CN220788891U - Acid bath device for producing stable regenerated cellulose filaments - Google Patents

Acid bath device for producing stable regenerated cellulose filaments Download PDF

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Publication number
CN220788891U
CN220788891U CN202322346880.5U CN202322346880U CN220788891U CN 220788891 U CN220788891 U CN 220788891U CN 202322346880 U CN202322346880 U CN 202322346880U CN 220788891 U CN220788891 U CN 220788891U
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China
Prior art keywords
pipe
acid
overflow
acid bath
barrel
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CN202322346880.5U
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李全岭
杨海军
王景彬
沈彦军
马东涛
张文超
王玉昆
王方然
杨中玉
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Xinxiang Chemical Fiber Co Ltd
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Xinxiang Chemical Fiber Co Ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P70/00Climate change mitigation technologies in the production process for final industrial or consumer products
    • Y02P70/50Manufacturing or production processes characterised by the final manufactured product
    • Y02P70/62Manufacturing or production processes characterised by the final manufactured product related technologies for production or treatment of textile or flexible materials or products thereof, including footwear

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Abstract

The utility model discloses an acid bath device for stabilizing regenerated cellulose filament production, and relates to the technical field of spinning. The acid bath balance device comprises a machine connecting pipe, an acid bath balance barrel, an acid inlet pipe, an overflow pipe and an overflow delivery pipe, wherein the upper end of the peripheral side surface of the machine connecting pipe is fixedly penetrated by the acid bath balance barrel which is vertically arranged, the acid inlet pipe is fixedly penetrated by the peripheral side of the acid bath balance barrel, and the middle part of the peripheral side of the acid inlet pipe is in penetrating connection with the acid bath balance barrel through the acid supplementing pipe; the periphery of the acid bath balancing barrel is also communicated and fixed with an overflow pipe opposite to the acid inlet pipe, and one side of the overflow pipe far away from the acid bath balancing barrel is also provided with an overflow delivery pipe. The acid bath balance barrel, the acid inlet pipe, the acid supplementing pipe, the overflow pipe and the overflow delivery pipe are arranged, so that the problem that the acid bath device cannot adjust the liquid level of the acid bath in a large range according to different kinds of process requirements is solved; and the overflow amount of the acid bath is insufficient, and the liquid level of the acid bath is not easy to control.

