EA201001565A1 - Получение легкосыпучих гранул метилглициндиуксусной кислоты - Google Patents
Получение легкосыпучих гранул метилглициндиуксусной кислотыInfo
- Publication number
- EA201001565A1 EA201001565A1 EA201001565A EA201001565A EA201001565A1 EA 201001565 A1 EA201001565 A1 EA 201001565A1 EA 201001565 A EA201001565 A EA 201001565A EA 201001565 A EA201001565 A EA 201001565A EA 201001565 A1 EA201001565 A1 EA 201001565A1
- Authority
- EA
- Eurasian Patent Office
- Prior art keywords
- range
- granules
- acetic acid
- methylglycindyux
- easyfunctions
- Prior art date
Links
- 239000008187 granular material Substances 0.000 title abstract 2
- 239000002253 acid Substances 0.000 title 1
- WPDWQJNKGVGVBB-UHFFFAOYSA-N acetic acid 2-(methylamino)acetic acid Chemical class CC(O)=O.CNCC(O)=O WPDWQJNKGVGVBB-UHFFFAOYSA-N 0.000 abstract 2
- 239000002002 slurry Substances 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical group [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical group 0.000 abstract 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
- 150000001342 alkaline earth metals Chemical group 0.000 abstract 1
- 150000003863 ammonium salts Chemical class 0.000 abstract 1
- 229910052739 hydrogen Inorganic materials 0.000 abstract 1
- 239000001257 hydrogen Substances 0.000 abstract 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000007921 spray Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
- C07C227/38—Separation; Purification; Stabilisation; Use of additives
- C07C227/40—Separation; Purification
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0047—Detergents in the form of bars or tablets
- C11D17/0065—Solid detergents containing builders
- C11D17/0073—Tablets
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
- C11D3/16—Organic compounds
- C11D3/26—Organic compounds containing nitrogen
- C11D3/33—Amino carboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3245—Aminoacids
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Detergent Compositions (AREA)
- Seeds, Soups, And Other Foods (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Настоящее изобретение относится к способу получения характеризующихся низкой гигроскопичностью легкосыпучих гранул одной или нескольких солей метилглициндиуксусной кислоты (МГДК), описывающихся формулой, где R = СН, а М представляет собой водород, щелочной металл, щелочно-земельный металл, аммоний или замещенный аммоний в соответствующих стехиометрических количествах, при этом способ включает стадии, на которых: i) нагревают концентрированную суспензию, содержащую метилглициндиуксусную кислоту (МГДК) и/или любые ее соли, при этом суспензия характеризуется уровнем содержания твердого вещества в диапазоне от 45 до 70%, а в подходящем случае в диапазоне от 50 до 70%, и уровнем влагосодержания в диапазоне от 30 вплоть до 55%, а в подходящем случае от 30 до 50% до температуры, находящейся в диапазоне от 50 до 120°С, предпочтительно составляющей около 80°С, и ii) подвергают упомянутую суспензию распылительному гранулированию с использованием температуры воздуха на входе, составляющей 120°С и менее.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP08153924 | 2008-04-01 | ||
| PCT/EP2009/053781 WO2009103822A1 (en) | 2008-04-01 | 2009-03-31 | Preparation of free flowing granules of methyglycine diacetic acid |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| EA201001565A1 true EA201001565A1 (ru) | 2011-02-28 |
