CN219167749U - Isomerism reaction condensation dewatering device - Google Patents
Isomerism reaction condensation dewatering device Download PDFInfo
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- CN219167749U CN219167749U CN202320246015.0U CN202320246015U CN219167749U CN 219167749 U CN219167749 U CN 219167749U CN 202320246015 U CN202320246015 U CN 202320246015U CN 219167749 U CN219167749 U CN 219167749U
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Abstract
The utility model provides a condensing and dehydrating device for an isomerism reaction, and belongs to the technical field of turpentine isomerism reaction. The isomerism reaction condensation dehydration device comprises an isomerism reaction kettle, wherein a condensation dehydrator is arranged on one side of the isomerism reaction kettle, a suction pump and an oil delivery pipe are arranged on one side of the isomerism reaction kettle, and the suction pump and the oil delivery pipe are positioned between the condensation dehydrator and the isomerism reaction kettle. According to the utility model, by starting the material suction pump, when the material suction pump is started, turpentine floating above the water surface enters the interior of the oil suction pipe, then enters the interior of the rectangular pipe, finally enters the interior of the second connecting pipe through the first connecting pipe, and finally enters the interior of the isomerization reaction kettle through the oil conveying pipe, so that the water content of turpentine entering the interior of the isomerization reaction kettle can be greatly reduced, the dehydration operation of turpentine is realized, and the reaction time of turpentine in the interior of the isomerization reaction kettle is greatly reduced.
Description
Technical Field
The utility model relates to the technical field of turpentine isomerization reaction, in particular to an isomerization reaction condensation dehydration device.
Background
Turpentine isomerization reaction is an important link in camphene production, and isomerization reaction time and conversion rate influence production efficiency and product yield. The original isomerization reaction time is long, generally about 30 hours, and the camphene content of the isomerization liquid is 67-70%;
experiments show that turpentine contains a small amount of water, the isomerization reaction is heated to 132+/-2 ℃, the water continuously flows back in the reaction kettle, and the reaction time is long when the isomerization reaction exists.
Disclosure of Invention
In order to overcome the above disadvantages, the present utility model provides an isomerism reaction condensation dehydration apparatus which overcomes the above technical problems or at least partially solves the above problems.
The utility model is realized in the following way:
the utility model provides a condensation dehydration device for isomerization reaction, which comprises an isomerization reaction kettle, wherein a condensation dehydrator is arranged at one side of the isomerization reaction kettle, a suction pump and an oil delivery pipe are arranged at one side of the isomerization reaction kettle, and the suction pump and the oil delivery pipe are positioned between the condensation dehydrator and the isomerization reaction kettle;
the condensing dehydrator comprises a shell, wherein the top surface and the bottom surface of the shell are respectively and fixedly connected with a top plate and a bottom plate, and the outer surface of the shell is respectively and fixedly connected with a water inlet pipe and a water outlet pipe;
the preheating assembly comprises a plurality of heating rods, and the plurality of heating rods are equally spaced on the top surface of the bottom plate.
In a preferred scheme, the inside of shell is provided with cursory, be provided with the haulage rope between the bottom surface of cursory and the top surface of bottom plate, the top surface fixed connection of one end and bottom plate of haulage rope, the other end and the bottom surface fixed connection of cursory of haulage rope.
In a preferred scheme, two oil suction pipes are fixedly connected to the inside of the buoy, rectangular pipes are fixedly connected to the top ends of the oil suction pipes, first connecting pipes are fixedly connected to the top surfaces of the rectangular pipes, and second connecting pipes are fixedly connected to the top ends of the first connecting pipes.
In a preferred scheme, the other end of the second connecting pipe is fixedly connected with a material suction port of a material suction pump, a material discharge port of the material suction pump is fixedly connected with one end of an oil delivery pipe, and the other end of the oil delivery pipe is fixedly connected with the heterogeneous reaction kettle and extends to the inside of the heterogeneous reaction kettle.
In a preferred scheme, the bottom surface of bottom plate is provided with the battery box, the inside fixed mounting of battery box has the battery, one side surface fixed mounting of battery box has control switch.