Description

Acid bath device for producing stable regenerated cellulose filaments
Technical Field
The utility model belongs to the technical field of spinning, and particularly relates to an acid bath device for stabilizing regenerated cellulose filament production.
Background
The concentration and temperature of sulfuric acid and zinc sulfate in the coagulation bath on the spinning machine are continuously reduced in the whole spinning process. To stabilize the spinning conditions we can continuously supply a constant composition and constant temperature acid bath to the spinning machine while flowing the diluted acid bath back to the acid station via a pipeline. In a sense, this constitutes the circulation of the acid bath. In the circulation system, the acid station sends acid bath meeting the technological requirements to a spinning machine bath tank, and viscose in the bath tank can be flushed out of a spinneret to carry out chemical reaction with sulfuric acid to generate fibers, wherein the concentration drop is generally in the range of 6g/L to 8 g/L. As the concentration and temperature of sulfuric acid and zinc sulfate in the coagulation bath decrease, the properties of the viscose fiber also fluctuate, which affects the quality of the fiber. The acid bath is indispensable in the regenerated cellulose filament production process, but the conventional acid bath balancing barrel still has the following defects in actual use:
In the existing practical production, the height of a traditional continuous spinning acid bath balancing barrel is 830mm, the diameter of the balancing barrel is 325mm, the highest flow rate of the acid bath per spindle position can reach about 35L/h when the balancing barrel keeps a certain liquid level, the flow rate can only meet the spinning condition that the spinning speed is not more than 160 m/min, and the production efficiency is relatively low; the conventional acid bath balance barrel is low in height, the flow velocity and flow rate of the acid bath in the glass tube under normal pressure are low, and the production requirement of high spinning speed cannot be met; the liquid level of the acid bath cannot be adjusted in a large range according to the process requirements of different varieties;
The conventional acid bath balance barrel is usually provided with only one overflow pipeline, so that the overflow amount of the acid bath is large, and when the liquid level is forcedly increased, the stop accident can occur because the circulation amount can not meet the production requirement.
Disclosure of utility model
The utility model aims to provide an acid bath device for stabilizing regenerated cellulose filament production, which solves the problem that the acid bath device cannot adjust the acid bath liquid level in a large range according to different kinds of process requirements by arranging an acid bath balancing barrel, an acid inlet pipe, an acid supplementing pipe, an overflow delivery pipe, an overflow branch pipe I, an overflow branch pipe II and an overflow branch pipe III; and the overflow amount of the acid bath is insufficient, and the liquid level of the acid bath is not easy to control.
In order to solve the technical problems, the utility model is realized by the following technical scheme:
The utility model relates to an acid bath device for stabilizing regenerated cellulose filament production, which comprises a machine connecting pipe, an acid bath balancing barrel, an acid inlet pipe, an overflow pipe and an overflow delivery pipe, wherein the upper end of the peripheral side surface of the machine connecting pipe is fixedly penetrated by the acid bath balancing barrel which is vertically arranged, the acid inlet pipe is fixedly penetrated by the peripheral side of the acid bath balancing barrel, and the middle part of the peripheral side of the acid inlet pipe is communicated with the acid bath balancing barrel through an acid supplementing pipe;
The acid bath enters through the acid inlet pipe and flows through the machine connecting pipe, gradually flows into the single-zone reaction bin, forms a certain liquid level height in the acid bath balancing barrel along with the continuous entering of the acid bath, and simultaneously ensures that the acid bath continuously flows out from the machine acid inlet of the machine connecting pipe; then, as the upper end of the acid inlet pipe is an inlet of the acid bath, the opening of the acid inlet valve is controlled, the entering amount of the acid bath is controlled, and meanwhile, the acid bath is injected into the acid bath balancing barrel and the machine connecting pipe by matching with the opening and closing of the acid supplementing pipe and the acid supplementing valve on the surface of the acid bath balancing barrel, the liquid level in the acid bath balancing barrel is controlled, the design of the acid supplementing pipe is directly communicated with the acid bath balancing barrel, the liquid level in the acid bath balancing barrel can be rapidly increased, the production processes of different varieties and different spinning speeds are realized, and the flow rate of single-ingot acid bath is kept to reach the production requirement; the flow rate of the acid bath can reach more than 120 (meters per minute), thereby meeting the technological requirements of improving the spinning speed;
