DE69705292D1 - Iridium-katalysiertes Carbonylierungsverfahren zur Herstellung von Essigsäure - Google Patents

Iridium-katalysiertes Carbonylierungsverfahren zur Herstellung von Essigsäure

Info

Publication number
DE69705292D1
DE69705292D1 DE69705292T DE69705292T DE69705292D1 DE 69705292 D1 DE69705292 D1 DE 69705292D1 DE 69705292 T DE69705292 T DE 69705292T DE 69705292 T DE69705292 T DE 69705292T DE 69705292 D1 DE69705292 D1 DE 69705292D1
Authority
DE
Germany
Prior art keywords
iridium
production
acetic acid
carbonylation process
catalyzed carbonylation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69705292T
Other languages
English (en)
Other versions
DE69705292T2 (de
Inventor
Evert Jan Ditzel
John Glenn Sunley
Robert John Watt
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BP Chemicals Ltd
Original Assignee
BP Chemicals Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BP Chemicals Ltd filed Critical BP Chemicals Ltd
Application granted granted Critical
Publication of DE69705292D1 publication Critical patent/DE69705292D1/de
Publication of DE69705292T2 publication Critical patent/DE69705292T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/10—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide
    • C07C51/12—Preparation of carboxylic acids or their salts, halides or anhydrides by reaction with carbon monoxide on an oxygen-containing group in organic compounds, e.g. alcohols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE69705292T 1996-12-19 1997-12-11 Iridium-katalysiertes Carbonylierungsverfahren zur Herstellung von Essigsäure Expired - Fee Related DE69705292T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GBGB9626429.6A GB9626429D0 (en) 1996-12-19 1996-12-19 Process

Publications (2)

Publication Number Publication Date
DE69705292D1 true DE69705292D1 (de) 2001-07-26
DE69705292T2 DE69705292T2 (de) 2001-10-11

Family

ID=10804718

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69705292T Expired - Fee Related DE69705292T2 (de) 1996-12-19 1997-12-11 Iridium-katalysiertes Carbonylierungsverfahren zur Herstellung von Essigsäure

Country Status (19)

Country Link
US (1) US5877348A (de)
EP (1) EP0849248B1 (de)
JP (1) JP4071333B2 (de)
KR (1) KR19980064382A (de)
CN (1) CN1117059C (de)
AR (1) AR010832A1 (de)
BR (1) BR9706621A (de)
CA (1) CA2225137C (de)
DE (1) DE69705292T2 (de)
GB (1) GB9626429D0 (de)
ID (1) ID19237A (de)
MY (1) MY128193A (de)
NO (1) NO975919L (de)
RU (1) RU2184724C2 (de)
SA (2) SA98190164B1 (de)
SG (1) SG55440A1 (de)
TW (1) TW462962B (de)
UA (1) UA51653C2 (de)
ZA (1) ZA9711273B (de)

