EA201590075A1 - Носители катализатора на основе карбида кремния, покрытого tio, для синтеза фишера-тропша - Google Patents

Носители катализатора на основе карбида кремния, покрытого tio, для синтеза фишера-тропша

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Publication number
EA201590075A1
EA201590075A1 EA201590075A EA201590075A EA201590075A1 EA 201590075 A1 EA201590075 A1 EA 201590075A1 EA 201590075 A EA201590075 A EA 201590075A EA 201590075 A EA201590075 A EA 201590075A EA 201590075 A1 EA201590075 A1 EA 201590075A1
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Eurasian Patent Office
Prior art keywords
tio
trips
fisher
synthesis
carrier
Prior art date
Application number
EA201590075A
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English (en)
Other versions
EA030287B1 (ru
Inventor
Юэфэн Лю
Кюонг Фам-Хюю
Патрик Нгуйен
Шарлотт Фам
Original Assignee
Сикат Каталистс, Инк.
Сантр Насьональ Де Ля Решерш Сьянтифик
Юниверсите Де Страсбур
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Priority claimed from FR1256028A external-priority patent/FR2992236A1/fr
Application filed by Сикат Каталистс, Инк., Сантр Насьональ Де Ля Решерш Сьянтифик, Юниверсите Де Страсбур filed Critical Сикат Каталистс, Инк.
Publication of EA201590075A1 publication Critical patent/EA201590075A1/ru
Publication of EA030287B1 publication Critical patent/EA030287B1/ru

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/02—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon
    • C07C1/04—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon from carbon monoxide with hydrogen
    • C07C1/0425—Catalysts; their physical properties
    • C07C1/043—Catalysts; their physical properties characterised by the composition
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/06—Silicon, titanium, zirconium or hafnium; Oxides or hydroxides thereof
    • B01J21/063—Titanium; Oxides or hydroxides thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/745—Iron
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/74—Iron group metals
    • B01J23/75—Cobalt
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
    • B01J27/20—Carbon compounds
    • B01J27/22—Carbides
    • B01J27/224—Silicon carbide
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/56—Foraminous structures having flow-through passages or channels, e.g. grids or three-dimensional monoliths
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/612—Surface area less than 10 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/60—Catalysts, in general, characterised by their form or physical properties characterised by their surface properties or porosity
    • B01J35/61—Surface area
    • B01J35/613—10-100 m2/g
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0203—Impregnation the impregnation liquid containing organic compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0205—Impregnation in several steps
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0207—Pretreatment of the support
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0209—Impregnation involving a reaction between the support and a fluid
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0201—Impregnation
    • B01J37/0213—Preparation of the impregnating solution
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C1/00—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon
    • C07C1/02—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon
    • C07C1/04—Preparation of hydrocarbons from one or more compounds, none of them being a hydrocarbon from oxides of a carbon from carbon monoxide with hydrogen
    • C07C1/0425—Catalysts; their physical properties
    • C07C1/0445—Preparation; Activation
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G2/00—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon
    • C10G2/30—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen
    • C10G2/32—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts
    • C10G2/33—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used
    • C10G2/331—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals
    • C10G2/332—Production of liquid hydrocarbon mixtures of undefined composition from oxides of carbon from carbon monoxide with hydrogen with the use of catalysts characterised by the catalyst used containing group VIII-metals of the iron-group

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • General Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Catalysts (AREA)
  • Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Способ получения носителя катализатора на основе SiC, покрытого, по меньшей мере частично, TiO, отличающийся тем, что способ включает следующие стадии, на которых (а) готовят носитель из β-SiC с высокой пористостью; (b) получают раствор по меньшей мере одного предшественника TiO; (с) носитель пропитывают полученным раствором; (d) сушат пропитанный носитель; (е) прокаливают пропитанный носитель для превращения предшественника TiOв TiO. Благодаря активной фазе из железа или кобальта этот катализатор является приемлемым для реакции Фишера-Тропша.
EA201590075A 2012-06-26 2013-06-24 НОСИТЕЛЬ КАТАЛИЗАТОРА НА ОСНОВЕ КАРБИДА КРЕМНИЯ, ПОКРЫТОГО TiO, ДЛЯ СИНТЕЗА ФИШЕРА-ТРОПША EA030287B1 (ru)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
FR1256028A FR2992236A1 (fr) 2012-06-26 2012-06-26 Supports de catalyseur a base de carbure de silicium recouvert de tio2 pour la synthese de fischer-tropsch
FR1257446 2012-07-31
PCT/FR2013/051465 WO2014001697A1 (fr) 2012-06-26 2013-06-24 Supports de catalyseur à base de carbure de silicium recouvert de TiO2 pour la synthèse de Fischer-Tropsch