An overflow pipe opposite to the acid inlet pipe is also communicated and fixed on the periphery of the acid bath balancing barrel, an overflow delivery pipe is also arranged beside the overflow pipe far away from the acid bath balancing barrel, and an overflow branch pipe I, an overflow branch pipe II and an overflow branch pipe III are sequentially communicated and fixed between the overflow pipe and the overflow delivery pipe from bottom to top;
The heights of the overflow branch pipe I, the overflow branch pipe II and the overflow branch pipe III relative to the whole are 50cm, 90cm and 115cm, namely three overflow ports with different heights, and when the opening size of an acid supplementing valve on an acid supplementing pipe is regulated, the liquid level in an acid bath balancing barrel is regulated between 50cm and 240 cm; excessive acid bath in the acid bath balance barrel overflows from the overflow pipe and is discharged through the overflow guide pipe connected with the corresponding overflow branch pipe I, the overflow branch pipe II and the overflow branch pipe III, and the opening and closing of the overflow regulating valves on the overflow branch pipe I, the overflow branch pipe II and the overflow branch pipe III are controlled; the spinning speed can be realized from 100 meters/min to 180 meters/min, and the acid bath liquid level is stabilized through the first overflow branch pipe, the second overflow branch pipe and the third overflow branch pipe, so that fluctuation is reduced, production is stabilized, and uniformity and consistency of product quality are ensured.
Further, one end of the machine connecting pipe is closed, the other end of the machine connecting pipe is provided with a through machine acid inlet, and the machine acid inlet is connected with the single-zone reaction bin so that the acid bath enters the single-zone reaction bin.
Further, the joint of the acid inlet pipe and the acid bath balancing barrel is lower than the joint of the overflow pipe and the acid bath balancing barrel, and the joint of the acid supplementing pipe and the acid bath balancing barrel is higher than the joint of the overflow pipe and the acid bath balancing barrel.
Further, an acid supplementing valve is fixed on the acid supplementing pipe, an acid inlet valve is fixed on the surface of the acid inlet pipe below the acid supplementing pipe, and the acid supplementing valve controls the opening and closing of the acid supplementing pipe and the flow; the acid inlet valve controls the opening and closing of the acid inlet pipe and the flow passing through the acid inlet pipe.
Further, an exhaust pipe is fixedly penetrated at the periphery of the acid bath balancing barrel above the acid supplementing pipe, and an exhaust valve is fixedly arranged on the surface of the exhaust pipe;
The gas generated in the acid bath is led out through the exhaust pipe, and is discharged after being treated correspondingly by controlling the discharge of the gas and the flow of the discharged gas through the opening and closing of the exhaust valve and the opening of the exhaust valve.
Further, an overflow main valve is fixed on the surface of the overflow pipe below the overflow branch pipe II, and overflow regulating valves are fixed on the surfaces of the overflow branch pipe I, the overflow branch pipe II and the overflow branch pipe III; the overflow main valve controls the opening and closing of the overflow pipe, and the overflow regulating valves on the overflow branch pipe I, the overflow branch pipe II and the overflow branch pipe III control the opening and closing of the corresponding branch pipes.
Further, the upper end of the acid bath balancing barrel is closed, and the upper end of the overflow delivery pipe is closed and the lower end of the overflow delivery pipe is communicated.
The utility model has the following beneficial effects:
The utility model solves the problem that the acid bath device can not adjust the liquid level of the acid bath in a large range according to different kinds of process requirements by arranging the acid bath balancing barrel, the acid inlet pipe and the acid supplementing pipe; the upper end of the acid inlet pipe is an acid bath inlet, the opening size of an acid inlet valve is controlled, the entering amount of the acid bath is controlled, meanwhile, the acid bath is injected into an acid bath balance barrel and a machine connecting pipe by matching with the opening and closing of the acid supplementing pipe and the acid supplementing valve on the surface of the acid bath balance barrel, the liquid level in the acid bath balance barrel is controlled, the design of the acid supplementing pipe is directly communicated with the acid bath balance barrel, the liquid level in the acid bath balance barrel can be rapidly increased, the production processes of different varieties and different spinning speeds are realized, the flow rate of single-ingot acid bath is kept to meet the production requirement, and the liquid level of the acid bath can be rapidly adjusted according to actual conditions; the height of the liquid level of the acid bath is between 50cm and 240 cm.