Families Citing this family (91)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB9626324D0 (en) * 1996-12-19 1997-02-05 Bp Chem Int Ltd Process
US6211405B1 (en) * 1998-10-23 2001-04-03 Celanese International Corporation Addition of iridium to the rhodium/inorganic iodide catalyst system
US6552221B1 (en) 1998-12-18 2003-04-22 Millenium Petrochemicals, Inc. Process control for acetic acid manufacture
US6137000A (en) * 1999-02-16 2000-10-24 Eastman Chemical Company Method for carbonylation of lower aliphatic alcohols using a supported iridium and lanthanide series catalyst
DE19917681C2 (de) * 1999-04-19 2003-02-27 Heraeus Gmbh W C Verfahren zur Herstellung von Iridiumacetat
US6274096B1 (en) 1999-11-01 2001-08-14 Acetex (Cyprus) Limited Methanol plant retrofit
US6232352B1 (en) 1999-11-01 2001-05-15 Acetex Limited Methanol plant retrofit for acetic acid manufacture
US6781014B1 (en) 1999-11-01 2004-08-24 Acetex (Cyprus) Limited Methanol plant retrofit for manufacture of acetic acid
US6458995B1 (en) 2000-03-31 2002-10-01 Celanese International Corporation Catalytic composition for carbonylation including iridium and pyridine polymers
KR20030016370A (ko) * 2000-07-06 2003-02-26 밀레니엄 페트로케미칼스 인코포레이티드 초산 제조를 위한 공정 제어 방법
US6627770B1 (en) 2000-08-24 2003-09-30 Celanese International Corporation Method and apparatus for sequesting entrained and volatile catalyst species in a carbonylation process
US6531630B2 (en) 2000-12-29 2003-03-11 Kenneth Ebenes Vidalin Bimodal acetic acid manufacture
GB0211560D0 (en) * 2002-05-20 2002-06-26 Bp Chem Int Ltd Process
GB0213485D0 (en) * 2002-06-12 2002-07-24 Bp Chem Int Ltd Process
GB0221800D0 (en) 2002-09-19 2002-10-30 Bp Chem Int Ltd Process
GB0222618D0 (en) * 2002-09-30 2002-11-06 Bp Chem Int Ltd Process
US6846951B1 (en) 2003-10-09 2005-01-25 Acetex (Cyprus) Limited Integrated process for acetic acid and methanol
MY146697A (en) 2004-07-09 2012-09-14 Acetex Cyprus Ltd Preparation of syngas for acetic acid synthesis by partial oxidation of methanol feedstock
CA2496839A1 (en) 2004-07-19 2006-01-19 Woodland Chemical Systems Inc. Process for producing ethanol from synthesis gas rich in carbon monoxide
CN100443173C (zh) * 2004-11-22 2008-12-17 中国科学院化学研究所 甲醇合成乙酸或乙酸甲酯合成乙酐的催化剂体系及应用
GB0601865D0 (en) * 2006-01-30 2006-03-08 Bp Chem Int Ltd Process
TWI465424B (zh) 2006-03-21 2014-12-21 Bp Chem Int Ltd 製造醋酸的方法
EA013194B1 (ru) * 2006-04-05 2010-02-26 Вудлэнд Байофьюэлс Инк. Способ получения этанола
GB0607395D0 (en) * 2006-04-12 2006-05-24 Bp Chem Int Ltd Process
DE102007014914B4 (de) * 2007-03-26 2013-09-12 Heraeus Precious Metals Gmbh & Co. Kg Katalytisch hochwirksame Edelmetall-Carboxylat-Verbindungen von Ir, Ru, Rh, Pd, Pt und Au
US7902398B2 (en) 2007-04-25 2011-03-08 Celanese International Corporation Method and apparatus for carbonylation with reduced catalyst loss
US7989659B2 (en) 2007-05-17 2011-08-02 Celanese International Corporation Method and apparatus for making acetic acid with improved light ends column productivity
US7619113B2 (en) * 2007-09-27 2009-11-17 Celanese International Corporation Method and apparatus for making acetic acid with improved purification
US7902397B2 (en) * 2007-10-11 2011-03-08 Celanese International Corporation Method and apparatus for making acetic acid with improved productivity
US7820855B2 (en) 2008-04-29 2010-10-26 Celanese International Corporation Method and apparatus for carbonylating methanol with acetic acid enriched flash stream
US8318977B2 (en) 2008-04-29 2012-11-27 Celanese International Corporation Methanol carbonylation system having absorber with multiple solvent options
US7884237B2 (en) 2008-11-07 2011-02-08 Celanese International Corp. Methanol carbonylation with improved aldehyde removal
US8168822B2 (en) 2009-07-07 2012-05-01 Celanese International Corporation Acetic acid production by way of carbonylation with enhanced reaction and flashing
US8455685B2 (en) 2009-07-07 2013-06-04 Celanese International Corporation Acetic anhydride production by way of carbonylation with enhanced reaction and flashing
CN102093196B (zh) * 2009-12-15 2013-03-06 上海吴泾化工有限公司 一种链烷醇和/或其活性衍生物的羰基化制备羧酸的方法
CN102093198B (zh) * 2009-12-15 2012-12-05 上海吴泾化工有限公司 一种生产乙酸的方法
WO2012039841A1 (en) 2010-02-02 2012-03-29 Celanese International Corporation Integrated process for producing alcohols from a mixed acid feed
US8575403B2 (en) 2010-05-07 2013-11-05 Celanese International Corporation Hydrolysis of ethyl acetate in ethanol separation process
US8932372B2 (en) 2010-02-02 2015-01-13 Celanese International Corporation Integrated process for producing alcohols from a mixed acid feed
US8569551B2 (en) 2010-05-07 2013-10-29 Celanese International Corporation Alcohol production process integrating acetic acid feed stream comprising water from carbonylation process
US8710279B2 (en) 2010-07-09 2014-04-29 Celanese International Corporation Hydrogenolysis of ethyl acetate in alcohol separation processes
US8859827B2 (en) 2011-11-18 2014-10-14 Celanese International Corporation Esterifying acetic acid to produce ester feed for hydrogenolysis
WO2012148509A1 (en) 2011-04-26 2012-11-01 Celanese International Corporation Process for producing ethanol using a stacked bed reactor
US9272970B2 (en) 2010-07-09 2016-03-01 Celanese International Corporation Hydrogenolysis of ethyl acetate in alcohol separation processes
US8664454B2 (en) 2010-07-09 2014-03-04 Celanese International Corporation Process for production of ethanol using a mixed feed using copper containing catalyst
US8378141B2 (en) 2010-08-16 2013-02-19 Celanese International Corporation Process and system for supplying vapor from drying column to light ends column
US8530696B2 (en) 2010-09-24 2013-09-10 Celanese International Corporation Pump around reactor for production of acetic acid