In a preferred scheme, both sides of the battery box are fixedly provided with fixing plates, and the inside of each fixing plate is sleeved with a mounting bolt in a threaded manner.
In a preferred embodiment, a plurality of reinforcing rods are provided between the top plate and the bottom plate, and the plurality of reinforcing rods are installed between the top plate and the bottom plate at equal intervals.
In a preferred embodiment, the control switch is electrically connected to a battery, and the battery is electrically connected to the heating rod.
The utility model provides a isomerism reaction condensing and dehydrating device, which has the beneficial effects that:
1. through setting up the condensation dehydrator, through starting the material pump that absorbs, when the material pump starts, the turpentine of floating above the surface of water enters into the inside of inhaling oil pipe, then enters into the inside of rectangular pipe, enters into the inside of second connecting pipe by first connecting pipe at last, enters into the inside of isomerism reation kettle through the oil pipe, consequently enters into the inside turpentine's of isomerism reation kettle moisture content can be great reduction to the realization is to the dehydration operation of turpentine, thereby has reduced the reaction time of turpentine in isomerism reation kettle inside greatly.
2. Through setting up preheating assembly, the battery through control switch control battery case inside is circular telegram the heating rod, preheats the turpentine that enters into the shell inside to realized after the turpentine that the dehydration was accomplished enters into the inside of isomerism reation kettle, there is certain temperature, further reduced isomerism reation kettle heating time.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present utility model, the drawings that are needed in the embodiments will be briefly described below, it being understood that the following drawings only illustrate some examples of the present utility model and therefore should not be considered as limiting the scope, and other related drawings may be obtained according to these drawings without inventive effort for a person skilled in the art.
FIG. 1 is a flow chart of a turpentine reaction provided by an embodiment of the present utility model;
fig. 2 is a schematic structural diagram of a condensation dehydration device according to an embodiment of the present utility model;
FIG. 3 is a schematic cross-sectional view of a condensing and dehydrating device according to an embodiment of the present utility model;
fig. 4 is a schematic bottom view of a condensation dehydration device according to an embodiment of the present utility model.
In the figure: 1. an isomerism reaction kettle; 2. condensing and dehydrating device; 3. a suction pump; 4. an oil delivery pipe; 5. a housing; 6. a top plate; 7. a bottom plate; 8. a water inlet pipe; 9. a water outlet pipe; 10. a first connection pipe; 11. a second connection pipe; 13. a reinforcing rod; 14. a rectangular tube; 15. an oil suction pipe; 16. a float; 17. a traction rope; 18. a heating rod; 19. a battery box; 20. a control switch; 21. a fixing plate; 22. and (5) installing a bolt.
Detailed Description
For the purpose of making the objects, technical solutions and advantages of the embodiments of the present utility model more apparent, the technical solutions of the embodiments of the present utility model will be clearly and completely described below with reference to the accompanying drawings in the embodiments of the present utility model, and it is apparent that the described embodiments are some embodiments of the present utility model, but not all embodiments. All other embodiments, based on the embodiments of the utility model, which are apparent to those of ordinary skill in the art without inventive faculty, are intended to be within the scope of the utility model.
