CN218689346U - Reaction device with temperature control device - Google Patents

Reaction device with temperature control device Download PDF

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Publication number
CN218689346U
CN218689346U CN202223020541.XU CN202223020541U CN218689346U CN 218689346 U CN218689346 U CN 218689346U CN 202223020541 U CN202223020541 U CN 202223020541U CN 218689346 U CN218689346 U CN 218689346U
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temperature control
reaction
temperature
control device
reaction device
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CN202223020541.XU
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易小芳
谭伟新
潘琳
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LINGNAN PHARMACEUTICAL Ltd
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LINGNAN PHARMACEUTICAL Ltd
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Abstract

The utility model belongs to the technical field of the reation kettle technique and specifically relates to reaction unit with temperature control device, including the operation panel and install in reaction unit, refrigerating plant and electronic box on the operation panel, integrated heating device and temperature control device on the electronic box, temperature control device including integrated in temperature controller on the electronic box and put in the reaction unit and with the temperature detection module that the temperature controller electricity is connected, be equipped with in the reaction unit respectively with refrigerating plant with the heat pipe that heating device connects, refrigerating plant with heating device respectively with the temperature controller electricity is connected. The application provides a reaction unit with temperature control device, its suitability and the precision of adjusting the temperature are higher, and the operating personnel of being convenient for carries out the experiment under the multiple different reaction condition.