US8877963B2 (en) 2010-09-28 2014-11-04 Celanese International Corporation Production of acetic acid with high conversion rate
US8394988B2 (en) 2010-09-28 2013-03-12 Celanese International Corporation Production of acetic acid with high conversion rate
US8461379B2 (en) 2010-10-12 2013-06-11 Celanese International Corporation Production of acetic acid comprising feeding at least one reactant to a recycle stream
BR112013009012A2 (pt) 2010-10-13 2016-07-12 Celanese Int Corp processo para a recuperação de promotores de halogêneo e romoção de compostos redutores de permanganato
CN101973866B (zh) * 2010-10-27 2013-04-24 上海华谊（集团）公司 一种羰化合成丙酸的制备方法
US8637698B2 (en) 2010-11-19 2014-01-28 Celanese International Corporation Production of acetic acid with an increased production rate
KR101879006B1 (ko) * 2010-12-15 2018-07-16 주식회사 다이셀 아세트산의 제조 방법
US8563773B2 (en) 2010-12-16 2013-10-22 Celanese International Corporation Eductor-based reactor and pump around loops for production of acetic acid
WO2012149137A1 (en) 2011-04-26 2012-11-01 Celanese International Corporation Process for the production of ethanol from an acetic acid feed and a recycled ethyl acetate feed
US9073816B2 (en) 2011-04-26 2015-07-07 Celanese International Corporation Reducing ethyl acetate concentration in recycle streams for ethanol production processes
US8884081B2 (en) 2011-04-26 2014-11-11 Celanese International Corporation Integrated process for producing acetic acid and alcohol
US8686199B2 (en) 2011-04-26 2014-04-01 Celanese International Corporation Process for reducing the concentration of acetic acid in a crude alcohol product
US8754268B2 (en) 2011-04-26 2014-06-17 Celanese International Corporation Process for removing water from alcohol mixtures
US8592635B2 (en) 2011-04-26 2013-11-26 Celanese International Corporation Integrated ethanol production by extracting halides from acetic acid
US8697908B2 (en) 2011-05-05 2014-04-15 Celanese International Corporation Removal of amine compounds from carbonylation process stream containing corrosion metal contaminants
US8952196B2 (en) 2011-05-05 2015-02-10 Celanese International Corporation Removal of aromatics from carbonylation process
US8895786B2 (en) 2011-08-03 2014-11-25 Celanese International Corporation Processes for increasing alcohol production
US9663437B2 (en) 2011-09-13 2017-05-30 Celanese International Corporation Production of acetic acid with high conversion rate
WO2013070209A1 (en) 2011-11-09 2013-05-16 Celanese International Corporation Integrated carbonylation and hydrogenation process to obtain ethanol
US8686201B2 (en) 2011-11-09 2014-04-01 Celanese International Corporation Integrated acid and alcohol production process having flashing to recover acid production catalyst
WO2013070210A1 (en) 2011-11-09 2013-05-16 Celanese International Corporation Integrated carbonylation and hydrogenation process to obtain ethanol having flashing to recover acid production catalyst
US8614359B2 (en) 2011-11-09 2013-12-24 Celanese International Corporation Integrated acid and alcohol production process
US8748673B2 (en) 2011-11-18 2014-06-10 Celanese International Corporation Process of recovery of ethanol from hydrogenolysis process
EP2782891A1 (de) 2011-11-22 2014-10-01 Celanese International Corporation Hydrierung von essigsäure zur herstellung von ethylacetat und reduzierung von ethylacetat zu ethanol
WO2013078207A1 (en) 2011-11-22 2013-05-30 Celanese International Corporation Esterifying an ethanol and acetic acid mixture to produce an ester feed for hydrogenolysis
WO2013089990A1 (en) 2011-12-14 2013-06-20 Celanese International Corporation Phasing reactor product from hydrogenating acetic acid into ethyl acetate feed to produce ethanol
WO2013101304A1 (en) 2011-12-29 2013-07-04 Celanese International Corporation Process for producing ethanol from impure methanol
WO2013119275A1 (en) 2012-02-08 2013-08-15 Celanese International Corporation Production of acetic acid from methanol
US8859810B2 (en) 2012-08-21 2014-10-14 Celanese International Corporation Process for recovering permanganate reducing compounds from an acetic acid production process
WO2014143840A2 (en) 2013-03-15 2014-09-18 Celanese International Corporation Process for separating product gas using carbonylation processes
MX2017004287A (es) 2014-10-02 2017-07-19 Celanese Int Corp Proceso para la produccion de acido acetico.
US9260369B1 (en) 2014-11-14 2016-02-16 Celanese International Corporation Processes for producing acetic acid product having low butyl acetate content
US9302975B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for flashing a reaction medium
US9561994B2 (en) 2015-01-30 2017-02-07 Celanese International Corporation Processes for producing acetic acid
US9487464B2 (en) 2015-01-30 2016-11-08 Celanese International Corporation Processes for producing acetic acid
US9512056B2 (en) 2015-02-04 2016-12-06 Celanese International Corporation Process to control HI concentration in residuum stream
US10413840B2 (en) 2015-02-04 2019-09-17 Celanese International Coporation Process to control HI concentration in residuum stream
US9505696B2 (en) 2015-02-04 2016-11-29 Celanese International Corporation Process to control HI concentration in residuum stream
US9382183B1 (en) 2015-07-01 2016-07-05 Celanese International Corporation Process for flashing a reaction medium
US9302974B1 (en) 2015-07-01 2016-04-05 Celanese International Corporation Process for producing acetic acid
CN108137468B (zh) 2015-10-02 2021-04-13 国际人造丝公司 使用水的再循环生产乙酸的方法
US9957216B2 (en) 2015-11-13 2018-05-01 Celanese International Corporation Processes for producing acetic acid
US9908835B2 (en) 2015-11-13 2018-03-06 Celanese International Corporation Processes for purifying acetic and hydrating anhydride
US20230202957A1 (en) 2020-06-03 2023-06-29 Celanese International Corporation Production and purification of acetic acid

