DE3689662D1 - Chlorination von Carbohydraten und anderen Alkoholen. - Google Patents

Chlorination von Carbohydraten und anderen Alkoholen.

Info

Publication number
DE3689662D1
DE3689662D1 DE86308119T DE3689662T DE3689662D1 DE 3689662 D1 DE3689662 D1 DE 3689662D1 DE 86308119 T DE86308119 T DE 86308119T DE 3689662 T DE3689662 T DE 3689662T DE 3689662 D1 DE3689662 D1 DE 3689662D1
Authority
DE
Germany
Prior art keywords
chlorination
carbohydrates
alcohols
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
DE86308119T
Other languages
English (en)
Other versions
DE3689662T2 (de
Inventor
Eleanor A O'brien
Thomas O'connor
Mathew R J Tuite
Leroy High
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Ortho McNeil Pharmaceutical Inc
Original Assignee
McNeilab Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by McNeilab Inc filed Critical McNeilab Inc
Publication of DE3689662D1 publication Critical patent/DE3689662D1/de
Application granted granted Critical
Publication of DE3689662T2 publication Critical patent/DE3689662T2/de
Anticipated expiration legal-status Critical
Expired - Lifetime legal-status Critical Current

Links

Classifications

    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L27/00Spices; Flavouring agents or condiments; Artificial sweetening agents; Table salts; Dietetic salt substitutes; Preparation or treatment thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D493/00Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system
    • C07D493/02Heterocyclic compounds containing oxygen atoms as the only ring hetero atoms in the condensed system in which the condensed system contains two hetero rings
    • C07D493/04Ortho-condensed systems
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07BGENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B39/00Halogenation
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00Preparation of halogenated hydrocarbons
    • C07C17/093Preparation of halogenated hydrocarbons by replacement by halogens
    • C07C17/16Preparation of halogenated hydrocarbons by replacement by halogens of hydroxyl groups
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H13/00Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids
    • C07H13/02Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids
    • C07H13/04Compounds containing saccharide radicals esterified by carbonic acid or derivatives thereof, or by organic acids, e.g. phosphonic acids by carboxylic acids having the esterifying carboxyl radicals attached to acyclic carbon atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07HSUGARS; DERIVATIVES THEREOF; NUCLEOSIDES; NUCLEOTIDES; NUCLEIC ACIDS
    • C07H5/00Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium
    • C07H5/02Compounds containing saccharide radicals in which the hetero bonds to oxygen have been replaced by the same number of hetero bonds to halogen, nitrogen, sulfur, selenium, or tellurium to halogen

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Biochemistry (AREA)
  • Biotechnology (AREA)
  • General Health & Medical Sciences (AREA)
  • Genetics & Genomics (AREA)
  • Molecular Biology (AREA)
  • Nutrition Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Saccharide Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE3689662T 1985-10-21 1986-10-20 Chlorination von Carbohydraten und anderen Alkoholen. Expired - Lifetime DE3689662T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB858525954A GB8525954D0 (en) 1985-10-21 1985-10-21 Chlorination of carbohydrates &c alcohols

Publications (2)

Publication Number Publication Date
DE3689662D1 true DE3689662D1 (de) 1994-03-31
DE3689662T2 DE3689662T2 (de) 1994-06-23

Family

ID=10587019

Family Applications (1)

Application Number Title Priority Date Filing Date
DE3689662T Expired - Lifetime DE3689662T2 (de) 1985-10-21 1986-10-20 Chlorination von Carbohydraten und anderen Alkoholen.

Country Status (21)

Country Link
US (1) US4783526A (de)
EP (1) EP0223421B1 (de)
JP (1) JPH0830073B2 (de)
KR (1) KR940000483B1 (de)
AR (1) AR243197A1 (de)
AT (1) ATE101856T1 (de)
AU (1) AU595250B2 (de)
CA (1) CA1284495C (de)
DE (1) DE3689662T2 (de)
DK (1) DK174926B1 (de)
ES (1) ES2051262T3 (de)
FI (1) FI88912C (de)
GB (2) GB8525954D0 (de)
IE (1) IE59558B1 (de)
IL (1) IL80370A (de)
MX (1) MX171629B (de)
NO (1) NO167034C (de)
NZ (1) NZ218009A (de)
PT (1) PT83580B (de)
SU (1) SU1634139A3 (de)
ZA (1) ZA867948B (de)

Families Citing this family (44)