Description

Reaction device with temperature control device
[ technical field ] A method for producing a semiconductor device
The utility model belongs to the technical field of reaction unit technique and specifically relates to reaction unit with temperature control device.
[ background of the invention ]
The reaction kettle is a reaction device, raw materials complete various reactions in a reaction device to generate new substances or change partial characteristics of the raw materials, and the reaction kettle is widely used in chemical and pharmaceutical industries. At present, a reaction kettle is needed in general chemical reactions, and when the temperature of the existing reaction kettle is regulated and controlled, the temperature of the existing reaction kettle is mainly regulated and controlled by connecting a heating pipe or a refrigerating guide pipe, and the heating pipe or the refrigerating guide pipe is stopped to work after the set temperature is reached, so that the temperature is difficult to regulate and control between required temperatures, and in an experiment stage, various reaction conditions are required to be tried for experiments, particularly for the regulation and control in the temperature aspect, the existing reaction device is difficult to accurately regulate and control, and the requirements of the experiments are difficult to achieve.
[ Utility model ] content
An object of the utility model is to provide a reaction unit with temperature control device, its suitability and the precision of adjusting the temperature are higher, and the operating personnel of being convenient for carries out the experiment under the multiple different reaction condition.
The application is realized by the following technical scheme: the reaction device with the temperature control device comprises an operation table, and a reaction device, a refrigerating device and an electric box which are arranged on the operation table, wherein a heating device and a temperature control device are integrated on the electric box, the temperature control device comprises a temperature controller which is integrated on the electric box, and a temperature detection module which is placed in the reaction device and is electrically connected with the temperature controller, a heat conduction pipe which is respectively connected with the refrigerating device and the heating device is arranged in the reaction device, the refrigerating device and the heating device are respectively electrically connected with the temperature controller, and when the reaction device works, the temperature controller switches and controls the refrigerating device or the heating device so as to regulate and control the temperature in the reaction device to the required temperature.
The reaction device with the temperature control device comprises a magnetic stirring table erected on the operating table and electrically connected with the electric box, and a thermostat pot arranged on the magnetic stirring table, wherein the thermostat pot is further provided with a containing cavity for embedding the heat conduction pipe.
According to the reaction device with the temperature control device, the thermostatic pot comprises the pot body and the upper cover covering the pot body, and the outer sides of the pot body and the upper cover are respectively provided with the heat insulation layers.
According to the reaction device with the temperature control device, the magnetic stirring table further comprises a fixing support which is arranged corresponding to the constant temperature pot and used for fixing the reactor.
In the reaction apparatus with a temperature control device, the fixing bracket includes a first supporting rod fixed on the magnetic stirring table, a fixing member detachable from the first supporting rod, a second supporting rod detachable from the fixing member, and a clamping assembly mounted on the second supporting rod for fixing the reactor.
The reaction device with the temperature control device comprises a first clamping part fixed on the second support rod, a second clamping part with one end hinged to the first clamping part, a screw rod penetrating through the first clamping part and the second clamping part, and an adjusting nut sleeved on one end of the screw rod.
The reaction device with the temperature control device as described above, the refrigeration device includes a heat exchanger and a refrigeration compressor electrically connected to the electric box, respectively, and the heat pipes are connected to the heating device and the refrigeration compressor, respectively, to conduct heat.
In the reaction apparatus having the temperature control device as described above, the operation table includes an operation table main body and a moving wheel attached to a lower end of the operation table main body.
In the reaction device with a temperature control device as described above, a partition is provided on a side of the console body close to the cooling device.
Compared with the prior art, the method has the following advantages:
the utility model discloses a reaction unit with temperature control device, through setting for the temperature control appearance is to required temperature, by the temperature control appearance switches heating device or refrigerating plant work to carry out temperature control when reacing required temperature, its suitability and the precision of adjusting temperature are higher, and the operating personnel of being convenient for carries out the experiment under the multiple different reaction condition.
[ description of the drawings ]
In order to more clearly illustrate the technical solutions in the embodiments of the present application, the drawings needed to be used in the description of the embodiments are briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present application, and it is obvious for those skilled in the art to obtain other drawings based on these drawings without creative efforts.
FIG. 1 is a schematic view of the structure of a reaction apparatus according to an embodiment of the present application.
FIG. 2 is an exploded view of a reaction apparatus according to an embodiment of the present application.
[ detailed description ] embodiments
In order to make the technical problems, technical solutions and advantageous effects solved by the present application more clear and obvious, the present application is further described in detail below with reference to the accompanying drawings and embodiments. It should be understood that the specific embodiments described herein are merely illustrative of the present application and are not intended to limit the present application.