Publications (2)

Publication Number Publication Date
EA201590075A1 true EA201590075A1 (ru) 2015-05-29
EA030287B1 EA030287B1 (ru) 2018-07-31

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Family Applications (1)

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EA201590075A EA030287B1 (ru) 2012-06-26 2013-06-24 НОСИТЕЛЬ КАТАЛИЗАТОРА НА ОСНОВЕ КАРБИДА КРЕМНИЯ, ПОКРЫТОГО TiO, ДЛЯ СИНТЕЗА ФИШЕРА-ТРОПША

Country Status (9)

Country Link
US (1) US9416066B2 (ru)
EP (1) EP2864044B1 (ru)
CN (1) CN104661748B (ru)
AU (1) AU2013283037B2 (ru)
BR (1) BR112014032448B1 (ru)
DK (1) DK2864044T3 (ru)
EA (1) EA030287B1 (ru)
WO (1) WO2014001697A1 (ru)
ZA (1) ZA201500420B (ru)

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WO2014207096A1 (en) * 2013-06-27 2014-12-31 Sicat Method for manufacturing shaped beta-sic mesoporous products and products obtained by this method
GB2544210B (en) * 2014-07-16 2020-10-21 Velocys Tech Ltd Cobalt-containing fischer-tropsch catalysts, methods of making, and methods of conducting fischer-tropsch synthesis
CN108698018A (zh) 2015-07-14 2018-10-23 英国石油有限公司 包含一种或多种酸和/或使用一种或多种酸制备的挤出的二氧化钛基材料
US20180200693A1 (en) 2015-07-14 2018-07-19 Ewen James Ferguson Extruded Titania-Based Materials Comprising Quaternary Ammonium Compounds and/or Prepared Using Quaternary Ammonium Compounds
CN108290145B (zh) 2015-07-14 2021-06-25 英国石油有限公司 包含中孔和大孔的挤出的二氧化钛基材料
US10682627B2 (en) 2015-07-14 2020-06-16 Bp P.L.C. Extruded titania-based material comprising zirconium oxide
KR101954067B1 (ko) * 2017-11-28 2019-03-06 한국과학기술연구원 촉매 금속이 담지된 다공질 탄화규소 구조체의 제조방법
WO2019236926A2 (en) * 2018-06-06 2019-12-12 Nexceris Innovation Holdings, Llc Catalyst support materials, catalyst supports, catalysts and reaction methods using catalysts
CN108855169A (zh) * 2018-08-16 2018-11-23 南京林业大学 用作填料的多孔碳化硅/改性二氧化钛复合光催化剂制备方法
CN109261184A (zh) * 2018-11-23 2019-01-25 哈尔滨工业大学 一种SiC/TiO2复合光催化纳米颗粒的制备方法

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FR2705340B1 (fr) 1993-05-13 1995-06-30 Pechiney Recherche Fabrication de mousse de carbure de silicium à partir d'une mousse de polyuréthane imprégnée de résine contenant du silicium.
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FR2965191A1 (fr) * 2010-09-23 2012-03-30 Centre Nat Rech Scient Reacteur a plaques pour la synthese fischer-tropsch

Also Published As

Publication number Publication date
ZA201500420B (en) 2016-05-25
WO2014001697A1 (fr) 2014-01-03
EP2864044B1 (fr) 2019-12-25
EP2864044A1 (fr) 2015-04-29
BR112014032448A2 (pt) 2017-06-27
EA030287B1 (ru) 2018-07-31
CN104661748B (zh) 2019-04-12
AU2013283037A8 (en) 2015-03-12
CN104661748A (zh) 2015-05-27
US20150191401A1 (en) 2015-07-09
DK2864044T3 (da) 2020-03-16
BR112014032448B1 (pt) 2020-11-17
AU2013283037B2 (en) 2017-05-25
AU2013283037A1 (en) 2015-01-22
US9416066B2 (en) 2016-08-16

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