* Cited by examiner, † Cited by third party
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GB8525953D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Preparation of galactopyranoside
GB8622345D0 (en) * 1986-09-17 1986-10-22 Tate & Lyle Plc Sucrose derivatives
GB8818430D0 (en) * 1988-08-03 1988-09-07 Tate & Lyle Plc Process
GB8822674D0 (en) * 1988-09-27 1988-11-02 Tate & Lyle Plc Preparation of acylated sucrose derivatives
US5218097A (en) * 1988-12-07 1993-06-08 Ciba-Geigy Corporation Process for the preparation of protected mono-sugar and oligo-sugar halides
US5122601A (en) * 1990-12-07 1992-06-16 Hawaiian Sugar Planters'association Synthesis of 2,3,3',4,4'-penta-o-methylsucrose
NZ240818A (en) 1990-12-14 1993-08-26 Mcneil Ppc Inc Liquid sucralose concentrate compositions containing preservative, buffer and liquid
DE4116365A1 (de) * 1991-05-18 1992-11-19 Basf Ag Verfahren zur herstellung von alkyl-, alkenyl- und alkinylchloriden
DE19523641A1 (de) * 1995-06-29 1997-01-02 Bayer Ag Verfahren zur Herstellung von substituierten Chloraromaten
US6448449B2 (en) * 2000-04-21 2002-09-10 Rhodia Chirex, Inc. Process for preparation of (R)-1- (aryloxy)propan-2-ol
CN1294139C (zh) * 2000-11-17 2007-01-10 塔特和莱利有限公司 改进的三氯蔗糖组合物及其制备方法
DE10218862A1 (de) * 2002-04-26 2003-11-06 Gruenenthal Gmbh Verfahren zur Chlorierung tertiärer Alkohole
US6943248B2 (en) * 2003-04-30 2005-09-13 Tate & Lyle Public Limited Company Crystalline form of sucralose, and method for producing it
US20060247180A1 (en) * 2005-04-29 2006-11-02 Bergey James L Purgative composition and uses thereof
CN101253187A (zh) * 2005-08-30 2008-08-27 法马德医疗保险私人有限公司 含有蔗糖酯的反应物中吡啶及其类似物的除去方法
DE102005043141A1 (de) * 2005-09-10 2007-03-15 Basf Ag Verfahren zur Chlorierung von Alkoholen
US7741477B2 (en) * 2006-01-10 2010-06-22 Alembic Limited Process for purification of sucralose
CN100418976C (zh) * 2006-04-03 2008-09-17 广州科宏食品添加物有限公司 一种三氯蔗糖的制备方法
US20090312538A1 (en) * 2006-07-06 2009-12-17 Alembic Limited process for the preparation of sucralose of high purity
BRPI0719916A2 (pt) * 2006-12-05 2014-03-04 Tate & Lyle Technology Ltd Recuperação de cloreto de tritila
CN100591684C (zh) * 2006-12-27 2010-02-24 盐城捷康三氯蔗糖制造有限公司 三氯蔗糖结晶方法
JP2008180466A (ja) * 2007-01-25 2008-08-07 Hoshizaki Electric Co Ltd 電装箱
CN101012253B (zh) * 2007-02-06 2010-04-14 启东东岳药业有限公司 6-pas的制备方法
CN101260126B (zh) * 2007-03-06 2010-12-22 盐城捷康三氯蔗糖制造有限公司 三氯蔗糖的结晶方法
CN101245085B (zh) * 2007-12-19 2012-02-01 上海同辰生物科技有限公司 一种三氯蔗糖的合成及纯化工艺
WO2009087677A1 (en) * 2007-12-24 2009-07-16 Alembic Limited An improved process for the preparation of 1, 6-dichloro-1, 6-dide0xy-beta-d-fruct0furan0syl-4-chl0r0-4-de0xy-alpha-galact0py ranoside
AR070082A1 (es) * 2008-01-04 2010-03-10 Tate & Lyle Technology Ltd Metodo para la produccion de sucralosa
WO2009117317A1 (en) * 2008-03-20 2009-09-24 Tate & Lyle Technology Ltd Removal of acids from tertiary amide solvents
US8436157B2 (en) * 2008-03-26 2013-05-07 Tate & Lyle Technology Limited Method for the production of sucralose
TW200946683A (en) * 2008-04-03 2009-11-16 Tate & Lyle Technology Ltd A process for the purification of aqueous feed streams containing sucralose extraction efficiency
US20090299055A1 (en) * 2008-04-03 2009-12-03 Tate & Lyle Technology Limited Purification of Sucralose Containing Feed Streams for Sucralose Crystallization
AR071134A1 (es) * 2008-04-03 2010-05-26 Tate & Lyle Technology Ltd Cristalizacion de sucralosa a partir de chorros que contienen sucralosa
WO2009124113A1 (en) * 2008-04-03 2009-10-08 Tate & Lyle Technology Ltd. Extraction of less polar impurities from sucralose containing aqueous feed streams
US8497367B2 (en) * 2008-04-03 2013-07-30 Tate & Lyle Technology Limited Sucralose purification process
GB2469157B (en) 2009-03-30 2011-07-06 John Kerr Process for removing dimethylamine during sucralose production
GB2469158B (en) 2009-03-31 2011-09-28 Peter J Seaberg Base-assisted formation of tin-sucrose adducts
GB2471348B (en) 2009-06-22 2011-12-14 Tate & Lyle Technology Ltd A method for producing sucralose-6-acylate
GB2474311B (en) * 2009-10-12 2012-10-17 Tate & Lyle Technology Ltd Low temperature, single solvent process for the production of sucrose-6-ester
GB2474310B (en) 2009-10-12 2012-02-29 Tate & Lyle Technology Ltd Process for the production of sucrose-6-ester
IT1403290B1 (it) * 2010-12-27 2013-10-17 Polimeri Europa Spa Componente solido di catalizzatore, catalizzatore comprendente detto componente solido, e procedimento di (co)polimerizzazione delle alfa-olefine
GB201110520D0 (en) 2011-05-10 2011-08-03 Tate & Lyle Technology Ltd Extraction of carboxylic acids with tin compounds
CN105829332B (zh) 2013-12-16 2018-10-02 塔特和莱利技术有限公司 蔗糖-6-酯的氯化
GB2551591B (en) 2016-06-23 2019-08-07 Tate & Lyle Tech Ltd Liquid-liquid extraction of DMF
CN114052236B (zh) * 2020-07-29 2023-08-22 盐城捷康三氯蔗糖制造有限公司 高甜度、低热量的复合甜味剂晶体及其制备方法

