CN216224397U - Reaction kettle for preparing nano material - Google Patents

Reaction kettle for preparing nano material Download PDF

Info

Publication number
CN216224397U
CN216224397U CN202122866800.XU CN202122866800U CN216224397U CN 216224397 U CN216224397 U CN 216224397U CN 202122866800 U CN202122866800 U CN 202122866800U CN 216224397 U CN216224397 U CN 216224397U
Authority
CN
China
Prior art keywords
reaction kettle
kettle body
box
rotating shaft
fixedly connected
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN202122866800.XU
Other languages
Chinese (zh)
Inventor
鲍建峰
李婧
李景华
胡志刚
张丰收
景爱华
李光大
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Henan University of Science and Technology
Original Assignee
Henan University of Science and Technology
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Henan University of Science and Technology filed Critical Henan University of Science and Technology
Priority to CN202122866800.XU priority Critical patent/CN216224397U/en
Application granted granted Critical
Publication of CN216224397U publication Critical patent/CN216224397U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The utility model discloses a reaction kettle for preparing nano materials, which relates to the technical field of reaction kettles and comprises a reaction kettle body, wherein a partition plate is fixedly arranged inside the reaction kettle body, a rack is fixedly arranged on the upper surface of the partition plate, a first rotating shaft is arranged inside the reaction kettle body, a first stirring rod is arranged outside the first rotating shaft, a first bevel gear is fixedly connected to the upper end of the first rotating shaft, and a transmission rod is slidably connected to the upper surface of the reaction kettle body, and the reaction kettle has the beneficial effects that: through the motor that sets up, can control the motor and rotate, under the mutually supporting of eccentric round pin axle and square frame, can drive the linkage case and carry out reciprocating motion from top to bottom, in the linkage case motion process, under the meshing connection effect through connecting gear and rack to can drive first pivot and rotate, and then carry out reciprocating motion from top to bottom when having realized first pivot rotation, improve stirring effect greatly.

