY ACIDS BY CHEMICAL MODIFICATION OF FATS, OILS, OR FATTY ACIDS OBTAINED THEREFROM
- C11C3/00—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom
- C11C3/04—Fats, oils, or fatty acids by chemical modification of fats, oils, or fatty acids obtained therefrom by esterification of fats or fatty oils

Landscapes

Chemical & Material Sciences (AREA)
General Chemical & Material Sciences (AREA)
Life Sciences & Earth Sciences (AREA)
Engineering & Computer Science (AREA)
Chemical Kinetics & Catalysis (AREA)
Oil, Petroleum & Natural Gas (AREA)
Wood Science & Technology (AREA)
Organic Chemistry (AREA)
Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Fats And Perfumes (AREA)
Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Hydrogenated Pyridines (AREA)

EP85115217A 1984-12-08 1985-11-30 Verfahren zur Herstellung von Fettsäuremethylestern Expired - Lifetime EP0184740B1 (de)

Priority Applications (1)

Application Number	Priority Date	Filing Date	Title
AT85115217T ATE61332T1 (de)	1984-12-08	1985-11-30	Verfahren zur herstellung von fettsaeuremethylestern.

Applications Claiming Priority (2)

Application Number	Priority Date	Filing Date	Title
DE19843444893 DE3444893A1 (de)	1984-12-08	1984-12-08	Verfahren zur herstellung von fettsaeuremethylestern
DE3444893		1984-12-08

Publications (3)

Publication Number	Publication Date
EP0184740A2 EP0184740A2 (de)	1986-06-18
EP0184740A3 true EP0184740A3 (en)	1987-09-09
EP0184740B1 EP0184740B1 (de)	1991-03-06

Family

ID=6252300

Family Applications (1)

Application Number	Title	Priority Date	Filing Date
EP85115217A Expired - Lifetime EP0184740B1 (de)	1984-12-08	1985-11-30	Verfahren zur Herstellung von Fettsäuremethylestern

Country Status (13)

Country	Link
US (1)	US4652406A (de)
EP (1)	EP0184740B1 (de)
JP (1)	JPH0662502B2 (de)
AT (1)	ATE61332T1 (de)
BR (1)	BR8506119A (de)
CA (1)	CA1261870A (de)
DE (2)	DE3444893A1 (de)
ES (1)	ES8606242A1 (de)
GB (1)	GB2168701B (de)
MX (1)	MX162267A (de)
MY (1)	MY101291A (de)
TR (1)	TR25060A (de)
ZA (1)	ZA859371B (de)