According to the utility model, the acid bath balance barrel, the overflow pipe, the overflow delivery pipe, the overflow branch pipe I, the overflow branch pipe II and the overflow branch pipe III are arranged, so that the problem that the overflow amount of the acid bath is insufficient and the liquid level of the acid bath is not easy to control is solved; the excessive acid bath in the acid bath balance barrel overflows from the overflow pipe, is discharged through the overflow guide pipe connected with the corresponding overflow branch pipe I, the overflow branch pipe II and the overflow branch pipe III, can realize spinning at different spinning speeds from 100 meters/minute to 180 meters/minute, and stabilizes the acid bath liquid level through the overflow branch pipe I, the overflow branch pipe II and the overflow branch pipe III, reduces fluctuation, stabilizes production, has smaller diameter than the conventional acid bath balance barrel, increases three overflow ports, and is provided with an acid bath liquid level supplementing valve so as to reduce the circulation volume of an acid bath system, stabilize the acid bath liquid level and facilitate operation; the overflow of the acid bath balancing barrel adopts 50cm, 90cm and 115cm opening overflow, can meet the adjustment of the liquid level of the acid bath at different spinning speeds, and maintains a certain overflow state to stabilize the liquid level of the acid bath.
Drawings
FIG. 1 is a perspective view of an acid bath apparatus for stabilizing the production of regenerated cellulose filaments;
FIG. 2 is a block diagram of another view of an acid bath apparatus for stabilizing regenerated cellulose filament production;
FIG. 3 is a cross-sectional view of an acid bath apparatus for stabilizing regenerated cellulose filament production;
fig. 4 is a cross-sectional view of the overflow tube and overflow delivery tube.
Reference numerals:
1. A machine connecting pipe; 101. an acid inlet of the machine table; 2. acid bath balancing barrels; 3. an acid inlet pipe; 301. an acid inlet valve; 302. acid supplementing pipes; 3021. acid supplementing valve; 4. an exhaust pipe; 401. an exhaust valve; 5. an overflow pipe; 501. an overflow main valve; 502. an overflow branch pipe I; 503. an overflow branch pipe II; 504. overflow branch pipe III; 505. an overflow regulating valve; 6. and an overflow delivery pipe.
Detailed Description
The technical solutions in the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model.
Referring to fig. 1-4, the utility model discloses an acid bath device for producing stable regenerated cellulose filaments, which comprises a machine connecting pipe 1, an acid bath balancing barrel 2, an acid inlet pipe 3, an overflow pipe 5 and an overflow delivery pipe 6, wherein the upper end of the peripheral side surface of the machine connecting pipe 1 is fixedly penetrated by the acid bath balancing barrel 2 which is vertically arranged, the acid inlet pipe 3 is fixedly penetrated by the peripheral side of the acid bath balancing barrel 2, and the middle part of the peripheral side of the acid inlet pipe 3 is fixedly penetrated by an acid supplementing pipe 302;
The acid bath enters through the acid inlet pipe 3 and flows through the machine connecting pipe 1, gradually flows into the single-zone reaction bin, forms a certain liquid level height in the acid bath balance barrel 2 along with the continuous entering of the acid bath, and simultaneously ensures that the acid bath continuously flows out from the machine acid inlet 101 of the machine connecting pipe 1; then, as the upper end of the acid inlet pipe 3 is an acid bath inlet, the opening of the acid inlet valve 301 is controlled, the acid bath inlet amount is controlled, and meanwhile, the acid bath is injected into the acid bath balance barrel 2 and the machine connecting pipe 1 by matching with the opening and closing of the acid supplementing pipe 302 and the surface acid supplementing valve 3021, the liquid level in the acid bath balance barrel 2 is controlled, the design of the acid supplementing pipe 302 is directly communicated with the acid bath balance barrel 2, the liquid level in the acid bath balance barrel 2 can be rapidly increased, the production process of different varieties and different spinning speeds is realized, and the single spindle acid bath flow rate is kept to reach the production requirement; the flow rate of the acid bath can reach more than 120 (meters per minute), thereby meeting the technological requirements of improving the spinning speed;
An overflow pipe 5 opposite to the acid inlet pipe 3 is fixedly penetrated at the periphery of the acid bath balance barrel 2, an overflow delivery pipe 6 is further arranged at one side of the overflow pipe 5 far away from the acid bath balance barrel 2, and an overflow branch pipe I502, an overflow branch pipe II 503 and an overflow branch pipe III 504 are sequentially penetrated and fixed between the overflow pipe 5 and the overflow delivery pipe 6 from bottom to top;