Description

Reaction kettle for preparing nano material
Technical Field
The utility model relates to the technical field of reaction kettles, in particular to a reaction kettle for preparing a nano material.
Background
The broad understanding of the reaction kettle is that the reaction kettle is a container for physical or chemical reaction, and the heating, evaporation, cooling and low-speed mixing functions required by the process are realized through the structural design and parameter configuration of the container. The material of the reaction kettle generally comprises carbon manganese steel, stainless steel, zirconium, nickel-based (Hash, Monel) alloy and other composite materials, the nano material means that the size of a structural unit ranges from 1 nanometer to 100 nanometers, and the preparation of the nano material is usually carried out in the reaction kettle.
But the stirring effect of the existing reaction kettle is not good, and reactants in the reaction kettle can not be fully reacted, so that the reaction effect of the nano material is achieved, high-temperature gas generated in the working process of the reaction kettle is not treated, and air pollution is caused by direct emission.
SUMMERY OF THE UTILITY MODEL
Aiming at the defects of the prior art, the utility model provides a reaction kettle for preparing a nano material, which solves the problems that the stirring effect is poor and high-temperature gas generated in the working process of the reaction kettle is not treated in the background technology.
In order to achieve the purpose, the utility model is realized by the following technical scheme: a reaction kettle for preparing nano materials comprises a reaction kettle body, wherein a partition plate is fixedly arranged inside the reaction kettle body, a rack is fixedly arranged on the upper surface of the partition plate, a first rotating shaft is arranged inside the reaction kettle body, a first stirring rod is arranged outside the first rotating shaft, a first bevel gear is fixedly connected to the upper end of the first rotating shaft, a transmission rod is slidably connected to the upper surface of the reaction kettle body, a linkage box is fixedly connected to one end of the transmission rod, the first rotating shaft is rotatably connected with the linkage box, a second rotating shaft is rotatably connected to one side of the linkage box, a second bevel gear is fixedly arranged at one end of the second rotating shaft, the second bevel gear is meshed with the first bevel gear, a connecting gear is fixedly connected to the other end of the second rotating shaft, the connecting gear is meshed with the rack, and a motor is fixedly arranged on the upper surface of the reaction kettle body, the output end of the motor is fixedly connected with a rotary table, and an eccentric pin shaft is fixedly mounted on the outer side of the rotary table.
Through using above-mentioned technical scheme, through the motor that sets up, can control the motor and rotate, under the mutually supporting of eccentric pin axle and square frame, can drive the linkage case and carry out reciprocating motion from top to bottom, in the linkage case motion process, under the meshing connection effect through connecting gear and rack, can control second bevel gear and rotate, thereby can drive first pivot and rotate, and then carried out reciprocating motion from top to bottom when having realized first pivot rotation, the stirring effect has been improved greatly, make the reactant in the reation kettle obtain the abundant reaction, the reaction efficiency is improved.
Preferably, one side of reation kettle body is close to the top position and is provided with the inlet pipe, the inside rotation of reation kettle body is connected with and rotates the seat, the outside fixed mounting who rotates the seat has the connecting rod, the outside fixed mounting of connecting rod has the second puddler, the outside of reation kettle body is close to the below position and is provided with row's material pipe, first pivot run through the baffle and with rotate seat sliding connection.
Through using above-mentioned technical scheme, can drive when first pivot is rotated and rotate the seat and rotate to the connecting rod drives a plurality of second puddlers and rotates, can prevent that nanometer raw materials from taking place to pile up in the bottom of reation kettle body.
Preferably, an air extraction box is fixedly mounted on the upper surface of the partition plate, and an air extraction pipe and an exhaust pipe are respectively arranged on the outer side of the air extraction box.
Through using above-mentioned technical scheme, the gas that the reation kettle body produced compresses to the inside of exhaust chamber through the exhaust tube, then is discharging through the blast pipe.
Preferably, the upper end of the transmission rod is fixedly connected with a square frame, the outer side of the square frame is fixedly connected with an L-shaped rod, and one end of the L-shaped rod is fixedly connected with a piston in an inner cavity of the air extraction box.
Through using above-mentioned technical scheme, when the stirring, the linkage box can drive the piston through L type pole and do the piston motion in the exhaust chamber inside to can discharge the inside of purifying box into through the blast pipe with the high-temperature gas that produces.
Preferably, the outside of reation kettle body is provided with the purifying box, the inside of purifying box is provided with the cooler bin, the blast pipe runs through the cooler bin.
Through using above-mentioned technical scheme, the inside coolant liquid of cooler bin can cool off the blast pipe, and then can cool down the inside high-temperature gas of blast pipe.
Preferably, the inside of purifying box is provided with the filter screen, the gas vent has been seted up in the outside of purifying box.
Through using above-mentioned technical scheme, can filter the gas that the reation kettle body produced, prevent direct discharge contaminated air.
The utility model provides a reaction kettle for preparing a nano material, which has the following beneficial effects:
1. this reation kettle that preparation nano-material was used, motor through setting up, can control the motor and rotate, under the mutually supporting of eccentric round pin axle and square frame, can drive the linkage case and carry out reciprocating motion from top to bottom, in the linkage case motion process, under the meshing connection effect through connecting gear and rack, can control second bevel gear and rotate, thereby can drive first pivot and rotate, and then carried out reciprocating motion from top to bottom when having realized first pivot rotation, the stirring effect has been improved greatly, make the reactant in the reation kettle obtain abundant reaction, the reaction efficiency is improved.
2. This reation kettle that preparation nano-material was used, linkage box through setting up, L type pole, mutually supporting of piston and exhaust box, in the stirring, the linkage box can drive the piston through L type pole and be the piston motion in the inside of exhaust box, thereby can discharge the inside of purifying box through the blast pipe with the high-temperature gas who produces, can cool off high-temperature gas through the cooler bin that sets up, then the filtration through the filter screen, the rethread gas vent is discharged, the problem that the high-temperature gas who produces directly discharges and causes air pollution has been solved.
