CU24429B1 - Método para recuperar escandio de alta pureza - Google Patents
Método para recuperar escandio de alta purezaInfo
- Publication number
- CU24429B1 CU24429B1 CU2017000067A CU20170067A CU24429B1 CU 24429 B1 CU24429 B1 CU 24429B1 CU 2017000067 A CU2017000067 A CU 2017000067A CU 20170067 A CU20170067 A CU 20170067A CU 24429 B1 CU24429 B1 CU 24429B1
- Authority
- CU
- Cuba
- Prior art keywords
- scandium
- extraction
- high purity
- recovering
- precipitate
- Prior art date
Links
Classifications
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B59/00—Obtaining rare earth metals
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F17/00—Compounds of rare earth metals
- C01F17/10—Preparation or treatment, e.g. separation or purification
- C01F17/13—Preparation or treatment, e.g. separation or purification by using ion exchange resins, e.g. chelate resins
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01F—COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
- C01F17/00—Compounds of rare earth metals
- C01F17/20—Compounds containing only rare earth metals as the metal element
- C01F17/206—Compounds containing only rare earth metals as the metal element oxide or hydroxide being the only anion
- C01F17/212—Scandium oxides or hydroxides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B1/00—Preliminary treatment of ores or scrap
- C22B1/02—Roasting processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/04—Extraction of metal compounds from ores or concentrates by wet processes by leaching
- C22B3/06—Extraction of metal compounds from ores or concentrates by wet processes by leaching in inorganic acid solutions, e.g. with acids generated in situ; in inorganic salt solutions other than ammonium salt solutions
- C22B3/08—Sulfuric acid, other sulfurated acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/26—Treatment or purification of solutions, e.g. obtained by leaching by liquid-liquid extraction using organic compounds
- C22B3/28—Amines
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/42—Treatment or purification of solutions, e.g. obtained by leaching by ion-exchange extraction
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2006/00—Physical properties of inorganic compounds
- C01P2006/80—Compositional purity
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Geology (AREA)
- Materials Engineering (AREA)
- Metallurgy (AREA)
- Mechanical Engineering (AREA)
- Environmental & Geological Engineering (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Manufacturing & Machinery (AREA)
- Geochemistry & Mineralogy (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Analytical Chemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Compounds Of Alkaline-Earth Elements, Aluminum Or Rare-Earth Metals (AREA)
Abstract
