CN217745811U - Extraction and separation purification device of ursolic acid - Google Patents

Abstract

The utility model discloses an extraction and separation purification device of ursolic acid, including support frame and supplementary filter equipment. The utility model discloses a set up supplementary filter equipment, under rose box and filter plate cooperation, can realize ursolic acid solution auxiliary filtration, and set up the adjusting part cooperation at filter plate middle part lower extreme under, can realize that the filter plate changes the use, guarantee the stability of filter effect, thereby the advantage of ursolic acid solution auxiliary filtration processing and filter department quick adjustment change use has been reached, and set up the flushing assembly on the inside right side of rose box, at the gear, the drive plate with remove frame cooperation transmission under, it can realize the reciprocal pulling of flushing machine to remove the frame, make the flushing machine realize reciprocal quick washing to the filter plate, improve the filter plate cleaning performance, thereby reached the supplementary quick washing of old filter plate, guarantee filter plate life's advantage.

Description

Extraction and separation purification device of ursolic acid

Technical Field

The utility model relates to an ursolic acid draws and separation and purification related field, especially relates to an extraction and separation and purification device of ursolic acid.

Background

Ursolic acid is also called ursolic acid, is a pentacyclic triterpenoid, is insoluble in water and petroleum ether, is easily soluble in dioxane, pyridine, ethanol and methanol, is widely existed in plants such as hawthorn, plantain herb, common selfheal fruit-spike, glossy privet fruit, rabdosia rubescens, spreading hedyotis herb and the like, has obvious effects of resisting inflammation, resisting tumor, resisting hepatitis, resisting diabetes and the like, is extracted and separated from the plants, and is extracted and separated from the plants.

At present when carrying out ursolic acid and draw and separation and purification device's use, draw and separate and purification device although can be fine realize the extraction and purification of ursolic acid, nevertheless in the process of drawing, the filtration measure often sets up inside equipment, leads to repetitious usage back, and unable fine change leads to not clearing up filtration department, leads to the ursolic acid solution quality to cause the influence easily.

SUMMERY OF THE UTILITY MODEL

Therefore, in order to solve the above insufficiency, the utility model provides an extraction and separation purification device of ursolic acid.

In order to achieve the purpose, the utility model adopts the following technical scheme: the utility model provides an ursolic acid draws and separation purification device, includes support frame and supplementary filter equipment, a processing section of thick bamboo is installed to the support frame upper end to processing section of thick bamboo upper end left side has seted up the feed inlet, the feed inlet right side is provided with DC motor relatively, the DC motor lower extreme is connected with the puddler, first notes liquid mouth and second notes liquid mouth have been seted up respectively to processing section of thick bamboo right side upper and lower both ends to the inside middle-end of processing section of thick bamboo is pegged graft mutually and is had first drain pipe, the inside lower extreme left and right sides of processing section of thick bamboo all is equipped with the hot plate, and has pegged graft mutually in the inside lower extreme middle part of processing section of thick bamboo and have the second drain pipe, supplementary filter equipment sets up in the support frame lower extreme, supplementary filter equipment includes rose box, filter plate, first outlet pipe, second outlet pipe, adjusting part and flushing part, rose box and support frame lower extreme fastening connection to the inside upper end of rose box is provided with the filter plate, rose box right side is pegged graft mutually respectively has first outlet pipe and second outlet pipe, adjusting part sets up in middle part lower extreme, flushing part sets up in the filter box inside upper end.

Preferably, the adjusting component comprises a shell, a motor, a rotating frame, a connecting rod, a rotating cylinder and an inserting rod, the left side of the shell is fixedly connected with the filter box, the motor is installed on the right side inside the shell, the front side of the motor is connected with the rotating frame, the connecting rod is installed at the upper end and the lower end of the middle of the rotating frame, the rotating cylinder and the rotating frame are oppositely arranged left and right, the rotating cylinder is inserted into the lower end of the inserting rod, and the upper end of the inserting rod is fixedly connected with the filter plate.

Preferably, the flushing assembly comprises a protective shell, a flushing machine, a moving frame, a driving plate, a gear and a driving motor, the upper end of the protective shell is fixedly connected with the filter box, the flushing machine is installed on the left side inside the protective shell, the left side of the flushing machine is communicated with the filter box, the right side of the flushing machine is connected with the moving frame, the moving frame is slidably connected with the inside of the protective shell, the driving plate is slidably connected with the inside of the moving frame, the right end of the front side of the driving plate is connected with the gear in a meshed mode, and the front side of the gear is connected with the driving motor.