| EA031547B1 EA031547B1 (ru) | 2019-01-31 |
Family
ID=40688576
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EA201001565A EA031547B1 (ru) | 2008-04-01 | 2009-03-31 | Получение легкосыпучих гранул, содержащих соли метилглициндиуксусной кислоты |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US8183410B2 (ru) |
| EP (2) | EP2257522B1 (ru) |
| BR (1) | BRPI0911375A2 (ru) |
| CA (1) | CA2719754C (ru) |
| EA (1) | EA031547B1 (ru) |
| MX (1) | MX2010010779A (ru) |
| PL (2) | PL2257522T3 (ru) |
| PT (1) | PT3061744T (ru) |
| TR (1) | TR201808032T4 (ru) |
| WO (1) | WO2009103822A1 (ru) |
Families Citing this family (87)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2009103822A1 (en) | 2008-04-01 | 2009-08-27 | Unilever Nv | Preparation of free flowing granules of methyglycine diacetic acid |
| BRPI1012868A2 (pt) * | 2009-05-20 | 2018-02-20 | Basf Se | processo para a preparacao de um po para pulverizacao, e, uso do po para pulverizacao |
| DE102009038951A1 (de) | 2009-08-26 | 2011-03-03 | Inprotec Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| AU2010305833A1 (en) * | 2009-10-12 | 2012-04-19 | Basf Se | Method for producing a powder containing one or more complexing agent salts |
| MY158493A (en) | 2009-10-30 | 2016-10-14 | Akzo Nobel Chemicals Int Bv | Use of a metal supplement in animal feed |
| CA2782583C (en) | 2009-12-24 | 2018-03-20 | Akzo Nobel Chemicals International B.V. | Coated particles of a glumatic acid n,n-diacetate chelating agent |
| DE102009060814A1 (de) | 2009-12-30 | 2011-07-07 | inprotec AG, 79423 | Verfahren zur Herstellung eines Feststoffs mit hinreichend geringer Hygroskopizität, der Glutaminsäure-N,N-diessigsäure (GLDA) oder ein Derivat davon enthält |
| PL2380962T3 (pl) | 2010-04-23 | 2017-01-31 | The Procter And Gamble Company | Cząstka |
| ES2646166T3 (es) | 2010-04-26 | 2017-12-12 | Novozymes A/S | Gránulos enzimáticos |
| ES2648240T3 (es) * | 2010-06-04 | 2017-12-29 | Dalli-Werke Gmbh & Co. Kg | Composición en partículas de baja higroscopicidad que comprende uno o más compuestos quelantes de aminopolicarboxilato |
| CA2809749A1 (en) * | 2010-09-27 | 2012-04-05 | Basf Se | Process for producing granules comprising one or more complexing agent salts |
| GB2491619B (en) * | 2011-06-09 | 2014-10-01 | Pq Silicas Bv | Builder granules and process for their preparation |
| CN107475235B (zh) | 2011-06-20 | 2022-09-13 | 诺维信公司 | 颗粒组合物 |
| CN103620029B (zh) | 2011-06-24 | 2017-06-09 | 诺维信公司 | 具有蛋白酶活性的多肽和编码它们的多核苷酸 |
| HUE058093T2 (hu) | 2011-06-30 | 2022-06-28 | Novozymes As | Eljárás alfa-amilázok szkrínelésére |
| US10711262B2 (en) | 2011-07-12 | 2020-07-14 | Novozymes A/S | Storage-stable enzyme granules |
| JP2014531895A (ja) | 2011-08-15 | 2014-12-04 | ノボザイムス アクティーゼルスカブ | セルラーゼ活性を有するポリペプチドおよびそれをコードするポリヌクレオチド |
| CN104204200B (zh) | 2011-09-22 | 2017-06-09 | 诺维信公司 | 具有蛋白酶活性的多肽和编码它们的多核苷酸 |
| PL2584028T3 (pl) * | 2011-10-19 | 2017-10-31 | Procter & Gamble | Cząstka |
| MX2014006205A (es) | 2011-11-25 | 2014-07-14 | Novozymes As | Variantes de subtilasa y polinucleotidos que las codifican. |
| US20140335596A1 (en) | 2011-12-20 | 2014-11-13 | Novozymes A/S | Subtilase Variants and Polynucleotides Encoding Same |
| EP2807254B1 (en) | 2012-01-26 | 2017-08-02 | Novozymes A/S | Use of polypeptides having protease activity in animal feed and detergents |