As shown in fig. 1-2, the embodiment of the present application provides a reaction apparatus with a temperature control device, including an operation table 1, and a reaction apparatus 2, a refrigeration apparatus 3 and an electrical box 4 installed on the operation table 1, the electrical box 4 is integrated with a heating device 41 and a temperature control device 42, the temperature control device 42 includes a temperature controller 43 integrated on the electrical box 4, and a temperature detection module 44 placed in the reaction apparatus 2 and electrically connected to the temperature controller 43, the reaction apparatus 2 is provided with a heat pipe 21 connected to the refrigeration apparatus 3 and the heating device 41, respectively, the refrigeration apparatus 3 and the heating device 41 are electrically connected to the temperature controller 43, respectively, when the reaction apparatus 2 operates, the temperature controller 43 controls the refrigeration apparatus 3 or the heating device 41 to control the temperature in the reaction apparatus 2 to a desired temperature, in the reaction apparatus of the existing experiment, various reaction conditions need to be tried, it is difficult for the existing reaction apparatus to achieve temperature control, the heat pipe 21 is connected to the refrigeration apparatus 3 and the heating device 41, the temperature controller 43 is switched to a desired temperature, and the reaction apparatus is capable of adjusting the temperature of adjusting the reaction conditions of the reaction apparatus to a variety of temperature, and adjusting the reaction apparatus is convenient for a high temperature adjustment, and a high temperature adjustment range of reaction apparatus, and a high accuracy of the reaction apparatus is convenient for a variety of reaction apparatus 20-20 ℃.
Reaction unit 2 is including setting up in on the operation panel 1 and with magnetic stirring platform 22 that 4 electricity of electronic box are connected and set up in thermostatic pot 23 on the magnetic stirring platform 22, still be equipped with the confession on the thermostatic pot 23 the holding chamber 24 of heat pipe 21 embedding, thermostatic pot 23 can change heat transfer medium as required, and when the service temperature is less than the temperature of 0 degree centigrade, can use not frozen liquid or silicon oil, when the service temperature is higher than 0 degree centigrade, can use water as the medium, through magnetic stirring platform 22 control stirring speed, stirs the heat transfer medium in reaction material and the thermostatic pot 23 simultaneously, and it can reach the temperature homogeneous, guarantees the normal clear of reaction.
Constant temperature pan 23 fits including pot body 25 and lid upper cover 26 on the pot body 25, pot body 25 with the outside of upper cover 26 is equipped with heat preservation 27 respectively, adopts heat preservation 27 to insulate against heat and keeps warm, avoids constant temperature pan 23 and external contact lead to the heat to run off.
The magnetic stirring table 22 further comprises a fixing support 28 which is arranged corresponding to the thermostatic pot 23 and used for fixing a reactor, wherein the fixing support 28 comprises a first supporting rod 281 fixed on the magnetic stirring table 22, a fixing member 282 detachable on the first supporting rod 281, a second supporting rod 283 detachable on the fixing member 282, and a clamping assembly 284 which is arranged on the second supporting rod 283 and used for fixing the reactor, the reactor can be selected to be 50ml-2000ml in size, the clamping assembly 284 comprises a first clamping part 285 fixed on the second supporting rod 283, a second clamping part 286 with one end hinged to the first clamping part 285, a screw 287 arranged on the first clamping part 285 and the second clamping part 286, and an adjusting nut 288 arranged on one end of the screw 287, the sizes of the openings of the first clamping part 285 and the second clamping part 286 are adjusted through the screw 287 and the adjusting nut 288, and the clamping stability is higher.
The cooling device 3 includes a heat exchanger 31 and a cooling compressor 32 electrically connected to the electric box 4, respectively, and the heat pipe 21 is connected to the heating device 41 and the cooling compressor 32, respectively, to conduct heat.
The operating table 1 comprises an operating table main body 11 and a moving wheel 12 arranged at the lower end of the operating table main body 11, so that an operator can move conveniently; operation panel main part 11 is close to be provided with baffle 13 on one side of refrigerating plant 3, when refrigerating plant 3 carries out the work heat transfer, to outer heat dissipation, install baffle 13 avoids operating personnel direct contact refrigerating plant 3 prevents to scald, and the security is higher.
In summary, the present application has, but is not limited to, the following beneficial effects:
the utility model discloses a reaction unit with temperature control device, including operation panel 1 and install in reaction unit 2, refrigerating plant 3 and electronic box 4 on the operation panel 1, integrated heating device 41 and temperature control device 42 on the electronic box 4, temperature control device 42 including integrated in temperature control appearance 43 on the electronic box 4 and put in reaction unit 2 and with the temperature detection module 44 that temperature control appearance 43 electricity is connected, be equipped with respectively in reaction unit 2 with refrigerating plant 3 with the heat pipe 21 that heating device 41 is connected, refrigerating plant 3 with heating device 41 respectively with temperature control appearance 43 electricity is connected during reaction unit 2 operation, temperature control appearance 43 switching control refrigerating plant 3 or heating device 41 is with regulation and control temperature in the reaction unit 2 to required temperature, in the reaction unit of present experiment, various reaction conditions need be tried to experiment, and present reaction unit is difficult to realize temperature regulation and control, will heat pipe 21 connects respectively refrigerating plant 3 with heating device 41, and by temperature control appearance 43 switches control appearance 43 in the reaction unit to the temperature control appearance is switched over to the reaction unit is higher temperature regulation and control personnel's temperature regulation and is the higher reaction condition of being convenient for carrying out the accuracy under the multiple reaction unit 2-20 ℃ of adjusting temperature.
The foregoing is illustrative of one or more embodiments provided in connection with the detailed description and is not intended to limit the disclosure to the particular forms disclosed. Similar or identical methods, structures, etc. as used herein, or several technical inferences or substitutions made on the concept of the present application should be considered as the scope of the present application.