Preferably, the lower end in the filter box inclines towards the lower right corner, and the first water outlet pipe and the second water outlet pipe arranged on the right side of the filter box are symmetrical up and down.

Preferably, the left side and the right side of the rotating frame are both in a semi-arc shape, and the left side and the right side of the rotating frame are both in sliding insertion connection with the rotating cylinder.

Preferably, the outer side of the middle part of the rotating cylinder is provided with a crossed groove, and the inner wall of the groove formed in the rotating cylinder is smooth.

Preferably, the spraying position of the lower end of the flushing machine inclines towards the right side, and the lower end of the flushing machine is opposite to the other filter plate up and down.

Preferably, the driving plate is transversely arranged along a hollow part in the movable frame, and a plurality of arc-shaped grooves and circular convex parts are respectively arranged on the front side of the driving plate.

The utility model has the advantages that:

the method has the advantages that: the utility model discloses a set up supplementary filter equipment, under rose box and filter plate cooperation, can realize ursolic acid solution and assist the filtration, and under the cooperation of filter plate middle part lower extreme setting adjusting part, can realize that the filter plate changes the use, guarantee the stability of filter effect to reach ursolic acid solution and assisted filtration treatment and the quick adjustment of filter department and changed the advantage of using.

The method has the advantages that: the utility model discloses a set up the washing subassembly in the inside right side upper end of rose box, under gear, drive plate and removal frame cooperation transmission, remove the frame and can realize the reciprocal pulling of flushing machine, make the flushing machine realize reciprocal quick washing to the filter plate, improve the filter plate cleaning performance to reached the supplementary quick washing of old filter plate, guaranteed filter plate life's advantage.

Drawings

FIG. 1 is a schematic structural view of the present invention;

FIG. 2 is a schematic view of the front cross-sectional structure of the present invention;

FIG. 3 is a schematic view of the front cross-sectional structure of the auxiliary filtering device of the present invention;

FIG. 4 is a schematic view of the front cross-sectional structure of the adjusting assembly of the present invention;

FIG. 5 is a schematic structural view of a three-dimensional portion of the adjusting assembly of the present invention;

FIG. 6 is a front view of the inner structure of the flushing assembly of the present invention;

fig. 7 is a schematic structural view of a three-dimensional part of the flushing assembly of the present invention.

Wherein: the device comprises a support frame-1, a treatment barrel-2, a feed inlet-3, a direct current motor-4, a stirring rod-5, a first liquid injection port-6, a second liquid injection port-7, a first water discharge pipe-8, a heating plate-9, a second water discharge pipe-10, an auxiliary filtering device-11, a filtering box-111, a filtering plate-112, a first water discharge pipe-113, a second water discharge pipe-114, a regulating component-115, a flushing component-116, a shell-1151, a motor-1152, a rotating frame-1153, a connecting rod-1154, a rotating barrel-1155, a splicing rod-1156, a protective shell-1161, a flushing machine-1162, a moving frame-1163, a driving plate-1164, a gear-1165 and a driving motor-1166.

Detailed Description

In order to further explain the technical solution of the present invention, the following detailed description is given by way of specific examples.

Please refer to fig. 1-2, the utility model provides an ursolic acid draws and separation purification device, including support frame 1 and auxiliary filter 11, a processing section of thick bamboo 2 is installed to support frame 1 upper end, and 2 upper ends of a processing section of thick bamboo have seted up feed inlet 3, 3 right sides of feed inlet are provided with direct current motor 4 relatively, 4 lower extremes of direct current motor are connected with puddler 5, both ends have been seted up respectively about 2 right sides of a processing section of thick bamboo and have been annotated mouth 6 and second and annotate liquid mouth 7, and 2 inside middle-end phase pegs graft of a processing section of thick bamboo has first drain pipe 8, 2 inside lower extreme left and right sides of a processing section of thick bamboo all are equipped with hot plate 9, and 2 inside lower extreme middle parts of a processing section of thick bamboo are pegged graft mutually and are had second drain pipe 10.