| WO2013120948A1 (en) | 2012-02-17 | 2013-08-22 | Novozymes A/S | Subtilisin variants and polynucleotides encoding same |
| CN104704102A (zh) | 2012-03-07 | 2015-06-10 | 诺维信公司 | 洗涤剂组合物和洗涤剂组合物中光增亮剂的取代 |
| CN117904080A (zh) | 2012-05-07 | 2024-04-19 | 诺维信公司 | 具有黄原胶降解活性的多肽以及编码其的核苷酸 |
| CN104394708A (zh) | 2012-06-20 | 2015-03-04 | 诺维信公司 | 具有蛋白酶活性的多肽在动物饲料和洗涤剂中的用途 |
| GB201214558D0 (en) | 2012-08-15 | 2012-09-26 | Reckitt Benckiser Nv | Detergent granule |
| MX363360B (es) | 2012-12-21 | 2019-03-21 | Novozymes As | Polipéptidos que poseen actividad proteasa y polinucleótidos que los codifican. |
| US9902946B2 (en) | 2013-01-03 | 2018-02-27 | Novozymes A/S | Alpha-amylase variants and polynucleotides encoding same |
| WO2014183921A1 (en) | 2013-05-17 | 2014-11-20 | Novozymes A/S | Polypeptides having alpha amylase activity |
| CN105264058B (zh) | 2013-06-06 | 2022-03-29 | 诺维信公司 | α-淀粉酶变体以及对其进行编码的多核苷酸 |
| EP3013955A1 (en) | 2013-06-27 | 2016-05-04 | Novozymes A/S | Subtilase variants and polynucleotides encoding same |
| EP3013956B1 (en) | 2013-06-27 | 2023-03-01 | Novozymes A/S | Subtilase variants and polynucleotides encoding same |
| RU2015156280A (ru) | 2013-07-04 | 2017-08-09 | Новозимс А/С | Полипептиды, обладающие эффектом против переосаждения, и полинуклеотиды, кодирующие их |
| US10150957B2 (en) | 2013-07-29 | 2018-12-11 | Novozymes A/S | Protease variants and polynucleotides encoding same |
| EP2832853A1 (en) | 2013-07-29 | 2015-02-04 | Henkel AG&Co. KGAA | Detergent composition comprising protease variants |
| CN105358684A (zh) | 2013-07-29 | 2016-02-24 | 诺维信公司 | 蛋白酶变体以及对其进行编码的多核苷酸 |
| WO2015049370A1 (en) | 2013-10-03 | 2015-04-09 | Novozymes A/S | Detergent composition and use of detergent composition |
| EP3453757B1 (en) | 2013-12-20 | 2020-06-17 | Novozymes A/S | Polypeptides having protease activity and polynucleotides encoding same |
| JP6900193B2 (ja) * | 2014-02-13 | 2021-07-07 | ビーエイエスエフ・ソシエタス・エウロパエアＢａｓｆ Ｓｅ | 粉末及び顆粒、この粉末及び顆粒の製造方法、並びに、その使用方法 |
| US20160333292A1 (en) | 2014-03-05 | 2016-11-17 | Novozymes A/S | Compositions and Methods for Improving Properties of Cellulosic Textile Materials with Xyloglucan Endotransglycosylase |
| CN106062270A (zh) | 2014-03-05 | 2016-10-26 | 诺维信公司 | 使用木葡聚糖内糖基转移酶改进非纤维素纺织材料的性质的组合物和方法 |
| CN106103708A (zh) | 2014-04-01 | 2016-11-09 | 诺维信公司 | 具有α淀粉酶活性的多肽 |
| US20170121695A1 (en) | 2014-06-12 | 2017-05-04 | Novozymes A/S | Alpha-amylase variants and polynucleotides encoding same |
| CN106661566A (zh) | 2014-07-04 | 2017-05-10 | 诺维信公司 | 枯草杆菌酶变体以及编码它们的多核苷酸 |
| EP3164486B1 (en) | 2014-07-04 | 2020-05-13 | Novozymes A/S | Subtilase variants and polynucleotides encoding same |
| EP3221447A1 (en) | 2014-11-20 | 2017-09-27 | Novozymes A/S | Alicyclobacillus variants and polynucleotides encoding same |
| EP3227444B1 (en) | 2014-12-04 | 2020-02-12 | Novozymes A/S | Subtilase variants and polynucleotides encoding same |
| WO2016096714A1 (en) | 2014-12-15 | 2016-06-23 | Henkel Ag & Co. Kgaa | Detergent composition comprising subtilase variants |
| EP3106508B1 (en) | 2015-06-18 | 2019-11-20 | Henkel AG & Co. KGaA | Detergent composition comprising subtilase variants |
| CN108012544A (zh) | 2015-06-18 | 2018-05-08 | 诺维信公司 | 枯草杆菌酶变体以及编码它们的多核苷酸 |
| EP3362556A1 (en) | 2015-10-14 | 2018-08-22 | Novozymes A/S | Polypeptide variants |
| CN108291215A (zh) | 2015-10-14 | 2018-07-17 | 诺维信公司 | 具有蛋白酶活性的多肽以及编码它们的多核苷酸 |