Claims (9)

1. The reaction device with the temperature control device is characterized by comprising an operation table (1), and a reaction device (2), a refrigerating device (3) and an electric box (4) which are arranged on the operation table (1), wherein the electric box (4) is integrated with a heating device (41) and a temperature control device (42), the temperature control device (42) comprises a temperature controller (43) which is integrated on the electric box (4) and a temperature detection module (44) which is placed in the reaction device (2) and is electrically connected with the temperature controller (43), a heat conduction pipe (21) which is respectively connected with the refrigerating device (3) and the heating device (41) is arranged in the reaction device (2), the refrigerating device (3) and the heating device (41) are respectively and electrically connected with the temperature controller (43), and when the reaction device (2) operates, the temperature controller (43) switches and controls the refrigerating device (3) or the heating device (41) so as to regulate and control the temperature in the reaction device (2) to the required temperature.
2. The reaction device with the temperature control device according to claim 1, wherein the reaction device (2) comprises a magnetic stirring table (22) erected on the operation table (1) and electrically connected with the electric box (4), and a thermostatic pot (23) arranged on the magnetic stirring table (22), and the thermostatic pot (23) is further provided with a containing cavity (24) for embedding the heat conducting pipe (21).
3. The reaction device with the temperature control device according to claim 2, wherein the thermostatic pot (23) comprises a pot body (25) and an upper cover (26) covering the pot body (25), and the outer sides of the pot body (25) and the upper cover (26) are respectively provided with an insulating layer (27).
4. The reaction device with temperature control device according to claim 2, characterized in that the magnetic stirring table (22) further comprises a fixing bracket (28) corresponding to the thermostat pot (23) for fixing the reactor.
5. The reaction apparatus with temperature control device according to claim 4, wherein the fixing bracket (28) comprises a first supporting rod (281) fixed on the magnetic stirring table (22), a fixing member (282) detachable from the first supporting rod (281), a second supporting rod (283) detachable from the fixing member (282), and a clamping assembly (284) mounted on the second supporting rod (283) for fixing the reactor.
6. The reaction device with the temperature control device as claimed in claim 5, wherein the clamping assembly (284) comprises a first clamping portion (285) fixed on the second support rod (283), a second clamping portion (286) having one end hinged to the first clamping portion (285), a screw rod (287) passing through the first clamping portion (285) and the second clamping portion (286), and an adjusting nut (288) sleeved on one end of the screw rod (287).
7. The reaction device with temperature control device according to claim 1, characterized in that the refrigeration device (3) comprises a heat exchanger (31) and a refrigeration compressor (32) electrically connected with the electric box (4), respectively, the heat conduction pipes (21) being connected with the heating device (41) and the refrigeration compressor (32), respectively, to conduct heat.
8. The reaction apparatus having a temperature control apparatus according to claim 1, wherein the operation table (1) comprises an operation table main body (11) and a moving wheel (12) attached to a lower end of the operation table main body (11).
9. The reaction device with temperature control device according to claim 8, characterized in that a partition plate (13) is provided on a side of the console body (11) close to the cooling device (3).
CN202223020541.XU 2022-11-14 2022-11-14 Reaction device with temperature control device Active CN218689346U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202223020541.XU CN218689346U (en) 2022-11-14 2022-11-14 Reaction device with temperature control device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202223020541.XU CN218689346U (en) 2022-11-14 2022-11-14 Reaction device with temperature control device

Publications (1)

Publication Number Publication Date
CN218689346U true CN218689346U (en) 2023-03-24

Family

ID=85617462

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202223020541.XU Active CN218689346U (en) 2022-11-14 2022-11-14 Reaction device with temperature control device

Country Status (1)

Country Link
CN (1) CN218689346U (en)

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