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SE9001245L (sv) *	1990-04-05	1991-10-06	Carl Johan Lindquist	Foerestringsprocess
US6262022B1 (en)	1992-06-25	2001-07-17	Novartis Ag	Pharmaceutical compositions containing cyclosporin as the active agent
CA2083346A1 (en) *	1991-12-13	1993-06-14	Eric G. Lundquist	A catalyzed esterification process
DE4209779C1 (de) *	1992-03-26	1993-07-15	Oelmuehle Leer Connemann Gmbh & Co., 2950 Leer, De
SG45449A1 (en)	1992-05-13	1998-01-16	Sandoz Ltd	Ophthalmic compositions
ES2168271T3 (es)	1992-09-25	2002-06-16	Novartis Ag	Composiciones farmaceuticas que contienen ciclosporinas.
AT399336B (de) *	1993-07-14	1995-04-25	Martin Mag Dr Mittelbach	Verfahren zur herstellung von fettsäurealkylestern
CZ295207B6 (cs) *	1997-01-30	2005-06-15	Novartis Ag	Tvrdá želatinová tobolka obsahující cyklosporin A
DE19732578C2 (de) *	1997-07-29	2000-08-24	Aventis Res & Tech Gmbh & Co	Verwendung von sulfonierten aromatischen Polyetherketon-Kationenaustauschern und sulfonierten Polyphenylensulfid-Kationenaustauschern als Katalysatoren
DE19810440C1 (de) *	1998-03-11	1999-09-23	Dhw Deutsche Hydrierwerke Gmbh	Verfahren zur Herstellung von ungesättigten Fettalkoholen aus Lauricölen
ATA16992000A (de)	2000-10-05	2001-12-15	Michael Dr Koncar	Verfahren zur herstellung von fettsäurealkylestern
US6965044B1 (en)	2001-07-06	2005-11-15	Iowa State University Research Foundation	Method of converting free fatty acids to fatty acid methyl esters with small excess of methanol
DE10154365A1 (de) *	2001-11-06	2003-05-15	Cognis Deutschland Gmbh	Verfahren zur Herstellung von Fettsäureestern aus nicht entsäuerten Fetten und Ölen
AT504727A1 (de)	2002-04-12	2008-07-15	Energea Umwelttechnologie Gmbh	Verfahren und anlage zur veresterung von fettsäuren
US20060042158A1 (en) *	2004-08-26	2006-03-02	Lee John H	Fuel products from plant or animal lipids
US7619104B2 (en) *	2005-04-04	2009-11-17	Renewable Products Development Laboratories, Inc.	Process for producing biodiesel or fatty acid esters from multiple triglyceride feedstocks
WO2007000913A1 (ja) *	2005-06-27	2007-01-04	Tokyo Institute Of Technology	高級脂肪酸エステルの製造方法
US7622600B1 (en) *	2006-01-06	2009-11-24	Redland Industries, Inc.	System and method for the continuous production of bio-diesel
US7828978B2 (en)	2006-01-11	2010-11-09	Doug Geier	Simultaneous synthesis and purification of a fatty acid monoester biodiesel fuel
CN101198677B (zh)	2006-04-28	2012-11-14	Sk化学股份有限公司	使用脂肪酸制备脂肪酸烷基酯的方法和设备
WO2008016330A2 (en) *	2006-08-01	2008-02-07	Sie Hendery @ Hendery	Bio formula to substitute diesel fuel
US20080289248A1 (en) *	2007-05-23	2008-11-27	Southern Illinois University Carbondale	Immobilized esterification catalysts for producing fatty acid alkyl esters
US20100130763A1 (en) *	2006-12-06	2010-05-27	Southern Illinois University Carbondale	Processes for the production of fatty acid alkyl esters
WO2008071041A1 (fr)	2006-12-15	2008-06-19	China Petroleum & Chemical Corporation	Procédé de préparation de biodiesel
US8288573B2 (en)	2006-12-15	2012-10-16	China Petroleum & Chemical Corporation	Process for preparing a bio-diesel
JP2008260819A (ja) *	2007-04-11	2008-10-30	National Institute Of Advanced Industrial & Technology	バイオディーゼル燃料の製造方法
US20080282606A1 (en) *	2007-04-16	2008-11-20	Plaza John P	System and process for producing biodiesel
US20100242346A1 (en) *	2007-09-19	2010-09-30	Best Energies, Inc	Processes for the esterification of free fatty acids and the production of biodiesel
US20090187035A1 (en) *	2008-01-22	2009-07-23	Cargill, Incorporated	Process for production of fatty acid alkyl esters
US20090247785A1 (en) *	2008-03-31	2009-10-01	The University Of Connecticut	Methods and systems for pretreatment of an oil stream
CN105176696A (zh)	2008-04-01	2015-12-23	Sk化学株式会社	使用脂肪酸制备脂肪酸烷基酯的方法
FR2929621A1 (fr) *	2008-04-08	2009-10-09	Arkema France	Utilisation d'acide methane sulfonique pour l'esterification d'acides gras
JP5646460B2 (ja) *	2008-05-14	2014-12-24	カウンシルオブサイエンティフィックアンドインダストリアルリサーチ	有効な潤滑剤ベースストックとしてのヒマシ油脂肪酸系エストリドエステルおよびそれらの誘導体
WO2009139884A1 (en) *	2008-05-14	2009-11-19	Ethox Chemicals, Llc	Natural butters reconstituted by transesterification with glycerin and its use in consmetics applications
KR101554607B1 (ko)	2008-11-07	2015-09-22	에스케이케미칼주식회사	지방산을 이용한 지방산알킬에스테르의 제조방법 및 장치
BRPI0921034B1 (pt) †	2008-11-17	2019-11-19	Basf Se	processo para preparar ésteres de ácido graxo e/ou misturas de éster de ácido graxo de alcoóis monovalentes de cadeia curta, e, uso de ácido metanossulfônico
SG172014A1 (en)	2008-12-08	2011-07-28	Initio Fuels Llc	Single step transesterification of feedstock using a gaseous catalyst
US20120124896A1 (en)	2009-06-26	2012-05-24	Research Institute Of Petroleum Processing, Sinopec	Diesel Composition and Method of Increasing Biodiesel Oxidation Stability
WO2011008058A2 (ko)	2009-07-17	2011-01-20	한국과학기술원	오일 생성능을 가지는 미생물을 이용한 지방산 알킬에스테르의 제조방법
MY151440A (en) *	2009-10-29	2014-05-30	Malaysian Palm Oil Board Mpob	A method of converting free fatty acid (ffa) from oil to methyl ester
AT510636B1 (de)	2010-10-28	2016-11-15	Wimmer Theodor	Verfahren zur herstellung von fettsäureestern niederer alkohole
CN102851122A (zh) *	2011-06-30	2013-01-02	中国石油化工股份有限公司	一种制备脂肪酸酯的方法
CN103013678B (zh) *	2011-09-20	2014-12-31	中国石油化工股份有限公司	降低生物柴油粗产品酸值的方法以及生物柴油的制备方法
KR102327852B1 (ko)	2013-07-22	2021-11-18	에스케이에코프라임 주식회사	지방을 이용한 지방산알킬에스테르의 제조방법
US9328054B1 (en)	2013-09-27	2016-05-03	Travis Danner	Method of alcoholisis of fatty acids and fatty acid gyicerides
CA2941399A1 (en) *	2014-03-04	2015-09-11	Basf Se	Method for degumming and esterification of an oil
ES2585706B1 (es) *	2016-04-21	2017-08-14	Soluciones Industriales Extremeñas Sll	Procedimiento mejorado para el refino y esterificación continua de cualquier material graso de origen vegetal o animal, especialmente diseñado para subproductos animales de categoría 1 y 2
ES2660207B8 (es) *	2016-09-21	2019-01-10	Bio Oils Huelva S L	Procedimiento de alta eficacia para la producción de alquil-ésteres de ácidos grasos mediante catálisis ácida y procedimiento de tratamiento
KR102289779B1 (ko) *	2016-11-25	2021-08-12	아르끄마 프랑스	지방산 처리를 위한 산 조성물
FR3059328B1 (fr) *	2016-11-25	2018-11-16	Arkema France	Composition acide pour le traitement d'acides gras
CN108977281A (zh) *	2018-07-05	2018-12-11	浙江恒翔化工有限公司	一种利用高酸价劣质油脂制备甲酯的方法
BR112021006249A2 (pt) *	2018-10-10	2021-07-06	Basf Se	método para produzir éster alquílico de ácido graxo
WO2021204610A1 (en) *	2020-04-07	2021-10-14	Basf Se	Energy efficient biodiesel production from natural or industrial waste oil