| US10975334B2 (en) | 2015-12-11 | 2021-04-13 | Basf Se | Process for manufacturing granules |
| CN109715792A (zh) | 2016-06-03 | 2019-05-03 | 诺维信公司 | 枯草杆菌酶变体和对其进行编码的多核苷酸 |
| EP3472294B1 (en) * | 2016-06-20 | 2020-07-22 | Basf Se | Powders and granules and process for making such powders and granules |
| EP3266860B1 (en) | 2016-07-08 | 2020-04-08 | The Procter and Gamble Company | Process for making a particle |
| CA3027272C (en) | 2016-07-13 | 2022-06-21 | The Procter & Gamble Company | Bacillus cibi dnase variants and uses thereof |
| BR112018077082B1 (pt) | 2016-07-15 | 2023-03-28 | Basf Se | Processo para fabricação de grânulos de sais, grânulo, uso de um grânulo |
| CN110891930B (zh) | 2017-07-07 | 2021-09-03 | 诺力昂化学品国际有限公司 | 制备氨基酸二乙酸的固体组合物的方法 |
| MX2020004145A (es) | 2017-10-27 | 2020-08-03 | Novozymes As | Variantes de desoxirribonucleasa (dnasa). |
| ES2910120T3 (es) | 2017-10-27 | 2022-05-11 | Procter & Gamble | Composiciones detergentes que comprenden variantes polipeptídicas |
| EP3781660A1 (en) | 2018-04-17 | 2021-02-24 | Novozymes A/S | Polypeptides comprising carbohydrate binding activity in detergent compositions and their use in reducing wrinkles in textile or fabric |
| CN112771143A (zh) | 2018-09-27 | 2021-05-07 | 巴斯夫欧洲公司 | 制备颗粒或粉末的方法 |
| WO2020094480A1 (en) | 2018-11-07 | 2020-05-14 | Basf Se | Process for manufacturing granules, and granules and their use |
| WO2020104231A1 (en) | 2018-11-19 | 2020-05-28 | Basf Se | Powders and granules containing a chelating agent and an enzyme |
| CN113382980A (zh) | 2018-12-21 | 2021-09-10 | 诺力昂化学品国际有限公司 | 甲基甘氨酸n,n-二乙酸的易碎相组合物 |
| AU2020242303A1 (en) | 2019-03-21 | 2021-06-24 | Novozymes A/S | Alpha-amylase variants and polynucleotides encoding same |
| CN113710789A (zh) * | 2019-04-01 | 2021-11-26 | 巴斯夫欧洲公司 | 制造颗粒或粉末的方法 |
| WO2020207944A1 (en) | 2019-04-10 | 2020-10-15 | Novozymes A/S | Polypeptide variants |
| US20220325204A1 (en) | 2019-08-27 | 2022-10-13 | Novozymes A/S | Detergent composition |
| US20220315866A1 (en) | 2019-09-19 | 2022-10-06 | Novozymes A/S | Detergent Composition |
| WO2021064068A1 (en) | 2019-10-03 | 2021-04-08 | Novozymes A/S | Polypeptides comprising at least two carbohydrate binding domains |
| EP4073217A1 (en) | 2019-12-11 | 2022-10-19 | Basf Se | Granules of mgda and (meth)acrylic acid homo- or co-polymer; process for making the same |
| BR112022016512A2 (pt) | 2020-02-20 | 2022-10-11 | Basf Se | Processo para produzir sal de metal alcalino, partículas em formato de coluna, e, uso de partículas em formato de coluna |
| WO2021185702A1 (en) | 2020-03-17 | 2021-09-23 | Basf Se | Process for making a granule |
| EP3892708A1 (en) | 2020-04-06 | 2021-10-13 | Henkel AG & Co. KGaA | Cleaning compositions comprising dispersin variants |
| US20230391713A1 (en) | 2020-06-19 | 2023-12-07 | Nouryon Chemicals International B.V. | Process to prepare a co granule of methylglycine n,n diacetic acid salts employing a crumbly phase composition of methylglycine n,n diacetic acid salts |
| RU2747177C1 (ru) * | 2020-07-30 | 2021-04-28 | Общество с ограниченной ответственностью "Синергетик" | Способ получения концентрированного средства для стирки и его упаковка |
| CN116507725A (zh) | 2020-10-07 | 2023-07-28 | 诺维信公司 | α-淀粉酶变体 |
| CN116323551A (zh) | 2020-12-17 | 2023-06-23 | 巴斯夫欧洲公司 | 制备氨基羧酸盐络合剂的固体碱金属盐的方法 |
| WO2022171780A2 (en) | 2021-02-12 | 2022-08-18 | Novozymes A/S | Alpha-amylase variants |