Drawings
FIG. 1 is a schematic structural view of the present invention;
FIG. 2 is a top view of the present invention;
FIG. 3 is an enlarged view taken at A of FIG. 1 in accordance with the present invention;
fig. 4 is an enlarged view of the utility model at B in fig. 1.
In the figure: 1. a reaction kettle body; 101. a feed pipe; 102. a rotating seat; 103. a connecting rod; 104. a second stirring rod; 105. a discharge pipe; 2. a partition plate; 201. a rack; 202. an air extraction box; 203. an air exhaust pipe; 204. an exhaust pipe; 3. a first rotating shaft; 301. a first stirring rod; 302. a first bevel gear; 4. a transmission rod; 401. a linkage box; 402. a second rotating shaft; 403. a second bevel gear; 404. a connecting gear; 405. a square frame; 406. an L-shaped rod; 407. a piston; 5. a motor; 501. a turntable; 502. an eccentric pin shaft; 6. a purification box; 601. a cooling tank; 602. a filter screen; 603. and (7) an exhaust port.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments.
Referring to fig. 1 to 4, the present invention provides a technical solution: the utility model provides a reation kettle that preparation nano-material was used, including reation kettle body 1, one side of reation kettle body 1 is close to the top position and is provided with inlet pipe 101, reation kettle body 1's inside rotation is connected with and rotates seat 102, the outside fixed mounting who rotates seat 102 has connecting rod 103, the outside fixed mounting of connecting rod 103 has second puddler 104, first pivot 3 pivoted can drive and rotate seat 102 and rotate simultaneously, thereby connecting rod 103 drives a plurality of second puddlers 104 and rotates, can prevent that nanometer raw materials from taking place to pile up in reation kettle body 1's bottom, reation kettle body 1's the outside is close to the below position and is provided with row material pipe 105, first pivot 3 run through baffle 2 and with rotation seat 102 sliding connection.
A partition plate 2 is fixedly arranged inside a reaction kettle body 1, a rack 201 is fixedly arranged on the upper surface of the partition plate 2, a first rotating shaft 3 is arranged inside the reaction kettle body 1, a first stirring rod 301 is arranged outside the first rotating shaft 3, a first bevel gear 302 is fixedly connected to the upper end of the first rotating shaft 3, a transmission rod 4 is slidably connected to the upper surface of the reaction kettle body 1, a linkage box 401 is fixedly connected to one end of the transmission rod 4, the first rotating shaft 3 is rotatably connected with the linkage box 401, a second rotating shaft 402 is rotatably connected to one side of the linkage box 401, a second bevel gear 403 is fixedly arranged at one end of the second rotating shaft 402, the second bevel gear 403 is meshed with the first bevel gear 302, a connecting gear 404 is fixedly connected to the other end of the second rotating shaft 402, the connecting gear 404 is meshed with the rack 201, a motor 5 is fixedly arranged on the upper surface of the reaction kettle body 1, and a turntable 501 is fixedly connected to the output end of the motor 5, carousel 501's outside fixed mounting has eccentric pin axle 502, motor 5 through setting up, can control motor 5 and rotate, under the mutually supporting of eccentric pin axle 502 and square frame 405, can drive linkage case 401 and carry out up-and-down reciprocating motion, in the linkage case 401 motion process, under the meshing connection effect through connecting gear 404 and rack 201, can control second bevel gear 403 and rotate, thereby can drive first pivot 3 and rotate, and then carried out up-and-down reciprocating motion when having realized first pivot 3 pivoted, the stirring effect has been improved greatly, make the reactant in the reation kettle obtain the abundant reaction, and the reaction efficiency is improved.
An air suction box 202 is fixedly arranged on the upper surface of the partition plate 2, an air suction pipe 203 and an exhaust pipe 204 are respectively arranged on the outer side of the air suction box 202, a square frame 405 is fixedly connected to the upper end of a transmission rod 4, an L-shaped rod 406 is fixedly connected to the outer side of the square frame 405, a piston 407 is fixedly connected to one end of the L-shaped rod 406 and is positioned in the inner cavity of the air suction box 202, the piston 407 can be controlled to do piston movement in the air suction box 202, so that gas generated by the reaction kettle body 1 is compressed into the air suction box 202 through the air suction pipe 203 and then is exhausted through the exhaust pipe 204, a purification box 6 is arranged on the outer side of the reaction kettle body 1, a cooling box 601 is arranged in the purification box 6, a water injection pipe and a water drainage pipe are respectively arranged on the outer side of the cooling box 601, so that cooling liquid in the cooling box 601 can be replaced, the exhaust pipe 204 penetrates through the cooling box 601, a filter screen 602 is arranged in the purification box 6, the gas vent 603 has been seted up in the outside of purifying box 6, through the linkage case 401 that sets up, L type pole 406, mutually supporting of piston 407 and exhaust box 202, when stirring, linkage case 401 can drive piston 407 through L type pole 406 and do the piston motion in the inside of exhaust box 202, thereby can discharge the high-temperature gas that produces into the inside of purifying box 6 through blast pipe 204, can cool off high-temperature gas through the cooler bin 601 that sets up, then through the filtration of filter screen 602, the rethread gas vent 603 is discharged, the problem of air pollution is caused in the direct emission of high-temperature gas that has solved the production.
In conclusion, when the reaction kettle for preparing the nano material is used, firstly, the nano material is discharged into a cavity of the reaction kettle body 1 through the feeding pipe 101, then the motor 5 is started, the motor 5 is controlled to rotate, the linkage box 401 can be driven to reciprocate up and down under the mutual matching of the eccentric pin shaft 502 and the square frame 405, the second bevel gear 403 can be controlled to rotate under the meshing connection action of the connecting gear 404 and the rack 201 in the motion process of the linkage box 401, so that the first rotating shaft 3 can be driven to rotate, the first rotating shaft 3 can further rotate and reciprocate up and down, the linkage box 401 can drive the piston 407 to do piston motion in the extraction box 202 through the L-shaped rod 406 while moving, so that the generated high-temperature gas can be discharged into the purification box 6 through the exhaust pipe 204, and the cooling box 601 can cool the high-temperature gas, then filtered by the filter screen 602 and discharged through the exhaust port 603.
The above description is only for the preferred embodiment of the present invention, but the scope of the present invention is not limited thereto, and any person skilled in the art should be considered to be within the technical scope of the present invention, and equivalent alternatives or modifications according to the technical solution of the present invention and the inventive concept thereof should be covered by the scope of the present invention.