Citations (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2383599A (en) *	1942-10-17	1945-08-28	Colgate Palmolive Peet Co	Treating fatty glycerides
US2383601A (en) *	1943-04-28	1945-08-28	Colgate Palmolive Peet Co	Treating fats and fatty oils
US4164506A (en) *	1977-03-17	1979-08-14	Kao Soap Co., Ltd.	Process for producing lower alcohol esters of fatty acids
EP0127104A1 (de) *	1983-05-30	1984-12-05	Henkel Kommanditgesellschaft auf Aktien	Verfahren zur Herstellung von Fettsäureestern kurzkettiger aliphatischer Alkohole aus freie Fettsäuren enthaltenden Fetten und/oder Ölen

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US22751A (en) *		1859-01-25		Ball furniture-caster
US2360844A (en) *	1941-11-26	1944-10-24	Du Pont	Preparation of detergents
US2486444A (en) *	1947-07-08	1949-11-01	Baker Castor Oil Co	Process of producing esters

1984
- 1984-12-08 DE DE19843444893 patent/DE3444893A1/de not_active Withdrawn
1985
- 1985-11-25 GB GB08528953A patent/GB2168701B/en not_active Expired
- 1985-11-30 EP EP85115217A patent/EP0184740B1/de not_active Expired - Lifetime
- 1985-11-30 AT AT85115217T patent/ATE61332T1/de not_active IP Right Cessation
- 1985-11-30 DE DE8585115217T patent/DE3582022D1/de not_active Expired - Fee Related
- 1985-12-04 TR TR85/48891A patent/TR25060A/xx unknown
- 1985-12-06 CA CA000497012A patent/CA1261870A/en not_active Expired
- 1985-12-06 ZA ZA859371A patent/ZA859371B/xx unknown
- 1985-12-06 US US06/806,074 patent/US4652406A/en not_active Expired - Fee Related
- 1985-12-06 ES ES549666A patent/ES8606242A1/es not_active Expired
- 1985-12-06 BR BR8506119A patent/BR8506119A/pt not_active IP Right Cessation
- 1985-12-09 MX MX866A patent/MX162267A/es unknown
- 1985-12-09 JP JP60277773A patent/JPH0662502B2/ja not_active Expired - Lifetime
1987
- 1987-04-02 MY MYPI87000423A patent/MY101291A/en unknown

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number	Priority date	Publication date	Assignee	Title
US2383599A (en) *	1942-10-17	1945-08-28	Colgate Palmolive Peet Co	Treating fatty glycerides
US2383601A (en) *	1943-04-28	1945-08-28	Colgate Palmolive Peet Co	Treating fats and fatty oils
US4164506A (en) *	1977-03-17	1979-08-14	Kao Soap Co., Ltd.	Process for producing lower alcohol esters of fatty acids
EP0127104A1 (de) *	1983-05-30	1984-12-05	Henkel Kommanditgesellschaft auf Aktien	Verfahren zur Herstellung von Fettsäureestern kurzkettiger aliphatischer Alkohole aus freie Fettsäuren enthaltenden Fetten und/oder Ölen