The heights of the overflow branch pipe I502, the overflow branch pipe II 503 and the overflow branch pipe III 504 relative to the whole are 50cm, 90cm and 115cm, namely three overflow ports with different heights, and when the opening size of the acid supplementing valve 3021 on the acid supplementing pipe 302 is regulated, the liquid level in the acid bath balance barrel 2 is regulated between 50cm and 240 cm; excessive acid bath in the acid bath balance barrel 2 overflows from the overflow pipe 5 and is discharged through the overflow guide pipe 6 which is connected with the corresponding overflow branch pipe I502, the overflow branch pipe II 503 and the overflow branch pipe III 504, and the opening and closing of the overflow regulating valves 505 on the overflow branch pipe I502, the overflow branch pipe II 503 and the overflow branch pipe III 504 are controlled; the spinning can be carried out at different spinning speeds from 100 meters/min to 180 meters/min, the acid bath liquid level is stabilized through the first overflow branch pipe 502, the second overflow branch pipe 503 and the third overflow branch pipe 504, fluctuation is reduced, production is stabilized, and uniformity and consistency of product quality are ensured.
One end of the machine connecting pipe 1 is closed, and the other end is provided with a through machine acid inlet 101; the machine acid inlet 101 is connected with the single-zone reaction bin, so that the acid bath enters the single-zone reaction bin.
The joint of the acid inlet pipe 3 and the acid bath balancing barrel 2 is lower than the joint of the overflow pipe 5 and the acid bath balancing barrel 2, and the joint of the acid supplementing pipe 302 and the acid bath balancing barrel 2 is higher than the joint of the overflow pipe 5 and the acid bath balancing barrel 2;
The acid supplementing pipe 302 is fixedly provided with an acid supplementing valve 3021, and the acid inlet valve 301 is fixed on the surface of the acid inlet pipe 3 below the acid supplementing pipe 302; the acid supplementing valve 3021 controls the opening and closing and the flow of the acid supplementing pipe 302; the acid inlet valve 301 controls the opening and closing of the acid inlet pipe 3 and the flow passing through the acid inlet pipe.
An exhaust pipe 4 is fixedly penetrated on the periphery side of the acid bath balance barrel 2 above the acid supplementing pipe 302, and an exhaust valve 401 is fixedly arranged on the surface of the exhaust pipe 4; the gas generated in the acid bath is led out through the exhaust pipe 4, and is discharged after being processed correspondingly by controlling the discharge of the gas and the flow of the discharged gas through the opening and closing of the exhaust valve 401 and the opening of the exhaust valve.
The surface of the overflow pipe 5 below the overflow branch pipe II 503 is fixed with an overflow main valve 501, and the surfaces of the overflow branch pipe I502, the overflow branch pipe II 503 and the overflow branch pipe III 504 are all fixed with an overflow regulating valve 505;
the overflow main valve 501 controls the opening and closing of the overflow pipe 5, and the overflow regulating valves 505 on the overflow branch pipe I502, the overflow branch pipe II 503 and the overflow branch pipe III 504 control the opening and closing of the corresponding branch pipes;
The upper end of the acid bath balancing barrel 2 is closed, and the upper end of the overflow delivery pipe 6 is closed and the lower end is communicated.
The specific working principle of the utility model is as follows: firstly, acid bath enters through the acid inlet pipe 3 and flows into the single-zone reaction bin through the machine connecting pipe 1 gradually, a certain liquid level is formed in the acid bath balance barrel 2 along with the continuous entering of the acid bath, meanwhile, the acid bath continuously flows out of the machine acid inlet 101 of the machine connecting pipe 1, the opening size of the acid inlet valve 301 is controlled, the entering amount of the acid bath is controlled, meanwhile, the acid bath is injected into the acid bath balance barrel 2 and the machine connecting pipe 1 by matching with the opening and closing of the acid supplementing pipe 302 and the surface acid supplementing valve 3021 thereof, the liquid level in the acid bath balance barrel 2 is controlled, the acid supplementing pipe 302 is directly communicated with the acid bath balance barrel 2, the liquid level in the acid bath balance barrel 2 can be rapidly increased, the liquid level range is between 50cm and 240cm, when the opening size of the acid supplementing valve 3021 on the acid supplementing pipe 302 is adjusted, the liquid level in the acid bath balance barrel 2 is adjusted between 50cm and 240cm, and the acid bath can be discharged from the overflow pipe 5, the overflow pipe 502 is correspondingly discharged through the overflow pipe 5, the liquid level I and the overflow pipe 503 is correspondingly discharged through the exhaust pipe 6, the exhaust pipe 401 is correspondingly opened and the exhaust pipe is stably, and the flow is stably discharged, and the flow is finally, the flow is stably discharged and the flow is discharged through the exhaust pipe 401 is correspondingly and is stably discharged and the exhaust pipe is opened and the flow is stable.
The foregoing is only a preferred embodiment of the present utility model, and the present utility model is not limited thereto, and any modification, equivalent replacement, and improvement of some of the technical features described in the foregoing embodiments are all within the scope of the present utility model.