<p>Se proporciona un método para recuperar escandio, con el que es posible recuperar fácil y eficientemente escandio de alta pureza de menas de óxido de níquel. Este método para recuperar escandio involucra pasar una solución que contiene escandio a través de una resina de intercambio iónico, después someter el eluyente eluido de la resina de intercambio iónico a extracción por solvente y separar el líquido residual de extracción y el agente de extracción después de la extracción, después realizar un proceso de oxalación en el líquido residual de extracción para obtener un precipitado de oxalato de escandio, y calcinar el precipitado para obtener óxido de escandio, en donde el método se caracteriza en que se utiliza un agente de extracción como el agente de extracción para la extracción por solvente.</p>
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
JP2014239086 | 2014-11-26 | ||
JP2015229343A JP5967284B2 (ja) | 2014-11-26 | 2015-11-25 | 高純度スカンジウムの回収方法 |
PCT/JP2015/083020 WO2016084830A1 (ja) | 2014-11-26 | 2015-11-25 | 高純度スカンジウムの回収方法 |
Publications (2)
Publication Number | Publication Date |
---|---|
CU20170067A7 CU20170067A7 (es) | 2018-02-08 |
CU24429B1 true CU24429B1 (es) | 2019-07-04 |
Family
ID=56123280
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CU2017000067A CU24429B1 (es) | 2014-11-26 | 2015-11-25 | Método para recuperar escandio de alta pureza |
Country Status (8)
Country | Link |
---|---|
US (1) | US10081851B2 (es) |
EP (1) | EP3208352B1 (es) |
JP (1) | JP5967284B2 (es) |
CN (1) | CN107002176B (es) |
AU (1) | AU2015351446B2 (es) |
CA (1) | CA2968341C (es) |
CU (1) | CU24429B1 (es) |
PH (1) | PH12017500865B1 (es) |
Families Citing this family (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP6004023B2 (ja) | 2015-02-02 | 2016-10-05 | 住友金属鉱山株式会社 | スカンジウムの回収方法 |
JP6406234B2 (ja) * | 2015-12-16 | 2018-10-17 | 住友金属鉱山株式会社 | スカンジウムの回収方法 |
JP6256491B2 (ja) | 2016-01-25 | 2018-01-10 | 住友金属鉱山株式会社 | スカンジウムの回収方法 |
JP6409796B2 (ja) * | 2016-02-23 | 2018-10-24 | 住友金属鉱山株式会社 | スカンジウムの回収方法 |
JP6816410B2 (ja) * | 2016-08-30 | 2021-01-20 | 住友金属鉱山株式会社 | スカンジウムの回収方法 |
WO2018097001A1 (ja) | 2016-11-24 | 2018-05-31 | 住友金属鉱山株式会社 | スカンジウムの精製方法 |
JP6922478B2 (ja) * | 2016-11-24 | 2021-08-18 | 住友金属鉱山株式会社 | スカンジウムの精製方法 |
JP6798078B2 (ja) * | 2016-11-30 | 2020-12-09 | 住友金属鉱山株式会社 | イオン交換処理方法、スカンジウムの回収方法 |
JP6874547B2 (ja) * | 2017-06-08 | 2021-05-19 | 住友金属鉱山株式会社 | スカンジウムの回収方法 |
JP6852599B2 (ja) * | 2017-07-05 | 2021-03-31 | 住友金属鉱山株式会社 | スカンジウムの精製方法 |
KR102178440B1 (ko) * | 2018-12-18 | 2020-11-13 | 주식회사 포스코 | 스칸듐을 회수하는 방법 |
JP7338179B2 (ja) * | 2019-03-14 | 2023-09-05 | 住友金属鉱山株式会社 | 高純度酸化スカンジウムの製造方法 |
CN110423902B (zh) * | 2019-08-29 | 2021-07-20 | 赣州有色冶金研究所有限公司 | 一种高纯碳酸稀土的制备方法及*** |
CN110541081A (zh) * | 2019-09-02 | 2019-12-06 | 中国恩菲工程技术有限公司 | 处理红土镍矿的方法 |
JP7463181B2 (ja) | 2020-04-22 | 2024-04-08 | Jx金属株式会社 | レアメタルの回収方法 |
JP2022024249A (ja) * | 2020-07-13 | 2022-02-09 | 住友金属鉱山株式会社 | スカンジウムの回収方法 |
CN114763586B (zh) * | 2021-01-11 | 2024-03-08 | 中国科学院江西稀土研究院 | 一种稀土母液强化中和相态重构与铝资源利用的方法 |
CN113337739B (zh) * | 2021-06-03 | 2023-03-21 | 赣州有色冶金研究所有限公司 | 一种负载稀土树脂的解吸方法以及稀土的回收方法 |
CN114314632A (zh) * | 2021-12-31 | 2022-04-12 | 湖南金坤新材料有限公司 | 一种提纯精氧化钪的方法 |
Family Cites Families (18)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4718995A (en) * | 1986-01-24 | 1988-01-12 | Gte Products Corporation | Recovery of tungsten, scandium, iron, and manganese from tungsten bearing material |