Also Published As

Publication number	Publication date
DE3444893A1 (de)	1986-06-12
GB2168701A (en)	1986-06-25
EP0184740A2 (de)	1986-06-18
ATE61332T1 (de)	1991-03-15
DE3582022D1 (de)	1991-04-11
MY101291A (en)	1991-09-05
TR25060A (tr)	1992-09-22
JPH0662502B2 (ja)	1994-08-17
ES8606242A1 (es)	1986-04-16
ES549666A0 (es)	1986-04-16
GB8528953D0 (en)	1986-01-02
MX162267A (es)	1991-04-19
ZA859371B (en)	1986-07-30
CA1261870A (en)	1989-09-26
US4652406A (en)	1987-03-24
EP0184740B1 (de)	1991-03-06
BR8506119A (pt)	1986-08-26
JPS61140544A (ja)	1986-06-27
GB2168701B (en)	1988-11-30

Legal Events

Date	Code	Title	Description
1986-05-03	PUAI	Public reference made under article 153(3) epc to a published international application that has entered the european phase	Free format text: ORIGINAL CODE: 0009012
1986-06-18	AK	Designated contracting states	Kind code of ref document: A2 Designated state(s): AT BE CH DE FR IT LI NL SE
1987-07-21	PUAL	Search report despatched	Free format text: ORIGINAL CODE: 0009013
1987-09-09	AK	Designated contracting states	Kind code of ref document: A3 Designated state(s): AT BE CH DE FR IT LI NL SE
1987-11-19	17P	Request for examination filed	Effective date: 19870925
1989-05-17	17Q	First examination report despatched	Effective date: 19890329
1991-01-19	GRAA	(expected) grant	Free format text: ORIGINAL CODE: 0009210
1991-03-06	AK	Designated contracting states	Kind code of ref document: B1 Designated state(s): AT BE CH DE FR IT LI NL SE
1991-03-06	REF	Corresponds to:	Ref document number: 61332 Country of ref document: AT Date of ref document: 19910315 Kind code of ref document: T
1991-03-29	ET	Fr: translation filed
1991-04-11	REF	Corresponds to:	Ref document number: 3582022 Country of ref document: DE Date of ref document: 19910411
1991-05-28	ITF	It: translation for a ep patent filed	Owner name: STUDIO JAUMANN
1992-01-09	PLBE	No opposition filed within time limit	Free format text: ORIGINAL CODE: 0009261
1992-01-09	STAA	Information on the status of an ep patent application or granted ep patent	Free format text: STATUS: NO OPPOSITION FILED WITHIN TIME LIMIT
1992-02-26	26N	No opposition filed
1993-10-20	PGFP	Annual fee paid to national office [announced via postgrant information from national office to epo]	Ref country code: CH Payment date: 19931020 Year of fee payment: 9
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1995-01-31	EAL	Se: european patent in force in sweden	Ref document number: 85115217.3
1995-05-31	BERE	Be: lapsed	Owner name: HENKEL K.G.A.A. Effective date: 19941130
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Publication	Publication Date	Title
GB2168701B (en)	1988-11-30	A process for the production of fatty acid methyl esters
CA2143441A1 (en)	1994-03-17	Recovery of tocopherol and sterol
FI116847B (fi)	2006-03-15	Menetelmä rasvahappoalkyyliestereiden valmistamiseksi
Bondioli	2004	The preparation of fatty acid esters by means of catalytic reactions
CA2264558A1 (en)	1998-03-26	Method for preparing fatty acid esters
ES543917A0 (es)	1986-01-16	Procedimiento para preparar esteres de acidos grasos de al- coholes primarios y secundarios de cadena corta
CZ111694A3 (en)	1995-02-15	Process for preparing esters of fatty acids with monovalent alcohols having a short chain
JP2003507495A (ja)	2003-02-25	トリグリセリドおよび脂肪酸の混合物から脂肪酸メチルエステルを生成する単相プロセス
CZ279421B6 (cs)	1995-04-12	Způsob výroby esterů mastných kyselin nižších alkoholů
AU2004267023A1 (en)	2005-03-03	Method of making alkyl esters using glycerin
DE3560167D1 (en)	1987-06-19	Process for the production of mixtures of c6-c10 fatty acids
MX9804560A (es)	1998-09-30	Recuperacion de tocoferoles.
EP0320043A3 (de)	1991-07-24	Verfahren zur Herstellung von Polyol-Fettsäureester
SU131352A1 (ru)	1959-11-30	Применение металлического натри в качестве катализатора