Claims (7)

1. The utility model provides an acid bath device of stable regenerated cellulose filament production, includes board connecting pipe (1), acid bath balancing vat (2), advances sour pipe (3), overflow pipe (5) and overflow delivery tube (6), its characterized in that: the upper end of the peripheral side surface of the machine connecting pipe (1) is fixedly penetrated by an acid bath balancing barrel (2) which is vertically arranged, the peripheral side of the acid bath balancing barrel (2) is fixedly penetrated by an acid inlet pipe (3), and the middle part of the peripheral side of the acid inlet pipe (3) is in penetrating connection with the acid bath balancing barrel (2) through an acid supplementing pipe (302);
The acid bath balance barrel (2) circumference side still link up and is fixed with overflow pipe (5) relative with advancing sour pipe (3), one side that overflow pipe (5) kept away from sour bath balance barrel (2) still is provided with overflow delivery tube (6), link up in proper order from bottom to top between overflow pipe (5) and overflow delivery tube (6) and be fixed with overflow branch pipe one (502), overflow branch pipe two (503) and overflow branch pipe three (504).
2. An acid bath apparatus for stabilizing the production of regenerated cellulose filaments as set forth in claim 1 wherein: one end of the machine connecting pipe (1) is closed, and the other end is provided with a through machine acid inlet (101).
3. An acid bath apparatus for stabilizing the production of regenerated cellulose filaments as set forth in claim 1 wherein: the joint of the acid inlet pipe (3) and the acid bath balancing barrel (2) is lower than the joint of the overflow pipe (5) and the acid bath balancing barrel (2), and the joint of the acid supplementing pipe (302) and the acid bath balancing barrel (2) is higher than the joint of the overflow pipe (5) and the acid bath balancing barrel (2).
4. An acid bath apparatus for stabilizing the production of regenerated cellulose filaments as set forth in claim 1 wherein: an acid supplementing valve (3021) is fixed on the acid supplementing pipe (302), and an acid inlet valve (301) is fixed on the surface of the acid inlet pipe (3) below the acid supplementing pipe (302).
5. An acid bath apparatus for stabilizing the production of regenerated cellulose filaments as set forth in claim 1 wherein: an exhaust pipe (4) is fixedly penetrated at the periphery of the acid bath balancing barrel (2) above the acid supplementing pipe (302), and an exhaust valve (401) is fixedly arranged on the surface of the exhaust pipe (4).
6. An acid bath apparatus for stabilizing the production of regenerated cellulose filaments as set forth in claim 1 wherein: and an overflow main valve (501) is fixed on the surface of an overflow pipe (5) below the overflow branch pipe II (503), and overflow regulating valves (505) are fixed on the surfaces of the overflow branch pipe I (502), the overflow branch pipe II (503) and the overflow branch pipe III (504).
7. An acid bath apparatus for stabilizing the production of regenerated cellulose filaments as set forth in claim 1 wherein: the upper end of the acid bath balancing barrel (2) is closed, and the upper end of the overflow delivery pipe (6) is closed and the lower end is communicated.
CN202322346880.5U 2023-08-31 2023-08-31 Acid bath device for producing stable regenerated cellulose filaments Active CN220788891U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202322346880.5U CN220788891U (en) 2023-08-31 2023-08-31 Acid bath device for producing stable regenerated cellulose filaments

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202322346880.5U CN220788891U (en) 2023-08-31 2023-08-31 Acid bath device for producing stable regenerated cellulose filaments

Publications (1)

Publication Number Publication Date
CN220788891U true CN220788891U (en) 2024-04-16

Family

ID=90630262

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202322346880.5U Active CN220788891U (en) 2023-08-31 2023-08-31 Acid bath device for producing stable regenerated cellulose filaments

Country Status (1)

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CN (1) CN220788891U (en)

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