Examples
Referring to fig. 1-4, the present utility model provides a technical solution: the isomerism reaction condensation dehydration device comprises an isomerism reaction kettle 1, wherein a condensation dehydrator 2 is arranged on one side of the isomerism reaction kettle 1, a suction pump 3 and an oil delivery pipe 4 are arranged on one side of the isomerism reaction kettle 1, the suction pump 3 and the oil delivery pipe 4 are positioned between the condensation dehydrator 2 and the isomerism reaction kettle 1, a plurality of reinforcing rods 13 are arranged between a top plate 6 and a bottom plate 7, the reinforcing rods 13 are arranged between the top plate 6 and the bottom plate 7 at equal intervals, and the reinforcing rods 13 are stainless steel rods, so that a good reinforcing effect can be achieved;
the condensing dehydrator 2 comprises a shell 5, a top surface and a bottom surface of the shell 5 are respectively and fixedly connected with a top plate 6 and a bottom plate 7, an outer surface of the shell 5 is respectively and fixedly connected with a water inlet pipe 8 and a water outlet pipe 9, a buoy 16 is arranged in the shell 5, a traction rope 17 is arranged between the bottom surface of the buoy 16 and the top surface of the bottom plate 7, one end of the traction rope 17 is fixedly connected with the top surface of the bottom plate 7, the other end of the traction rope 17 is fixedly connected with the bottom surface of the buoy 16, two oil suction pipes 15 are fixedly connected in the buoy 16, the top ends of the oil suction pipes 15 are fixedly connected with rectangular pipes 14, the top surface of the rectangular pipes 14 is fixedly connected with a first connecting pipe 10, the top end of the first connecting pipe 10 is fixedly connected with a second connecting pipe 11, the other end of the second connecting pipe 11 is fixedly connected with a suction port of the suction pump 3, the discharge port of the suction pump 3 is fixedly connected with one end of the oil delivery pipe 4, the other end of the oil delivery pipe 4 is fixedly connected with the isomerization reaction kettle 1 and extends into the isomerization reaction kettle 1, when the suction pump 3 is started, turpentine floating above the water surface enters into the interior of the oil suction pipe 15 and then enters into the interior of the rectangular pipe 14, finally enters into the interior of the second connecting pipe 11 through the first connecting pipe 10 and finally enters into the isomerization reaction kettle 1 through the oil delivery pipe 4, so that the water content of turpentine entering into the isomerization reaction kettle 1 can be greatly reduced, the dehydration operation of turpentine is realized, and the reaction time of turpentine in the isomerization reaction kettle 1 is greatly reduced;
the preheating component comprises a plurality of heating rods 18, the heating rods 18 are uniformly arranged on the top surface of the bottom plate 7 at equal intervals, a battery box 19 is arranged on the bottom surface of the bottom plate 7, a storage battery is fixedly arranged in the battery box 19, a control switch 20 is fixedly arranged on one side surface of the battery box 19, the control switch 20 is electrically connected with the storage battery, the storage battery is electrically connected with the heating rods 18, the control switch 20 is used for controlling the storage battery in the battery box 19 to electrify the heating rods 18 and preheat turpentine entering the shell 5, therefore, after the dehydrated turpentine enters the isomerization reaction kettle 1, a certain temperature exists, the heating time of the isomerization reaction kettle 1 is further reduced, a fixing plate 21 is fixedly arranged on two sides of the battery box 19, a mounting bolt 22 is sleeved on the inner portion of the fixing plate 21 in a threaded manner, and the battery box 19 can be conveniently and rapidly mounted on the bottom surface of the bottom plate 7 through the fixing plate 21 and the mounting bolt 22.
Specifically, the working process or working principle of the isomerism reaction condensation dehydration device is as follows: when the turpentine dehydrator is used, turpentine firstly enters the shell 5 from the water inlet pipe 8, then the buoy 16 floats above the liquid level under the action of buoyancy, then the density of oil is smaller than that of water, so that turpentine floats above the water surface, then the turpentine enters the inside of the oil suction pipe 15 by starting the oil suction pump 3, the turpentine floats above the water surface enters the inside of the rectangular pipe 14 when the oil suction pump 3 is started, finally enters the inside of the second connecting pipe 11 from the first connecting pipe 10, finally enters the inside of the isomerization reaction kettle 1 from the oil conveying pipe 4, the water content of turpentine entering the inside of the isomerization reaction kettle 1 can be greatly reduced, the reaction time of turpentine in the isomerization reaction kettle 1 is greatly reduced, the condition that a small amount of water is contained in the existing turpentine is heated to 132+/-2 ℃ in the reaction kettle is avoided, the reaction time can be long when the water exists, and the storage battery box 19 is controlled by the control switch 20 to control the inside of the storage battery to enter the inside of the isomerization reaction kettle 1 when the dehydration operation is performed, the turpentine is heated to the inside of the isomerization reaction kettle 1, and the temperature of the isomerization reaction kettle is further reduced, and the turpentine enters the inside of the isomerization reaction kettle 1 is heated to a certain time after the isomerization reaction kettle is heated, and the inside of the isomerization reaction kettle is further heated to be heated.