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1192205B (de) * 1962-12-31 1965-05-06 Basf Ag Verfahren zur Herstellung von Triaryldihaloge-niden von Elementen der V. Hauptgruppe
US3715407A (en) * 1971-03-01 1973-02-06 Gen Electric Chlorination of ketonic acetyl groups
DE3065399D1 (en) * 1979-12-18 1983-11-24 Tate & Lyle Plc Crystalline 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
GB2065648B (en) * 1979-12-20 1983-08-17 Tate & Lyle Ltd Preparation of 4,1',6'-trichloro-4,1',6'-trideoxgalactosucrose
DE3062467D1 (en) * 1979-12-20 1983-04-28 Tate & Lyle Plc Process for the preparation of 4,1',6'-trichloro-4,1',6'-trideoxy-galactosucrose
US4302869A (en) * 1980-05-15 1981-12-01 John Hackney Hand puller for ropes
DE3220105A1 (de) * 1982-05-28 1983-12-01 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung in (alpha)-stellung chlorierten stickstoff-heterocyclen
IE55619B1 (en) * 1982-09-13 1990-11-21 Tate & Lyle Plc 6-derivatives of 4,1',6'-trichloro-4,1',6'-trideoxygalactosucrose
US4692514A (en) * 1985-12-20 1987-09-08 Uop Inc. Process for separating ketoses from alkaline- or pyridine-catalyzed isomerization products
JPS61247656A (ja) * 1985-04-22 1986-11-04 ハリマセラミック株式会社 炭素含有塩基性耐火物
GB8525953D0 (en) * 1985-10-21 1985-11-27 Mcneilab Inc Preparation of galactopyranoside

Also Published As

Publication number Publication date
KR870003717A (ko) 1987-05-04
EP0223421A3 (en) 1988-12-07
DK503186D0 (da) 1986-10-20
GB8525954D0 (en) 1985-11-27
FI864236A (fi) 1987-04-22
IE862762L (en) 1987-04-21
AU595250B2 (en) 1990-03-29
EP0223421B1 (de) 1994-02-23
AU6421386A (en) 1987-04-30
CA1284495C (en) 1991-05-28
GB2182039B (en) 1989-10-25
FI864236A0 (fi) 1986-10-20
DK174926B1 (da) 2004-03-01
US4783526A (en) 1988-11-08
DK503186A (da) 1987-04-22
PT83580B (pt) 1989-05-31
KR940000483B1 (ko) 1994-01-21
EP0223421A2 (de) 1987-05-27
FI88912B (fi) 1993-04-15
PT83580A (en) 1986-11-01
NZ218009A (en) 1988-11-29
FI88912C (fi) 1993-07-26
ES2051262T3 (es) 1994-06-16
NO167034B (no) 1991-06-17
JPH0830073B2 (ja) 1996-03-27
AR243197A1 (es) 1993-07-30
MX171629B (es) 1993-11-10
GB2182039A (en) 1987-05-07
IL80370A0 (en) 1987-01-30
IE59558B1 (en) 1994-03-09
GB8625108D0 (en) 1986-11-26
ZA867948B (en) 1988-05-25
ATE101856T1 (de) 1994-03-15
JPS62135487A (ja) 1987-06-18
NO864191L (no) 1987-04-22
NO167034C (no) 1991-09-25
IL80370A (en) 1992-01-15
DE3689662T2 (de) 1994-06-23
SU1634139A3 (ru) 1991-03-07
NO864191D0 (no) 1986-10-20

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8328 Change in the person/name/address of the agent

Representative=s name: BOEHMERT & BOEHMERT, 28209 BREMEN