| EP4301504A1 (en) | 2021-03-04 | 2024-01-10 | Basf Se | Process for making a particulate coated organic salt, and particulate coated salt |
| WO2022268885A1 (en) | 2021-06-23 | 2022-12-29 | Novozymes A/S | Alpha-amylase polypeptides |
| WO2023025637A1 (en) | 2021-08-25 | 2023-03-02 | Basf Se | Process for making a granule or powder containing a complexing agent |
| WO2023110611A1 (en) | 2021-12-17 | 2023-06-22 | Basf Se | Process for making granules and powders |
| WO2024046786A1 (en) | 2022-08-29 | 2024-03-07 | Basf Se | Process for preparing a solid composition comprising at least one aminocarboxylate complexing agent |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3956379A (en) * | 1970-10-23 | 1976-05-11 | Ethyl Corporation | Process for recovering NTA |
| DD296680A5 (de) | 1990-07-13 | 1991-12-12 | Veb Petrolchemisches Kombinat Schwedt,De | Verfahren zur granulierung des trinatriumsalzes der nitrilotriessigsaeure |
| DE19649681A1 (de) | 1996-11-29 | 1998-06-04 | Basf Ag | Verfahren zur Herstellung eines kristallinen Feststoffes aus Glycin-N,N-diessigsäure-Derivaten mit hinreichend geringer Hygroskopizität |
| US6770616B1 (en) * | 1999-03-04 | 2004-08-03 | The Procter & Gamble Company | Detergent tablet |
| DE19937345A1 (de) * | 1999-08-11 | 2001-02-15 | Basf Ag | Mischpulver oder Mischgranulat auf Basis von Glycin-N,N-diessigsäure |
| GB2415695A (en) * | 2004-07-02 | 2006-01-04 | Reckitt Benckiser Nv | Detergent composition comprising a chelating agent |
| DE102004032320A1 (de) | 2004-07-02 | 2006-01-19 | Basf Ag | Mischpulver oder Mischgranulat auf Basis von MGDA |
| EP1721962B1 (en) * | 2005-05-11 | 2008-08-13 | Unilever N.V. | Dishwashing composition and process for washing dishes |
| WO2009103822A1 (en) | 2008-04-01 | 2009-08-27 | Unilever Nv | Preparation of free flowing granules of methyglycine diacetic acid |
-
2009
- 2009-03-31 WO PCT/EP2009/053781 patent/WO2009103822A1/en active Application Filing
- 2009-03-31 PL PL09712776.5T patent/PL2257522T3/pl unknown
- 2009-03-31 BR BRPI0911375A patent/BRPI0911375A2/pt not_active Application Discontinuation
- 2009-03-31 MX MX2010010779A patent/MX2010010779A/es active IP Right Grant
- 2009-03-31 EP EP09712776.5A patent/EP2257522B1/en active Active
- 2009-03-31 PL PL16156441T patent/PL3061744T3/pl unknown
- 2009-03-31 CA CA2719754A patent/CA2719754C/en not_active Expired - Fee Related
- 2009-03-31 US US12/935,007 patent/US8183410B2/en active Active
- 2009-03-31 TR TR2018/08032T patent/TR201808032T4/tr unknown
- 2009-03-31 EA EA201001565A patent/EA031547B1/ru not_active IP Right Cessation
- 2009-03-31 EP EP16156441.4A patent/EP3061744B1/en not_active Revoked
- 2009-03-31 PT PT161564414T patent/PT3061744T/pt unknown
Also Published As
| Publication number | Publication date |
|---|---|
| EP2257522A1 (en) | 2010-12-08 |
| EA031547B1 (ru) | 2019-01-31 |
| PL3061744T3 (pl) | 2018-10-31 |
| CA2719754A1 (en) | 2009-08-27 |
| EP3061744A1 (en) | 2016-08-31 |
| US8183410B2 (en) | 2012-05-22 |
| WO2009103822A1 (en) | 2009-08-27 |
| US20110054215A1 (en) | 2011-03-03 |
| MX2010010779A (es) | 2010-12-21 |
| PL2257522T3 (pl) | 2016-09-30 |
| TR201808032T4 (tr) | 2018-06-21 |
| EP3061744B1 (en) | 2018-05-09 |
| EP2257522B1 (en) | 2016-03-23 |
| PT3061744T (pt) | 2018-06-19 |
| CA2719754C (en) | 2017-02-14 |
| BRPI0911375A2 (pt) | 2015-12-29 |
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