DK3727688T3 - Katalysatorsystem og fremgangsmåde til fremstilling af dimethylether - Google Patents

Katalysatorsystem og fremgangsmåde til fremstilling af dimethylether Download PDF

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Publication number
DK3727688T3
DK3727688T3 DK18825690.3T DK18825690T DK3727688T3 DK 3727688 T3 DK3727688 T3 DK 3727688T3 DK 18825690 T DK18825690 T DK 18825690T DK 3727688 T3 DK3727688 T3 DK 3727688T3
Authority
DK
Denmark
Prior art keywords
catalyst system
production procedure
dimethylether
dimethylether production
procedure
Prior art date
Application number
DK18825690.3T
Other languages
English (en)
Inventor
Sabine Schuster
Ekkehard Schwab
Stefan Altwasser
Harry Kaiser
Stephan A Schunk
Manuela Gaab
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Application granted granted Critical
Publication of DK3727688T3 publication Critical patent/DK3727688T3/da

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Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/024—Multiple impregnation or coating
    • B01J37/0244—Coatings comprising several layers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/40—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively
    • B01J29/42—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of the pentasil type, e.g. types ZSM-5, ZSM-8 or ZSM-11, as exemplified by patent documents US3702886, GB1334243 and US3709979, respectively containing iron group metals, noble metals or copper
    • B01J29/46—Iron group metals or copper
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0063—Granulating
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
    • C07C41/01—Preparation of ethers
    • C07C41/09—Preparation of ethers by dehydration of compounds containing hydroxy groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C43/00—Ethers; Compounds having groups, groups or groups
    • C07C43/02—Ethers
    • C07C43/03—Ethers having all ether-oxygen atoms bound to acyclic carbon atoms
    • C07C43/04—Saturated ethers
    • C07C43/043—Dimethyl ether
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2529/00—Catalysts comprising molecular sieves
    • C07C2529/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites, pillared clays
    • C07C2529/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • C07C2529/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups C07C2529/08 - C07C2529/65
    • C07C2529/72—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups C07C2529/08 - C07C2529/65 containing iron group metals, noble metals or copper
    • C07C2529/76—Iron group metals or copper

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DK18825690.3T 2017-12-20 2018-12-20 Katalysatorsystem og fremgangsmåde til fremstilling af dimethylether DK3727688T3 (da)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP17208927 2017-12-20
PCT/EP2018/086095 WO2019122078A1 (en) 2017-12-20 2018-12-20 Catalyst system and process for preparing dimethyl ether

Publications (1)

Publication Number Publication Date
DK3727688T3 true DK3727688T3 (da) 2022-04-25

Family

ID=60781795

Family Applications (1)

Application Number Title Priority Date Filing Date
DK18825690.3T DK3727688T3 (da) 2017-12-20 2018-12-20 Katalysatorsystem og fremgangsmåde til fremstilling af dimethylether

Country Status (8)

Country Link
US (1) US11529616B2 (da)
EP (1) EP3727688B1 (da)
JP (1) JP2021508286A (da)
CN (1) CN111491732A (da)
CA (1) CA3086707A1 (da)
DK (1) DK3727688T3 (da)
RU (1) RU2020123775A (da)
WO (1) WO2019122078A1 (da)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP4194433A1 (de) 2021-12-07 2023-06-14 Linde GmbH Verfahren und anlage zur herstellung von dimethylether
EP4194432A1 (de) * 2021-12-07 2023-06-14 Linde GmbH Reaktor und verfahren zur herstellung von methanolfolgeprodukten und insbesondere dimethylether
EP4257579A1 (de) * 2022-04-07 2023-10-11 Linde GmbH Verfahren und anlage zur herstellung von dimethylether

Family Cites Families (26)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA2053615C (en) 1990-10-24 1999-02-02 Thomas H. Hsuing Liquid phase process for dimethyl ether synthesis
JP2976716B2 (ja) * 1992-08-25 1999-11-10 工業技術院長 メタノール合成用触媒及びその製造方法
DK0721799T3 (da) * 1995-01-11 2000-05-01 United Catalysts Inc Aktiveret og stabiliseret kobberoxid- og zinkoxidkatalysator og fremgangsmåde til fremstilling heraf
JP3421902B2 (ja) * 1996-05-22 2003-06-30 ジェイエフイーホールディングス株式会社 ジメチルエーテルの製造方法
JPH09276689A (ja) * 1996-04-19 1997-10-28 Nkk Corp スラリー床反応器
US6147125A (en) 1996-05-13 2000-11-14 Nkk Corporation Method and apparatus for producing dimethyl ether
JP3916715B2 (ja) * 1996-12-26 2007-05-23 ジェイエフイーホールディングス株式会社 ジメチルエーテルの製造方法
DE10111198A1 (de) 2001-03-08 2002-09-19 Basf Ag Methanolreformierungskatalysator mit verringertem Volumenschwund
US6638892B1 (en) 2002-04-18 2003-10-28 Conocophillips Company Syngas conversion and catalyst system employed therefor
KR100454091B1 (ko) * 2002-12-11 2004-10-26 한국화학연구원 미정제 메탄올로부터 디메틸에테르의 제조방법
KR100629939B1 (ko) * 2004-10-15 2006-09-28 에스케이 주식회사 단열반응기에서 미정제 메탄올로부터 디메틸에테르의제조방법
CN100566831C (zh) 2005-06-22 2009-12-09 中国石油化工股份有限公司 用于合成气制取二甲醚的催化剂
KR100812099B1 (ko) * 2006-11-28 2008-03-12 한국가스공사 디메틸에테르 제조용 혼합촉매, 이의 제조방법 및 이를 이용한 디메틸에테르 제조방법
EP1932592A1 (en) * 2006-12-13 2008-06-18 Casale Chemicals S.A. Process and catalyst for the production of dimethylether
CN101497043A (zh) * 2008-02-01 2009-08-05 北京石油化工学院 制备液化石油气所用的催化剂及其制备方法
JP5258617B2 (ja) * 2009-02-23 2013-08-07 三井化学株式会社 銅系触媒の製造方法
CN102950021B (zh) * 2011-08-30 2014-11-26 中国科学院大连化学物理研究所 一种用于浆态床反应的生物质合成气合成二甲醚催化剂
US20130211147A1 (en) * 2011-09-02 2013-08-15 Michael Cheiky Low pressure dimethyl ether synthesis catalyst
US9610568B2 (en) 2012-02-15 2017-04-04 Basf Se Catalytically active body for the synthesis of dimethyl ether from synthesis gas
US9393555B2 (en) * 2012-02-15 2016-07-19 Basf Se Catalytically active body for the synthesis of dimethyl ether from synthesis gas
US9295978B2 (en) * 2012-02-15 2016-03-29 Basf Corporation Catalyst and method for the direct synthesis of dimethyl ether from synthesis gas
CA2870222A1 (en) 2012-04-24 2013-10-31 Basf Se Catalytically active body for the synthesis of dimethyl ether from synthesis gas
US9296665B2 (en) * 2012-12-13 2016-03-29 Pioneer Energy Inc. Synthesis of drop-in liquid fuels and chemicals from methanol, ethanol or syngas using mixed catalysts
RU2528409C1 (ru) 2013-02-21 2014-09-20 Федеральное государственное бюджетное учреждение науки Ордена Трудового Красного Знамени Институт нефтехимического синтеза им. А.В. Топчиева Российской академии наук (ИНХС РАН) Способ получения диметилового эфира методом одностадийного синтеза и его выделения
WO2014174107A1 (en) * 2013-04-26 2014-10-30 Bp P.L.C. Production of hydrocarbons from synthesis gas
WO2015095201A1 (en) * 2013-12-16 2015-06-25 Cool Planet Energy Systems, Inc. Low pressure dimethyl ether synthesis catalyst

Also Published As

Publication number Publication date
EP3727688B1 (en) 2022-02-16
CA3086707A1 (en) 2019-06-27
US11529616B2 (en) 2022-12-20
RU2020123775A (ru) 2022-01-20
WO2019122078A1 (en) 2019-06-27
CN111491732A (zh) 2020-08-04
US20200316570A1 (en) 2020-10-08
JP2021508286A (ja) 2021-03-04
EP3727688A1 (en) 2020-10-28

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DK3727688T3 (da) Katalysatorsystem og fremgangsmåde til fremstilling af dimethylether