EA200400736A1 - Способ извлечения капролактама - Google Patents

Способ извлечения капролактама

Info

Publication number
EA200400736A1
EA200400736A1 EA200400736A EA200400736A EA200400736A1 EA 200400736 A1 EA200400736 A1 EA 200400736A1 EA 200400736 A EA200400736 A EA 200400736A EA 200400736 A EA200400736 A EA 200400736A EA 200400736 A1 EA200400736 A1 EA 200400736A1
Authority
EA
Eurasian Patent Office
Prior art keywords
caprolactam
lactams
water
light
product containing
Prior art date
Application number
EA200400736A
Other languages
English (en)
Other versions
EA007536B1 (ru
Inventor
Теодорус Мария Сметс
Герардус Вилхелмус Адрианус Хангкс
Original Assignee
ДСМ Ай Пи ЭССЕТС Б.В.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ДСМ Ай Пи ЭССЕТС Б.В. filed Critical ДСМ Ай Пи ЭССЕТС Б.В.
Publication of EA200400736A1 publication Critical patent/EA200400736A1/ru
Publication of EA007536B1 publication Critical patent/EA007536B1/ru

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D223/00—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom
    • C07D223/02—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings
    • C07D223/06—Heterocyclic compounds containing seven-membered rings having one nitrogen atom as the only ring hetero atom not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D223/08—Oxygen atoms
    • C07D223/10—Oxygen atoms attached in position 2
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/16—Separation or purification
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
    • B01D3/146—Multiple effect distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0033—Other features
    • B01D5/0036—Multiple-effect condensation; Fractional condensation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Other In-Based Heterocyclic Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyrrole Compounds (AREA)
  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
  • Processing Of Solid Wastes (AREA)
  • Polyamides (AREA)

Abstract

Изобретение относится к способу извлечения капролактама из смеси, содержащей капролактам, воду, легкие и тяжелые компоненты, путем проведения первой вакуумной перегонки смеси, приводящей в результате к получению первого кубового продукта, содержащего тяжелые компоненты и капролактам, и первого дистиллятного продукта, содержащего капролактам, воду, ненасыщенные лактамы и легкие компоненты; и проведения, по меньшей мере, для части ненасыщенных лактамов гидрирования.Международная заявка была опубликована вместе с отчетом о международном поиске.
EA200400736A 2001-11-26 2002-11-25 Способ извлечения капролактама EA007536B1 (ru)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
NL1019432 2001-11-26
PCT/NL2002/000761 WO2003045911A1 (en) 2001-11-26 2002-11-25 Process for recovering caprolactam

Publications (2)

Publication Number Publication Date
EA200400736A1 true EA200400736A1 (ru) 2004-10-28
EA007536B1 EA007536B1 (ru) 2006-10-27

Family

ID=19774344

Family Applications (1)

Application Number Title Priority Date Filing Date
EA200400736A EA007536B1 (ru) 2001-11-26 2002-11-25 Способ извлечения капролактама

Country Status (15)

Country Link
US (1) US7141668B2 (ru)
EP (1) EP1448518A1 (ru)
JP (1) JP2005510562A (ru)
KR (1) KR20040063970A (ru)
CN (1) CN1277818C (ru)
AU (1) AU2002347653A1 (ru)
BR (1) BR0214414A (ru)
CO (1) CO5590953A2 (ru)
CZ (1) CZ2004622A3 (ru)
EA (1) EA007536B1 (ru)
MX (1) MXPA04004955A (ru)
MY (1) MY132420A (ru)
PL (1) PL370209A1 (ru)
TW (1) TW200408623A (ru)
WO (1) WO2003045911A1 (ru)

Families Citing this family (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE10253094A1 (de) * 2002-11-13 2004-05-27 Basf Ag Verfahren zur Reinigung von Caprolactam
DE602004009173T2 (de) 2003-05-23 2008-06-26 Dsm Ip Assets B.V. Verfahren zur herstellung von caprolactam durch mischen von cyclohexanonoxim mit einer reaktionsmischung unter turbulenten strömungsbedingungen
MXPA06001028A (es) * 2003-07-25 2006-04-27 Dsm Ip Assets Bv Procesos para purificar caprolactamas.
JP4755829B2 (ja) * 2005-01-11 2011-08-24 花王株式会社 ピロリジン誘導体の製造方法
JP4983041B2 (ja) * 2006-02-21 2012-07-25 住友化学株式会社 カプロラクタムの精製方法
EP2123767A1 (en) * 2008-05-20 2009-11-25 DSM IP Assets B.V. Preparation of epsilon-caprolactam via lysine cyclisation
EP2123768A1 (en) * 2008-05-20 2009-11-25 DSM IP Assets B.V. Preparation of (Z)-6,7-dihydro-1H-azepin-2(5H)-one
TW201000635A (en) * 2008-05-20 2010-01-01 Dsm Ip Assets Bv Preparation of epsilon-caprolactam from (Z)-6,7-dihydro-1H-azepin-2(5H)-one
US8540870B2 (en) * 2009-06-25 2013-09-24 Uop Llc Process for separating pitch from slurry hydrocracked vacuum gas oil
US8202480B2 (en) * 2009-06-25 2012-06-19 Uop Llc Apparatus for separating pitch from slurry hydrocracked vacuum gas oil
JP6003755B2 (ja) * 2012-12-19 2016-10-05 東レ株式会社 ラクタムの精製方法
US8841445B2 (en) 2012-12-19 2014-09-23 Basf Se Process for preparing purified caprolactam from the Beckmann rearrangement of cyclohexane oxime
DE102013107238A1 (de) * 2013-07-09 2015-01-15 L'Air Liquide, Société Anonyme pour l'Etude et l'Exploitation des Procédés Georges Claude Verfahren zur Rückgewinnung von Epsilon-Caprolactam aus Extraktwasser
CA2962917C (en) * 2014-10-29 2019-04-30 Dong-A St Co., Ltd. Novel pyridopyrimidinone compounds for modulating the catalytic activity of histone lysine demethylases (kdms)

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL8102280A (nl) * 1981-05-09 1982-12-01 Stamicarbon Werkwijze voor het zuiveren van epsilon-caprolactam.
NL8303028A (nl) * 1983-08-31 1985-03-18 Stamicarbon Winning van caprolactam uit caprolactam-bevattend destillatie-residu.
DE3735054A1 (de) * 1987-10-16 1989-04-27 Basf Ag Verfahren zur gewinnung von caprolactam aus leichtsiedern oder schwersiedern der caprolactamdestillation oder gemischen derselben

Also Published As

Publication number Publication date
BR0214414A (pt) 2004-09-14
MXPA04004955A (es) 2004-08-11
EA007536B1 (ru) 2006-10-27
MY132420A (en) 2007-10-31
WO2003045911A1 (en) 2003-06-05
CN1596245A (zh) 2005-03-16
US20050176954A1 (en) 2005-08-11
AU2002347653A1 (en) 2003-06-10
US7141668B2 (en) 2006-11-28
PL370209A1 (en) 2005-05-16
TW200408623A (en) 2004-06-01
CN1277818C (zh) 2006-10-04
KR20040063970A (ko) 2004-07-15
JP2005510562A (ja) 2005-04-21
CZ2004622A3 (cs) 2004-10-13
CO5590953A2 (es) 2005-12-30
EP1448518A1 (en) 2004-08-25

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Legal Events

Date Code Title Description
MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): AM AZ KZ KG MD TJ TM

MM4A Lapse of a eurasian patent due to non-payment of renewal fees within the time limit in the following designated state(s)

Designated state(s): BY RU