US4626280A (en) * | 1986-01-24 | 1986-12-02 | Gte Products Corporation | Recovery of tungsten, scandium, iron, and manganese from tungsten bearing material |
US4765909A (en) * | 1987-04-23 | 1988-08-23 | Gte Laboratories Incorporated | Ion exchange method for separation of scandium and thorium |
JPH03173725A (ja) | 1989-12-01 | 1991-07-29 | Univ Tohoku | 希土類元素の分別方法 |
JP3344194B2 (ja) | 1996-01-18 | 2002-11-11 | 大平洋金属株式会社 | 酸化鉱石からの高純度レアーアースメタル酸化物の製造方法 |
JP3327110B2 (ja) | 1996-03-18 | 2002-09-24 | 大平洋金属株式会社 | スカンジュウム・トリフラートの製造方法 |
US7282187B1 (en) * | 1996-03-26 | 2007-10-16 | Caboi Corporation | Recovery of metal values |
JP3428292B2 (ja) | 1996-04-26 | 2003-07-22 | 大平洋金属株式会社 | Sc金属の回収方法 |
US5787332A (en) * | 1996-09-26 | 1998-07-28 | Fansteel Inc. | Process for recovering tantalum and/or niobium compounds from composites containing a variety of metal compounds |
JP3848271B2 (ja) * | 2003-02-27 | 2006-11-22 | 独立行政法人科学技術振興機構 | N,n’−ビスホスホノアルカンジアミン化合物、及びその製造方法、並びにその用途 |
US20120207656A1 (en) * | 2011-02-11 | 2012-08-16 | Emc Metals Corporation | System and Method for Recovery of Scandium Values From Scandium-Containing Ores |
US9499881B2 (en) * | 2012-12-04 | 2016-11-22 | Lixivia, Inc. | Refining methods and agents for rare earth production |
TW201439331A (zh) | 2013-01-10 | 2014-10-16 | Bloom Energy Corp | 自鈦殘餘物流回收鈧的方法 |
FR3001465B1 (fr) * | 2013-01-30 | 2015-03-13 | Eramet | Procede d'extraction selective du scandium |
JP5652503B2 (ja) * | 2013-05-10 | 2015-01-14 | 住友金属鉱山株式会社 | スカンジウム回収方法 |
CN103361486B (zh) * | 2013-07-18 | 2014-10-29 | 攀枝花市精研科技有限公司 | 从含钪和钛的废酸液中提取高纯氧化钪及钛的方法 |
CN103468978B (zh) | 2013-08-15 | 2016-03-30 | 中国恩菲工程技术有限公司 | 一种从红土镍矿硫酸浸出液中提钪的方法 |
JP6172099B2 (ja) * | 2014-09-24 | 2017-08-02 | 住友金属鉱山株式会社 | スカンジウムの回収方法 |
-
2015
- 2015-11-25 AU AU2015351446A patent/AU2015351446B2/en not_active Ceased
- 2015-11-25 JP JP2015229343A patent/JP5967284B2/ja active Active
- 2015-11-25 US US15/526,862 patent/US10081851B2/en not_active Expired - Fee Related
- 2015-11-25 CU CU2017000067A patent/CU24429B1/es unknown
- 2015-11-25 CA CA2968341A patent/CA2968341C/en not_active Expired - Fee Related
- 2015-11-25 EP EP15863799.1A patent/EP3208352B1/en active Active
- 2015-11-25 CN CN201580062282.0A patent/CN107002176B/zh not_active Expired - Fee Related
-
2017
- 2017-05-10 PH PH12017500865A patent/PH12017500865B1/en unknown
Also Published As
Publication number | Publication date |
---|---|
CA2968341A1 (en) | 2016-06-02 |
AU2015351446A1 (en) | 2017-06-08 |
CN107002176B (zh) | 2019-03-05 |
PH12017500865A1 (en) | 2017-11-06 |
EP3208352A1 (en) | 2017-08-23 |
PH12017500865B1 (en) | 2017-11-06 |
JP2016108664A (ja) | 2016-06-20 |
US20170321301A1 (en) | 2017-11-09 |
CA2968341C (en) | 2018-04-03 |
US10081851B2 (en) | 2018-09-25 |
EP3208352B1 (en) | 2019-07-24 |
EP3208352A4 (en) | 2017-10-18 |
AU2015351446B2 (en) | 2018-08-02 |
CU20170067A7 (es) | 2018-02-08 |
CN107002176A (zh) | 2017-08-01 |
JP5967284B2 (ja) | 2016-08-10 |
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