Referring to fig. 3, the auxiliary filtering device 11 is disposed at the lower end of the support frame 1, the auxiliary filtering device 11 includes a filtering box 111, a filtering plate 112, a first water outlet pipe 113, a second water outlet pipe 114, a regulating component 115 and a flushing component 116, the filtering box 111 is fastened to the lower end of the support frame 1, and the filtering plate 112 is disposed at the upper end inside the filtering box 111, so that the filtering plate 112 achieves auxiliary filtering treatment of ursolic acid solution, the first water outlet pipe 113 and the second water outlet pipe 114 are respectively inserted into the right side of the filtering box 111, the regulating component 115 is disposed at the lower end of the middle of the filtering plate 112, so that the filtering plate 112 is quickly regulated and replaced by the regulating component 115, the flushing component 116 is disposed at the upper end inside the filtering box 111, so that the auxiliary filtering plate cleaning activity of the filtering plate 112 is achieved by the flushing component 116, the lower end inside the filtering box 111 is inclined towards the lower right side, and the first water outlet pipe 113 and the second water outlet pipe 114 disposed at the right side of the filtering box 111 are symmetrical up and down, so that the first water outlet pipe 113 and the second water outlet pipe 114 both achieve stable drainage activity.

Referring to fig. 4-5, the adjusting assembly 115 includes a housing 1151, a motor 1152, a rotating frame 1153, a connecting rod 1154, a rotating cylinder 1155 and an inserting rod 1156, the left side of the housing 1151 is fixedly connected to the filter box 111, and the motor 1152 is installed on the right side inside the housing 1151, so that the housing 1151 ensures the stability of installation of internal parts, the front side of the motor 1152 is connected to the rotating frame 1153, and the connecting rods 1154 are installed at the upper and lower ends of the middle portion of the rotating frame 1153, so that the rotating frame 1153 and the connecting rod 1154 are mutually matched to realize stable pushing movement, the rotating cylinder 1155 and the rotating frame 1153 are oppositely arranged on the left and right sides, and the rotating cylinder 1155 is inserted into the lower end of the inserting rod 1156, so that the rotating cylinder 1155 and the inserting rod 1156 realize stable inserting movement, the upper end of the inserting rod 1156 is fixedly connected to the filter plate 112, the left and right sides of the rotating frame 1153 are both in a semi-arc shape, and the left and right sides of the rotating frame 1153 are slidably inserted into the rotating cylinder 1155, so that the rotating cylinder 1155 realizes stable and intermittent movement.

Referring to fig. 6-7, the washing assembly 116 includes a protective shell 1161, a washing machine 1162, a moving frame 1163, a driving plate 1164, a gear 1165 and a driving motor 1166, the upper end of the protective shell 1161 is fixedly connected to the filter box 111, the washing machine 1162 is installed on the left side inside the protective shell 1161, so that the protective shell 1161 achieves safety protection of internal parts, the left side of the washing machine 1162 is communicated with the filter box 111, the right side of the washing machine 1162 is connected to the moving frame 1163, so that the washing machine 1162 achieves efficient auxiliary cleaning activities, the moving frame 1163 is connected to the protective shell 1161 in a sliding manner, the driving plate 1164 is connected to the moving frame 1163 in a sliding manner, so that the moving frame 1163 stably moves back and forth along the protective shell 1161, the gear 1165 is connected to the right end of the front side of the driving plate 1164 in a meshing manner, the driving plate 1165 achieves meshing stable connection activities, the spraying position of the lower end of the washing machine 1162 is inclined to the right side, the lower end of the washing machine 1162 is vertically opposite to the other washing machine 116112, so that the driving plate 1164 and the circular filter plate 1164 is transversely provided with a plurality of the circular filter plate 1164.

The working principle is as follows:

firstly, when the ursolic acid extraction, separation and purification device is used, ethyl acetate and clean water can be poured into the treatment cylinder 2 through the first liquid injection port 6, then the ursolic acid raw material can be poured through the feed port 3 formed on the left side of the upper end of the treatment cylinder 2, when the raw material contacts with the ethyl acetate solution, impurity removal activity can be realized, meanwhile, the direct current motor 4 arranged on the right side of the feed port 3 oppositely can be operated, the direct current motor 4 can realize the driving of the stirring rod 5 connected with the lower end, the stirring rod 5 can realize the stirring of the mixture at the lower end, the impurity removal efficiency of the ursolic acid raw material can be improved, after the impurity removal activity is completed, the raw material can be conveyed to the lower end in the treatment cylinder 2 through the first water discharge pipe 8 arranged at the middle end in the treatment cylinder 2, then, a worker pours alkaline water through a second liquid injection port 7, and performs heating activities by operating heating plates 9 arranged on the left and right sides of the lower end inside the treatment cylinder 2, so that the ursolic acid raw material and the alkaline water perform alkali-dissolving acid-precipitating activities, the ursolic acid in the ursolic acid raw material can be fully extracted after a period of heating and boiling activities, and finally, the quick treatment is realized by arranging a second drain pipe 10 in the middle of the lower end of the treatment cylinder 2, and in order to improve the quality of extracting the ursolic acid, the worker can perform multiple experimental productions through the properties of ethyl acetate dosage, alcohol concentration, acid-base dosage and the like, so that certain standard meets the high-quality production of the ursolic acid;