It should be noted that, the suction pump 3 and the heating rod 18 are devices or apparatuses existing in the prior art, or are devices or apparatuses that can be implemented in the prior art, and the power supply, the specific composition and the principle thereof are clear to those skilled in the art, so they will not be described in detail.
Claims (8)
1. The isomerism reaction condensation dehydration device comprises an isomerism reaction kettle (1), and is characterized in that a condensation dehydrator (2) is arranged on one side of the isomerism reaction kettle (1), a suction pump (3) and an oil delivery pipe (4) are arranged on one side of the isomerism reaction kettle (1), and the suction pump (3) and the oil delivery pipe (4) are positioned between the condensation dehydrator (2) and the isomerism reaction kettle (1);
the condensing dehydrator (2) comprises a shell (5), wherein a top plate (6) and a bottom plate (7) are respectively and fixedly connected with the top surface and the bottom surface of the shell (5), and a water inlet pipe (8) and a water outlet pipe (9) are respectively and fixedly connected with the outer surface of the shell (5);
the preheating assembly comprises a plurality of heating rods (18), and the plurality of heating rods (18) are equally spaced on the top surface of the bottom plate (7).
2. The isomerism reaction condensation dehydration device according to claim 1, characterized in that a buoy (16) is arranged in the shell (5), a haulage rope (17) is arranged between the bottom surface of the buoy (16) and the top surface of the bottom plate (7), one end of the haulage rope (17) is fixedly connected with the top surface of the bottom plate (7), and the other end of the haulage rope (17) is fixedly connected with the bottom surface of the buoy (16).
3. The isomerism reaction condensation dehydration device according to claim 2, characterized in that the inside of the buoy (16) is fixedly connected with two oil suction pipes (15), the top ends of the oil suction pipes (15) are fixedly connected with rectangular pipes (14), the top surface of each rectangular pipe (14) is fixedly connected with a first connecting pipe (10), and the top end of each first connecting pipe (10) is fixedly connected with a second connecting pipe (11).
4. The isomerism reaction condensation dehydration device according to claim 3, wherein the other end of the second connecting pipe (11) is fixedly connected with a suction port of a suction pump (3), a discharge port of the suction pump (3) is fixedly connected with one end of an oil delivery pipe (4), and the other end of the oil delivery pipe (4) is fixedly connected with the isomerism reaction kettle (1) and extends to the inside of the isomerism reaction kettle (1).
5. The isomerism reaction condensation dehydration device according to claim 1, characterized in that a battery box (19) is arranged on the bottom surface of the bottom plate (7), a storage battery is fixedly arranged in the battery box (19), and a control switch (20) is fixedly arranged on one side surface of the battery box (19).
6. The isomerism reaction condensation dehydration device according to claim 5, wherein both sides of the battery box (19) are fixedly provided with a fixing plate (21), and the inside of the fixing plate (21) is sheathed with a mounting bolt (22) by screw threads.
7. The isomerism reaction condensation dehydration device according to claim 1, characterized in that a plurality of reinforcing rods (13) are arranged between the top plate (6) and the bottom plate (7), and the reinforcing rods (13) are equally spaced between the top plate (6) and the bottom plate (7).
8. The apparatus according to claim 5, wherein the control switch (20) is electrically connected to a battery, and the battery is electrically connected to the heating rod (18).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320246015.0U CN219167749U (en) | 2023-02-17 | 2023-02-17 | Isomerism reaction condensation dewatering device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202320246015.0U CN219167749U (en) | 2023-02-17 | 2023-02-17 | Isomerism reaction condensation dewatering device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN219167749U true CN219167749U (en) | 2023-06-13 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202320246015.0U Active CN219167749U (en) | 2023-02-17 | 2023-02-17 | Isomerism reaction condensation dewatering device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN219167749U (en) |
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2023
- 2023-02-17 CN CN202320246015.0U patent/CN219167749U/en active Active
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