DE69201978T2 - Verfahren zur Herstellung von Terephthalsäure. - Google Patents
Verfahren zur Herstellung von Terephthalsäure.Info
- Publication number
- DE69201978T2 DE69201978T2 DE69201978T DE69201978T DE69201978T2 DE 69201978 T2 DE69201978 T2 DE 69201978T2 DE 69201978 T DE69201978 T DE 69201978T DE 69201978 T DE69201978 T DE 69201978T DE 69201978 T2 DE69201978 T2 DE 69201978T2
- Authority
- DE
- Germany
- Prior art keywords
- preparation
- terephthalic acid
- terephthalic
- acid
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C63/00—Compounds having carboxyl groups bound to a carbon atoms of six-membered aromatic rings
- C07C63/14—Monocyclic dicarboxylic acids
- C07C63/15—Monocyclic dicarboxylic acids all carboxyl groups bound to carbon atoms of the six-membered aromatic ring
- C07C63/26—1,4 - Benzenedicarboxylic acid
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
- C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
- C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
- C07C51/255—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting
- C07C51/265—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of compounds containing six-membered aromatic rings without ring-splitting having alkyl side chains which are oxidised to carboxyl groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/42—Separation; Purification; Stabilisation; Use of additives
- C07C51/487—Separation; Purification; Stabilisation; Use of additives by treatment giving rise to chemical modification
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/52—Improvements relating to the production of bulk chemicals using catalysts, e.g. selective catalysts
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Heat Treatment Of Water, Waste Water Or Sewage (AREA)
- Treatment Of Water By Oxidation Or Reduction (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
GB919102393A GB9102393D0 (en) | 1991-02-05 | 1991-02-05 | Production of terephthalic acid |
GB9102393 | 1991-02-05 |
Publications (3)
Publication Number | Publication Date |
---|---|
DE69201978D1 DE69201978D1 (de) | 1995-05-18 |
DE69201978T2 true DE69201978T2 (de) | 1995-08-24 |
DE69201978T3 DE69201978T3 (de) | 2005-03-10 |
Family
ID=10689524
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE69201978T Expired - Lifetime DE69201978T3 (de) | 1991-02-05 | 1992-02-03 | Verfahren zur Herstellung von Terephthalsäure. |
Country Status (12)
Country | Link |
---|---|
US (2) | US5304676A (de) |
EP (1) | EP0498591B2 (de) |
JP (1) | JPH0558948A (de) |
KR (1) | KR100214397B1 (de) |
CN (2) | CN1038580C (de) |
CA (1) | CA2059719C (de) |
DE (1) | DE69201978T3 (de) |
ES (1) | ES2070586T5 (de) |
GB (2) | GB9102393D0 (de) |
IN (1) | IN185008B (de) |
MX (1) | MX9200478A (de) |
TW (1) | TW326037B (de) |
Families Citing this family (65)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
GB9104776D0 (en) * | 1991-03-07 | 1991-04-17 | Ici Plc | Process for the production of terephthalic acid |
GB9310070D0 (en) * | 1992-05-29 | 1993-06-30 | Ici Plc | Process for the production of purified terephthalic acid |
GB9303191D0 (en) * | 1993-02-17 | 1993-03-31 | Ici Plc | Separation process |
EG20284A (en) * | 1993-02-17 | 1998-07-30 | Ici Plc | Separation process |
US5612007A (en) * | 1994-10-14 | 1997-03-18 | Amoco Corporation | Apparatus for preparing aromatic carboxylic acids with efficient energy recovery |
CN1163693C (zh) * | 1995-06-05 | 2004-08-25 | 纳幕尔杜邦公司 | 废气处理方法 |
US5961942A (en) * | 1995-06-05 | 1999-10-05 | E. I. Du Pont De Nemours And Company | Effluent gas treatment |
US5929274A (en) | 1995-06-07 | 1999-07-27 | Hfm International, Inc. | Method to reduce carboxybenzaldehyde isomers in terephthalic acid or isophthalic acid |
US6013835A (en) | 1995-06-07 | 2000-01-11 | Hfm International, Inc. | Method and apparatus for preparing purified terephthalic acid |
US5767311A (en) | 1995-06-07 | 1998-06-16 | Glitsch International, Inc. | Method and apparatus for preparing purified terephtalic acid |
US6054610A (en) | 1995-06-07 | 2000-04-25 | Hfm International, Inc. | Method and apparatus for preparing purified terephthalic acid and isophthalic acid from mixed xylenes |
DE69522590T2 (de) * | 1995-12-30 | 2002-07-11 | Sunkyong Ind Ltd | Verfahren zur herstellung von terephthalsäure |
WO1998041478A1 (en) * | 1997-03-14 | 1998-09-24 | E.I. Du Pont De Nemours And Company | Treatment of effluent streams containing organic acids |
GB9705349D0 (en) | 1997-03-14 | 1997-04-30 | Ici Plc | Treatment of effluent streams |
US6137001A (en) * | 1998-02-11 | 2000-10-24 | Bp Amoco Corporation | Process for preparing aromatic carboxylic acids with efficient treatments of gaseous effluent |
US6765113B2 (en) | 2000-07-19 | 2004-07-20 | E.I. Du Pont De Nemours And Company | Production of aromatic carboxylic acids |
WO2002092214A1 (fr) * | 2001-05-15 | 2002-11-21 | Mitsubishi Chemical Corporation | Procede de production d'un compose |
US7485747B2 (en) * | 2001-06-04 | 2009-02-03 | Eastman Chemical Company | Two stage oxidation process for the production of aromatic dicarboxylic acids |
US7196215B2 (en) * | 2001-06-04 | 2007-03-27 | Eastman Chemical Company | Process for the production of purified terephthalic acid |
ITMI20021423A1 (it) * | 2002-06-27 | 2003-12-29 | Eurotecnica Dev & Licensing S | Processo per la separazione dell'acqua prodotta nella ossidazione catalitica di idrocarburi aromatici ad acidi aromatici policarbossilici |
ES2295644T3 (es) * | 2002-07-09 | 2008-04-16 | Invista Technologies S.A.R.L. | Procedimiento para producir acidos dicarboxilicos aromaticos en condiciones supercriticas. |
AU2003289482A1 (en) * | 2003-01-07 | 2004-07-29 | Mitsubishi Chemical Corporation | Process for producing high-purity terephthalic acid |
CN100453517C (zh) * | 2003-01-10 | 2009-01-21 | 三菱化学株式会社 | 芳香羧酸的制备方法和对苯二甲酸的制备方法 |
US20050256335A1 (en) * | 2004-05-12 | 2005-11-17 | Ovidiu Marin | Providing gases to aromatic carboxylic acid manufacturing processes |
CN1960961B (zh) * | 2004-05-28 | 2011-06-22 | 三菱化学株式会社 | 高纯度对苯二甲酸的制造方法 |
US7572936B2 (en) | 2004-09-02 | 2009-08-11 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7692036B2 (en) | 2004-11-29 | 2010-04-06 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7608733B2 (en) * | 2004-09-02 | 2009-10-27 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7399882B2 (en) * | 2004-09-02 | 2008-07-15 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7495125B2 (en) * | 2004-09-02 | 2009-02-24 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7381836B2 (en) * | 2004-09-02 | 2008-06-03 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7586000B2 (en) * | 2004-09-02 | 2009-09-08 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7589231B2 (en) * | 2004-09-02 | 2009-09-15 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7582793B2 (en) | 2004-09-02 | 2009-09-01 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7910769B2 (en) * | 2004-09-02 | 2011-03-22 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7390921B2 (en) * | 2004-09-02 | 2008-06-24 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7608732B2 (en) * | 2005-03-08 | 2009-10-27 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7683210B2 (en) * | 2004-09-02 | 2010-03-23 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7361784B2 (en) * | 2004-09-02 | 2008-04-22 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7572932B2 (en) * | 2004-09-02 | 2009-08-11 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US20060047153A1 (en) * | 2004-09-02 | 2006-03-02 | Wonders Alan G | Optimized liquid-phase oxidation |
US7615663B2 (en) * | 2004-09-02 | 2009-11-10 | Eastman Chemical Company | Optimized production of aromatic dicarboxylic acids |
US7568361B2 (en) * | 2004-09-02 | 2009-08-04 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7504535B2 (en) | 2004-09-02 | 2009-03-17 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7371894B2 (en) * | 2004-09-02 | 2008-05-13 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7507857B2 (en) * | 2004-09-02 | 2009-03-24 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7482482B2 (en) * | 2004-09-02 | 2009-01-27 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7692037B2 (en) * | 2004-09-02 | 2010-04-06 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7741515B2 (en) * | 2004-09-02 | 2010-06-22 | Eastman Chemical Company | Optimized liquid-phase oxidation |
DE602006015446D1 (de) * | 2005-03-21 | 2010-08-26 | Bp Corp North America Inc | Verfahren und vorrichtung zur herstellung aromatischer carboxyl-säuren einschliesslich reiner formen davon |
BRPI0609572A2 (pt) * | 2005-03-22 | 2010-04-20 | Mitsubishi Chem Corp | processo para a produção de ácido tereftálico de alta pureza |
US7884232B2 (en) * | 2005-06-16 | 2011-02-08 | Eastman Chemical Company | Optimized liquid-phase oxidation |
US7402694B2 (en) * | 2005-08-11 | 2008-07-22 | Eastman Chemical Company | Process for removal of benzoic acid from an oxidizer purge stream |
US7358389B2 (en) * | 2006-01-04 | 2008-04-15 | Eastman Chemical Company | Oxidation system employing internal structure for enhanced hydrodynamics |
US7355068B2 (en) * | 2006-01-04 | 2008-04-08 | Eastman Chemical Company | Oxidation system with internal secondary reactor |
CN100368370C (zh) * | 2006-03-29 | 2008-02-13 | 中国石化仪征化纤股份有限公司 | 对二甲苯氧化母液中悬浮物的回收***装置 |
CN101152969B (zh) * | 2006-09-29 | 2011-01-19 | 中国石油化工股份有限公司石油化工科学研究院 | 对苯二甲酸生产废水的处理方法 |
WO2009141968A1 (ja) * | 2008-05-20 | 2009-11-26 | 株式会社日立プラントテクノロジー | 精製テレフタル酸分離母液の処理方法 |
CN102421741B (zh) | 2009-04-24 | 2014-03-26 | 英威达技术有限公司 | 用于处理、纯化粗对苯二甲酸及相关过程流的方法、步骤及*** |
KR101975177B1 (ko) | 2011-08-16 | 2019-05-07 | 푸락 바이오켐 비.브이. | 발효 브로스 후처리에 유용한, 염산을 사용하는 침전에 의한 카복실산 마그네슘염으로부터의 카복실산의 회수 |
US9376364B2 (en) | 2011-08-16 | 2016-06-28 | Purac Biochem B.V. | Acid/salt separation |
CN102798679B (zh) * | 2012-09-03 | 2014-01-15 | 绍兴汉青环保科技有限公司 | 一种pta 生产装置气体中有机物的气相色谱分析方法 |
CA2933721A1 (en) | 2013-12-18 | 2015-06-25 | Bp Corporation North America Inc. | Improved process and apparatus for manufacturing aromatic carboxylic acids |
EP3374318B1 (de) | 2015-11-13 | 2021-01-20 | SABIC Global Technologies B.V. | Verfahren mit verwendung von ionenaustauschharzen zur behandlung von abwasser, das aus der herstellung von gereinigter terephtalsäure stammt |
CN113318471B (zh) * | 2021-07-08 | 2024-05-31 | 山东友道化学有限公司 | 二甲苯氧化反应液的处理方法及*** |
Family Cites Families (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2849483A (en) * | 1954-07-30 | 1958-08-26 | Chemstrand Corp | Method of purifying aromatic dicarboxylic acids |
GB970491A (en) * | 1960-10-18 | 1964-09-23 | Standard Oil Co | Production of aromatic carboxylic acids |
GB970492A (en) * | 1960-10-18 | 1964-09-23 | Standard Oil Co | Production of aromatic carboxylic acids |
NL6606774A (de) * | 1965-05-17 | 1966-11-18 | ||
FR1569704A (de) * | 1968-02-26 | 1969-06-06 | ||
US3592847A (en) * | 1968-05-02 | 1971-07-13 | Allied Chem | Process for the purification of terephthalic acid |
GB1373230A (en) * | 1971-12-23 | 1974-11-06 | Mitsui Petrochemical Ind | Process for producing terephthalic acid |
JPS52128344A (en) * | 1976-04-20 | 1977-10-27 | Mitsubishi Gas Chem Co Inc | Preparation of high-purity terephthalic acid |
US4467111A (en) * | 1981-10-29 | 1984-08-21 | Standard Oil Company (Indiana) | Process for purification of crude terephthalic acid |
US5166420A (en) * | 1986-10-20 | 1992-11-24 | Mitsui Petrochemical Industries, Ltd. | Process for the production of high purity terephthalic acid |
US4933492A (en) * | 1988-10-13 | 1990-06-12 | Amoco Corporation | Purification of crude isophthalic acid |
-
1991
- 1991-02-05 GB GB919102393A patent/GB9102393D0/en active Pending
-
1992
- 1992-01-30 CA CA002059719A patent/CA2059719C/en not_active Expired - Lifetime
- 1992-01-30 US US07/827,205 patent/US5304676A/en not_active Ceased
- 1992-02-01 KR KR1019920001597A patent/KR100214397B1/ko not_active IP Right Cessation
- 1992-02-03 ES ES92300888T patent/ES2070586T5/es not_active Expired - Lifetime
- 1992-02-03 DE DE69201978T patent/DE69201978T3/de not_active Expired - Lifetime
- 1992-02-03 CN CN92101420A patent/CN1038580C/zh not_active Ceased
- 1992-02-03 EP EP92300888A patent/EP0498591B2/de not_active Expired - Lifetime
- 1992-02-03 GB GB929202241A patent/GB9202241D0/en active Pending
- 1992-02-03 IN IN75DE1992 patent/IN185008B/en unknown
- 1992-02-04 MX MX9200478A patent/MX9200478A/es unknown
- 1992-02-05 JP JP4019980A patent/JPH0558948A/ja active Pending
- 1992-02-26 TW TW081101427A patent/TW326037B/zh active
-
1996
- 1996-04-19 US US08/634,991 patent/USRE36008E/en not_active Expired - Lifetime
- 1996-08-15 CN CN96109973A patent/CN1130328C/zh not_active Expired - Fee Related
Also Published As
Publication number | Publication date |
---|---|
TW326037B (en) | 1998-02-01 |
USRE36008E (en) | 1998-12-22 |
KR100214397B1 (ko) | 1999-08-02 |
CA2059719A1 (en) | 1992-08-06 |
KR920016399A (ko) | 1992-09-24 |
DE69201978T3 (de) | 2005-03-10 |
US5304676A (en) | 1994-04-19 |
CN1130328C (zh) | 2003-12-10 |
EP0498591B2 (de) | 2004-10-13 |
DE69201978D1 (de) | 1995-05-18 |
EP0498591B1 (de) | 1995-04-12 |
GB9102393D0 (en) | 1991-03-20 |
JPH0558948A (ja) | 1993-03-09 |
IN185008B (de) | 2000-10-21 |
GB9202241D0 (en) | 1992-03-18 |
ES2070586T3 (es) | 1995-06-01 |
MX9200478A (es) | 1992-08-01 |
CN1064675A (zh) | 1992-09-23 |
EP0498591A2 (de) | 1992-08-12 |
CA2059719C (en) | 2002-10-08 |
ES2070586T5 (es) | 2005-05-01 |
CN1150944A (zh) | 1997-06-04 |
EP0498591A3 (en) | 1993-01-27 |
CN1038580C (zh) | 1998-06-03 |
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Legal Events
Date | Code | Title | Description |
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8363 | Opposition against the patent | ||
8328 | Change in the person/name/address of the agent |
Free format text: DERZEIT KEIN VERTRETER BESTELLT |
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8327 | Change in the person/name/address of the patent owner |
Owner name: E.I. DU PONT DE NEMOURS AND CO., WILMINGTON, DEL., |
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8328 | Change in the person/name/address of the agent |
Free format text: R.A. KUHNEN & P.A. WACKER PATENTANWALTSGESELLSCHAFT MBH, 85354 FREISING |
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8366 | Restricted maintained after opposition proceedings | ||
8327 | Change in the person/name/address of the patent owner |
Owner name: ADVANSA BV, HOOFDDORP, NL |
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8328 | Change in the person/name/address of the agent |
Representative=s name: PATENTANWAELTE ZELLENTIN & PARTNER GBR, 80331 MUENCHEN |
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8327 | Change in the person/name/address of the patent owner |
Owner name: LA SEDA DE BARCELONA S.A., BARCELONA, ES |