secondly, when the ursolic acid extracting, separating and purifying device is used, although the extracting, separating and purifying device can well realize the extraction and purification of the ursolic acid, in the extracting process, a filtering measure is often arranged in the device, so that after the device is used for multiple times, the filtering measure cannot be well replaced, the filtering position is not cleaned, and the quality of the ursolic acid solution is easily influenced;

thirdly, therefore, by arranging the auxiliary filtering device 11 at the lower end of the supporting frame 1, i.e. the ursolic acid can enter the interior of the filtering tank 111 along the second water discharging pipe 10 and contact with the filtering plate 112 arranged at the upper end of the interior of the filtering tank 111 to perform auxiliary filtering activity, so as to avoid the debris still existing in the interior of the ursolic acid to influence the subsequent processing effect, and the filtered ursolic acid can be discharged quickly along the first water discharging pipe 113 arranged at the lower end of the right side of the filtering tank 111, and for better realizing the filtering plate replacing activity, the filtering plate 112 can be rotated and replaced by operating the adjusting component 115 arranged at the lower end of the middle part of the filtering plate 112, firstly, by operating the motor 1152 arranged at the right side of the interior of the housing 1151, the motor 1152 is driven by the rotating frame 1153 connected with the front side, under the rotation of the rotating frame 1153, connecting rods 1154 are connected with the upper end and the lower end of the rotating frame 1153, the left side of the rotating frame 1153 can be pushed relative to the rotating cylinder 1155, the rotating cylinder 155 can rotate for 180 degrees intermittently, and then the middle part of the rotating cylinder 1155 is inserted with the insertion rod 1156, so that the left old filter plate 112 can be driven to rotate to the right side, and the right new filter plate 112 can be rotated to the lower end of the first drainage pipe 10, so that the re-filtration use is realized, and meanwhile, when the rotating frame 1153 rotates, the rotating cylinder 1154 can be blocked and moved under the matching of the left and right semi-arcs, so that the rotating cylinder 1155 is prevented from rotating for an overlarge angle, and the advantages of auxiliary filtration treatment of the ursolic acid solution and quick adjustment and replacement of a filtration part are achieved;

fourthly, in order to further ensure the use efficiency of the filter plates 112, the washing assembly 116 is further arranged at the upper end of the right side in the filter box 111 to realize the quick washing of the filter plates 112, that is, by operating the washing machine 1162, the old filter plates 112 at the right side can be washed, and in order to ensure the stability of the washing of the filter plates 112, the driving motor 1166 arranged at the front side of the gear 1165 is operated to drive the driving motor 1166 to be connected with the gear 1165 at the rear side, and under the rotation of the gear 1165, the gear 1165 can be matched with a plurality of round convex parts arranged at the front side of the driving plate 1164 to realize the left-right movement of the driving plate 1164, and under the left-right movement of the driving plate 1164, the moving frame 1163 is connected with the outer side of the driving plate 1164 in a sliding manner, so that the washing machine 1162 at the left side can realize the reciprocating washing of the filter plates 112, the full washing effect is ensured, and the sewage generated by washing can be discharged along the second water outlet pipe 114 arranged at the upper end of the right side of the filter box 111 to realize the quick washing of the old filter plates 112, thereby achieving the quick washing and ensuring the advantages of the auxiliary service life of the old filter plates 112.

The utility model provides an ursolic acid draw and separation and purification device, through setting up auxiliary filter 11, under rose box 111 and filter plate 112 cooperation, can realize ursolic acid solution auxiliary filter, and set up under adjusting part 115 cooperation at filter plate 112 middle part lower extreme, can realize filter plate 112 change use, guarantee the stability of filter effect, thereby the auxiliary filtration of ursolic acid solution is handled and the advantage of changing the use of filter department quick adjustment has been reached, and set up washing component 116 on rose box 111 inside right side upper end, at gear 1165, drive plate 1164 and removal frame 1163 cooperation transmission under, remove frame 1163 and can realize the reciprocal pulling of flushing machine 1162, make flushing machine 1162 realize reciprocal quick washing to filter plate 112, improve filter plate 112 cleaning performance, thereby reached the supplementary quick washing of old filter plate 112, guarantee filter plate 112 life's advantage.