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB8904125D0 (en) * 1989-02-23 1989-04-05 British Petroleum Co Plc Process for preparing carboxylic acids
US5672743A (en) * 1993-09-10 1997-09-30 Bp Chemicals Limited Process for the production of acetic acid
CN1070167C (zh) * 1994-05-13 2001-08-29 派蒂斯艾西提克公司 用基于铱和碘化物的可溶性催化剂制备羧酸或相应酯的方法
GB9503382D0 (en) * 1995-02-21 1995-04-12 Bp Chem Int Ltd Process
US5696284A (en) * 1995-06-21 1997-12-09 Bp Chemicals Limited Process for the carbonylation of alkyl alcohols and/or reactive derivatives thereof

Also Published As

Publication number Publication date
EP0849248B1 (de) 2001-06-20
EP0849248A1 (de) 1998-06-24
JPH10310550A (ja) 1998-11-24
SA98190161B1 (ar) 2006-10-09
TW462962B (en) 2001-11-11
MY128193A (en) 2007-01-31
DE69705292T2 (de) 2001-10-11
KR19980064382A (ko) 1998-10-07
GB9626429D0 (en) 1997-02-05
BR9706621A (pt) 1999-05-18
ID19237A (id) 1998-06-28
CA2225137C (en) 2008-05-20
US5877348A (en) 1999-03-02
CN1117059C (zh) 2003-08-06
UA51653C2 (uk) 2002-12-16
NO975919L (no) 1998-06-22
MX9710438A (es) 1998-09-30
SG55440A1 (en) 1998-12-21
CA2225137A1 (en) 1998-06-19
ZA9711273B (en) 1999-06-15
SA98190164B1 (ar) 2006-10-11
CN1187482A (zh) 1998-07-15
AR010832A1 (es) 2000-07-12
JP4071333B2 (ja) 2008-04-02
NO975919D0 (no) 1997-12-16
RU2184724C2 (ru) 2002-07-10

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee