DE68919566D1 - Verfahren zur Synthese von Rohrzuckerderivaten durch eine regiokselektive Reaktion. - Google Patents
Verfahren zur Synthese von Rohrzuckerderivaten durch eine regiokselektive Reaktion.Info
- Publication number
- DE68919566D1 DE68919566D1 DE68919566T DE68919566T DE68919566D1 DE 68919566 D1 DE68919566 D1 DE 68919566D1 DE 68919566 T DE68919566 T DE 68919566T DE 68919566 T DE68919566 T DE 68919566T DE 68919566 D1 DE68919566 D1 DE 68919566D1
- Authority
- DE
- Germany
- Prior art keywords
- regiocselective
- synthesis
- reaction
- cane sugar
- sugar derivatives
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H11/00—Compounds containing saccharide radicals esterified by inorganic acids; Metal salts thereof
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/04—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
- C07H13/06—Fatty acids
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H13/00—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
- C07H13/02—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
- C07H13/08—Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals directly attached to carbocyclic rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07H—SUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
- C07H23/00—Compounds containing boron, silicon, or a metal, e.g. chelates, vitamin B12
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Biochemistry (AREA)
- Biotechnology (AREA)
- General Health & Medical Sciences (AREA)
- Genetics & Genomics (AREA)
- Molecular Biology (AREA)
- Saccharide Compounds (AREA)
- Steroid Compounds (AREA)
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/220,641 US4950746A (en) | 1988-07-18 | 1988-07-18 | Process for synthesizing sucrose derivatives by regioselective reaction |
Publications (2)
Publication Number | Publication Date |
---|---|
DE68919566D1 true DE68919566D1 (de) | 1995-01-12 |
DE68919566T2 DE68919566T2 (de) | 1995-04-13 |
Family
ID=22824357
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
DE68919566T Expired - Lifetime DE68919566T2 (de) | 1988-07-18 | 1989-07-17 | Verfahren zur Synthese von Rohrzuckerderivaten durch eine regiokselektive Reaktion. |
Country Status (24)
Country | Link |
---|---|
US (1) | US4950746A (de) |
EP (1) | EP0352048B1 (de) |
JP (1) | JP2725710B2 (de) |
KR (1) | KR0143234B1 (de) |
AR (1) | AR245136A1 (de) |
AT (1) | ATE114664T1 (de) |
AU (1) | AU618107B2 (de) |
CA (1) | CA1323625C (de) |
DE (1) | DE68919566T2 (de) |
DK (1) | DK170027B1 (de) |
ES (1) | ES2065386T3 (de) |
FI (1) | FI91874C (de) |
GR (1) | GR1002250B (de) |
IE (1) | IE65990B1 (de) |
IL (1) | IL91004A (de) |
MX (1) | MX172793B (de) |
NO (1) | NO171855C (de) |
NZ (1) | NZ229823A (de) |
PH (1) | PH26098A (de) |
PT (1) | PT91186B (de) |
RU (1) | RU2041233C1 (de) |
TR (1) | TR27628A (de) |
YU (1) | YU47159B (de) |
ZA (1) | ZA895427B (de) |
Families Citing this family (51)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US5089608A (en) * | 1990-03-23 | 1992-02-18 | Mcneil-Ppc, Inc. | Selective 6-acylation of sucrose mediated by cyclic adducts of dialkyltin oxides and diols |
US5034551A (en) * | 1990-04-23 | 1991-07-23 | Noramco, Inc. | Process for recovery of organotin esters from reaction mixtures containing the same and re-use of the recovered organotin compounds |
US5023329A (en) * | 1990-04-23 | 1991-06-11 | Noramco, Inc. | Sucrose-6-ester production process |
GR910100356A (el) * | 1990-08-27 | 1992-08-31 | Mcneil Ppc Inc | Καταλυόμενη μέ?οδος εστέρος-6-σακχαρόζης. |
US5470969A (en) * | 1990-08-27 | 1995-11-28 | Mcneil-Ppc, Inc. | Catalyzed sucrose-6-ester process |
FR2670493A1 (fr) * | 1990-12-13 | 1992-06-19 | Isochem Sa | Nouveaux composes monoesters du saccharose tels que les 2-0-acylsaccharoses et les 6-0-acylsaccharoses, ainsi que leurs procedes de synthese. |
US5298611A (en) * | 1993-03-12 | 1994-03-29 | Mcneil-Ppc, Inc. | Sucralose pentaester production |
IL114551A0 (en) | 1994-07-11 | 1995-11-27 | Us Agriculture | Chemically synthesized sugar esters for the control of soft bodied arthropods |
US6608039B1 (en) | 1994-07-11 | 2003-08-19 | The United States Of America As Represented By The Secretary Of Agriculture | Chemically synthesized sugar esters for the control of soft-bodied arthropods |
US5498709A (en) | 1994-10-17 | 1996-03-12 | Mcneil-Ppc, Inc. | Production of sucralose without intermediate isolation of crystalline sucralose-6-ester |
RU2159773C2 (ru) | 1995-11-28 | 2000-11-27 | МакНЕЙЛ-ППС, ИНК. | Способы получения сложного эфира сахарозы по положению 6 |
US6121430A (en) * | 1998-12-28 | 2000-09-19 | University Of Iowa Research Foundation | Regiospecific synthesis of glucose-based surfactants |
US7018667B2 (en) | 2000-11-17 | 2006-03-28 | Tate & Lyle Public Limited Company | Meltable form of sucralose |
RU2279437C2 (ru) * | 2000-11-17 | 2006-07-10 | Тейт Энд Лайл Паблик Лимитед Компани | Усовершенствованная сукралозная композиция и способ ее получения |
US6890581B2 (en) * | 2002-04-05 | 2005-05-10 | Tate & Lyle Public Limited Company | Methods for buffer stabilized aqueous deacylation |
US6943248B2 (en) * | 2003-04-30 | 2005-09-13 | Tate & Lyle Public Limited Company | Crystalline form of sucralose, and method for producing it |
CN1176094C (zh) * | 2003-05-23 | 2004-11-17 | 广东省食品工业研究所 | 一种三氯蔗糖的合成方法 |
US20050214425A1 (en) * | 2004-03-23 | 2005-09-29 | Roma Vazirani | Sugar substitute prepared with nutritive and high-intensity sweeteners |
US20090105470A1 (en) * | 2005-02-22 | 2009-04-23 | Pharmed Medicare Private Limited , A Corporation | Tin Mediated Regioselective Synthesis of Sucrose-6-Esters |
US7750146B2 (en) | 2005-03-18 | 2010-07-06 | Tate & Lyle Plc | Granular sucralose |
US20060247180A1 (en) * | 2005-04-29 | 2006-11-02 | Bergey James L | Purgative composition and uses thereof |
US20060276639A1 (en) * | 2005-06-01 | 2006-12-07 | Healthy Brands, Llc | Conversion of sucralose-6-ester to sucralose |
CN100418976C (zh) * | 2006-04-03 | 2008-09-17 | 广州科宏食品添加物有限公司 | 一种三氯蔗糖的制备方法 |
CN101092438A (zh) * | 2006-06-22 | 2007-12-26 | 南京莱因医药科技有限公司 | 6-o-苯甲酰三氯半乳型蔗糖四乙酯的制备方法 |
GB0702854D0 (en) * | 2007-01-09 | 2007-03-28 | Tate & Lyle Plc | Method for the synthesis of sucrose-6-esters |
US20080227971A1 (en) * | 2007-01-19 | 2008-09-18 | Leinhos Duane A | Deacylation of sucralose-6-acylates |
GB0702857D0 (en) * | 2007-01-19 | 2007-03-28 | Tate & Lyle Plc | Improved sucralose production method |
US20090076261A1 (en) * | 2007-09-13 | 2009-03-19 | Polymed Therapeutics, Inc. | Novel process for preparing sucrose-6-esters |
CN101245085B (zh) | 2007-12-19 | 2012-02-01 | 上海同辰生物科技有限公司 | 一种三氯蔗糖的合成及纯化工艺 |
AR070082A1 (es) * | 2008-01-04 | 2010-03-10 | Tate & Lyle Technology Ltd | Metodo para la produccion de sucralosa |
US7932380B2 (en) | 2008-03-06 | 2011-04-26 | Wanhe International (Group) Co. Ltd. | Process for the preparation of sucralose |
US8557976B2 (en) * | 2008-03-13 | 2013-10-15 | Tate & Lyle Technology Limited | Microbial consortia and methods for their use |
EP2254677A1 (de) * | 2008-03-20 | 2010-12-01 | Tate & Lyle Technology Limited | Entfernung von säuren aus tertiäramid-lösungsmitteln |
US8436157B2 (en) * | 2008-03-26 | 2013-05-07 | Tate & Lyle Technology Limited | Method for the production of sucralose |
US8497367B2 (en) * | 2008-04-03 | 2013-07-30 | Tate & Lyle Technology Limited | Sucralose purification process |
AR071134A1 (es) * | 2008-04-03 | 2010-05-26 | Tate & Lyle Technology Ltd | Cristalizacion de sucralosa a partir de chorros que contienen sucralosa |
US20090259036A1 (en) * | 2008-04-03 | 2009-10-15 | Tate & Lyle Technology Limited | Extraction of less polar impurities from sucralose containing aqueous feed streams |
TW200946683A (en) * | 2008-04-03 | 2009-11-16 | Tate & Lyle Technology Ltd | A process for the purification of aqueous feed streams containing sucralose extraction efficiency |
US20090299055A1 (en) * | 2008-04-03 | 2009-12-03 | Tate & Lyle Technology Limited | Purification of Sucralose Containing Feed Streams for Sucralose Crystallization |
GB2469157B (en) | 2009-03-30 | 2011-07-06 | John Kerr | Process for removing dimethylamine during sucralose production |
GB2469158B (en) * | 2009-03-31 | 2011-09-28 | Peter J Seaberg | Base-assisted formation of tin-sucrose adducts |
GB2471348B (en) | 2009-06-22 | 2011-12-14 | Tate & Lyle Technology Ltd | A method for producing sucralose-6-acylate |
GB2474311B (en) * | 2009-10-12 | 2012-10-17 | Tate & Lyle Technology Ltd | Low temperature, single solvent process for the production of sucrose-6-ester |
GB2474310B (en) * | 2009-10-12 | 2012-02-29 | Tate & Lyle Technology Ltd | Process for the production of sucrose-6-ester |
CN101759728B (zh) * | 2010-01-08 | 2012-01-11 | 江苏巨邦制药有限公司 | 三氯蔗糖的生产及精制方法 |
GB201110520D0 (en) | 2011-05-10 | 2011-08-03 | Tate & Lyle Technology Ltd | Extraction of carboxylic acids with tin compounds |
US10227367B2 (en) | 2013-12-16 | 2019-03-12 | Tate & Lyle Technology Limited | Chlorination of sucrose-6-esters |
GB2544217B (en) | 2014-08-08 | 2020-03-25 | Tate & Lyle Tech Ltd | Chlorination of sucrose-6-esters |
GB2536480B (en) | 2015-03-17 | 2019-09-04 | Tate & Lyle Tech Ltd | DMF Distillation |
WO2017091437A1 (en) | 2015-11-24 | 2017-06-01 | Archer Daniels Midland Company | Organotin catalysts in esterification processes of furan-2,5-dicarboxylic acid (fdca) |
GB2551591B (en) | 2016-06-23 | 2019-08-07 | Tate & Lyle Tech Ltd | Liquid-liquid extraction of DMF |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4435440A (en) * | 1976-01-08 | 1984-03-06 | Tate & Lyle Limited | Sweeteners |
EP0030804B1 (de) * | 1979-12-18 | 1983-10-19 | TATE & LYLE PUBLIC LIMITED COMPANY | Kristallin-4,1',6'-trichlor-4,1',6'-trideoxy-galactosucrose |
DE3062467D1 (en) * | 1979-12-20 | 1983-04-28 | Tate & Lyle Plc | Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose |
DE3165986D1 (en) * | 1980-07-08 | 1984-10-18 | Tate & Lyle Plc | Process for the preparation of 4, 1',6'-trichloro-4,1',6'-trideoxygalactosucrose (tgs) |
-
1988
- 1988-07-18 US US07/220,641 patent/US4950746A/en not_active Expired - Lifetime
-
1989
- 1989-07-04 NZ NZ229823A patent/NZ229823A/xx unknown
- 1989-07-12 YU YU139389A patent/YU47159B/sh unknown
- 1989-07-12 AU AU38048/89A patent/AU618107B2/en not_active Expired
- 1989-07-17 EP EP89307228A patent/EP0352048B1/de not_active Expired - Lifetime
- 1989-07-17 AT AT89307228T patent/ATE114664T1/de not_active IP Right Cessation
- 1989-07-17 ZA ZA895427A patent/ZA895427B/xx unknown
- 1989-07-17 JP JP1182762A patent/JP2725710B2/ja not_active Expired - Lifetime
- 1989-07-17 ES ES89307228T patent/ES2065386T3/es not_active Expired - Lifetime
- 1989-07-17 IE IE231089A patent/IE65990B1/en not_active IP Right Cessation
- 1989-07-17 GR GR890100456A patent/GR1002250B/el not_active IP Right Cessation
- 1989-07-17 DK DK352689A patent/DK170027B1/da not_active IP Right Cessation
- 1989-07-17 AR AR89314425A patent/AR245136A1/es active
- 1989-07-17 FI FI893455A patent/FI91874C/fi not_active IP Right Cessation
- 1989-07-17 NO NO892926A patent/NO171855C/no not_active IP Right Cessation
- 1989-07-17 IL IL9100489A patent/IL91004A/en unknown
- 1989-07-17 PT PT91186A patent/PT91186B/pt active IP Right Grant
- 1989-07-17 DE DE68919566T patent/DE68919566T2/de not_active Expired - Lifetime
- 1989-07-17 CA CA000605839A patent/CA1323625C/en not_active Expired - Lifetime
- 1989-07-17 RU SU4614609/04A patent/RU2041233C1/ru not_active IP Right Cessation
- 1989-07-18 TR TR00931/89A patent/TR27628A/xx unknown
- 1989-07-18 MX MX016842A patent/MX172793B/es unknown
- 1989-07-18 KR KR1019890010134A patent/KR0143234B1/ko not_active IP Right Cessation
- 1989-07-18 PH PH38957A patent/PH26098A/en unknown
Also Published As
Similar Documents
Publication | Publication Date | Title |
---|---|---|
DE68919566D1 (de) | Verfahren zur Synthese von Rohrzuckerderivaten durch eine regiokselektive Reaktion. | |
FR2645533B1 (fr) | Procede de synthese de sulfonylimidures | |
DE68919914D1 (de) | Verfahren zur Herstellung von Rohrzucker-Fettsäurepolyester. | |
DE3578979D1 (de) | Verfahren zur synthese von jodbenzol. | |
DE68913429D1 (de) | Verfahren zur Herstellung von Silicium-Einkristallen. | |
ATE66678T1 (de) | Verfahren zur herstellung von makrolidderivaten. | |
ATE39249T1 (de) | Verfahren zur herstellung von polyisocyanatopolyisocyanuraten durch katalytische cyclotrimerisierung von polyisocyanaten. | |
DE68921153D1 (de) | Chemisches Verfahren zur Herstellung von Purinderivaten. | |
DE68921655D1 (de) | Verfahren zur Herstellung von Mustern. | |
MA21148A1 (fr) | Procede de preparation de compose b-lactamique et intermediaires pour sa synthese . | |
FR2654102B1 (fr) | Procede de synthese de derives polyazotes cycliques. | |
DE68913030D1 (de) | Verfahren zur Herstellung von Propylen. | |
DE69021239D1 (de) | Verfahren zur Herstellung von ellagischer Säure. | |
DE59105904D1 (de) | Verfahren zur glycosidasekatalysierten Synthese von Glycokonjugaten. | |
DE68911308D1 (de) | Verfahren für die Herstellung von mono- und diisopropylnaphthalen. | |
PT92726A (pt) | Processo de eliminacao de etanol de bebidas produzidas por fermentacao | |
DE58907777D1 (de) | Verfahren zur Herstellung von Caprolactam. | |
DE69023532D1 (de) | Verfahren zur Synthese von Acylamino-Organosilicium-Verbindungen. | |
DE69011719D1 (de) | Verfahren zur Synthese von Acylamino-organosilicium-Verbindungen. | |
DE3883407D1 (de) | Verfahren zur Herstellung von Fruit-Chips. | |
DE68923912D1 (de) | Verfahren zur Herstellung von 3-Pyrrolidinol. | |
DE69010956D1 (de) | Verfahren zur Synthese von Acylaminogruppen enthaltenden Siliziumverbindungen. | |
DE58907409D1 (de) | Verfahren zur Herstellung von Caprolactam. | |
DE69201245D1 (de) | Verfahren zur Synthese von Hydrogenoperfluoralkanen. | |
DE69006888D1 (de) | Verfahren zur Synthese von Acylamino-Organosilicon-Verbindungen. |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
8364 | No opposition during term of opposition | ||
8327 | Change in the person/name/address of the patent owner |
Owner name: TATE & LYLE PLC, LONDON, GB |
|
8328 | Change in the person/name/address of the agent |
Representative=s name: MARKS & CLERK, LUXEMBOURG, LU |
|
8327 | Change in the person/name/address of the patent owner |
Owner name: TATE & LYLE TECHNOLOGY LTD., LONDON, GB |