Although the present invention has been described in detail with reference to the foregoing embodiments, it will be apparent to those skilled in the art that modifications may be made to the embodiments described in the foregoing embodiments, or equivalents may be substituted for elements thereof. Any modification, equivalent replacement, or improvement made within the spirit and principle of the present invention should be included in the protection scope of the present invention.

Claims (8)

1. An extraction, separation and purification device for ursolic acid comprises a support frame (1), wherein a treatment barrel (2) is installed at the upper end of the support frame (1), a feed inlet (3) is formed in the left side of the upper end of the treatment barrel (2), a direct current motor (4) is oppositely arranged on the right side of the feed inlet (3), the lower end of the direct current motor (4) is connected with a stirring rod (5), a first liquid injection port (6) and a second liquid injection port (7) are respectively formed in the upper end and the lower end of the right side of the treatment barrel (2), a first water drainage pipe (8) is inserted into the middle end of the interior of the treatment barrel (2), heating plates (9) are respectively arranged on the left side and the right side of the lower end of the interior of the treatment barrel (2), and a second water drainage pipe (10) is inserted into the middle end of the interior of the treatment barrel (2);

the method is characterized in that: still include supplementary filter equipment (11), supplementary filter equipment (11) set up in support frame (1) lower extreme, supplementary filter equipment (11) include rose box (111), filter plate (112), first outlet pipe (113), second outlet pipe (114), adjusting part (115) and wash subassembly (116), rose box (111) and support frame (1) lower extreme fastening connection to rose box (111) inside upper end is provided with filter plate (112), rose box (111) right side is pegged graft mutually respectively and is had first outlet pipe (113) and second outlet pipe (114), adjusting part (115) set up in filter plate (112) middle part lower extreme, wash subassembly (116) and set up in rose box (111) inside upper end.

2. The device for extracting, separating and purifying ursolic acid according to claim 1, characterized in that: the adjusting assembly (115) comprises a shell (1151), a motor (1152), a rotating rack (1153), a connecting rod (1154), a rotating cylinder (1155) and an inserting rod (1156), the left side of the shell (1151) is fixedly connected with the filter box (111), the motor (1152) is installed on the right side of the inside of the shell (1151), the front side of the motor (1152) is connected with the rotating rack (1153), the connecting rod (1154) is installed at the upper end and the lower end of the middle of the rotating rack (1153), the rotating cylinder (1155) and the rotating rack (1153) are oppositely arranged left and right, the rotating cylinder (1155) is inserted into the lower end of the inserting rod (1156), and the upper end of the inserting rod (1156) is fixedly connected with the filter plate (112).

3. The device for extracting, separating and purifying ursolic acid according to claim 1, wherein: washing subassembly (116) is including protecting crust (1161), flushing machine (1162), remove frame (1163), drive plate (1164), gear (1165) and driving motor (1166), protecting crust (1161) upper end and rose box (111) fixed connection to flushing machine (1162) are installed to protecting crust (1161) inside left side, flushing machine (1162) left side is linked together with rose box (111), and flushing machine (1162) right side is connected with removing frame (1163), remove frame (1163) and protecting crust (1161) inside sliding connection to remove frame (1163) inside sliding connection has drive plate (1164), drive plate (1164) front side right-hand member meshing is connected with gear (1165), and gear (1165) front side is connected with driving motor (1166).

4. The device for extracting, separating and purifying ursolic acid according to claim 1, wherein: the lower end in the filter box (111) inclines towards the lower right corner, and the first water outlet pipe (113) and the second water outlet pipe (114) arranged on the right side of the filter box (111) are symmetrical up and down.

5. The device for extracting, separating and purifying ursolic acid according to claim 2, characterized in that: the left side and the right side of the rotating frame (1153) are in a semi-arc shape, and the left side and the right side of the rotating frame (1153) are in sliding insertion connection with the rotating cylinder (1155).

6. The device for extracting, separating and purifying ursolic acid according to claim 2, characterized in that: the outer side of the middle part of the rotating cylinder (1155) is provided with a crossed groove, and the inner wall of the groove formed in the rotating cylinder (1155) is smooth.

7. The device for extracting, separating and purifying ursolic acid according to claim 3, wherein: the spraying position of the lower end of the washing machine (1162) inclines to the right side, and the lower end of the washing machine (1162) is opposite to the other filter plate (112) up and down.

8. The device for extracting, separating and purifying ursolic acid according to claim 3, wherein: the driving plate (1164) is transversely arranged along the hollow part in the movable frame (1163), and a plurality of arc-shaped grooves and round bulges are respectively arranged on the front side of the driving plate (1164).

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