Claims (6)

1. A reation kettle that preparation nano-material used, includes reation kettle body (1), its characterized in that: the reaction kettle comprises a reaction kettle body (1), a partition plate (2) is fixedly arranged in the reaction kettle body (1), a rack (201) is fixedly arranged on the upper surface of the partition plate (2), a first rotating shaft (3) is arranged in the reaction kettle body (1), a first stirring rod (301) is arranged on the outer side of the first rotating shaft (3), a first bevel gear (302) is fixedly connected to the upper end of the first rotating shaft (3), a transmission rod (4) is slidably connected to the upper surface of the reaction kettle body (1), a linkage box (401) is fixedly connected to one end of the transmission rod (4), the first rotating shaft (3) is rotatably connected with the linkage box (401), a second rotating shaft (402) is rotatably connected to one side of the linkage box (401), a second bevel gear (403) is fixedly arranged at one end of the second rotating shaft (402), and the second bevel gear (403) is meshed with the first bevel gear (302), the other end fixedly connected with connecting gear (404) of second pivot (402), connecting gear (404) is connected with rack (201) meshing, the last fixed surface of reation kettle body (1) installs motor (5), the output fixedly connected with carousel (501) of motor (5), the outside fixed mounting of carousel (501) has eccentric round pin axle (502).
2. The reaction kettle for preparing nano-materials according to claim 1, characterized in that: one side of reation kettle body (1) is close to the top position and is provided with inlet pipe (101), the inside rotation of reation kettle body (1) is connected with rotates seat (102), the outside fixed mounting who rotates seat (102) has connecting rod (103), the outside fixed mounting of connecting rod (103) has second puddler (104), the outside of reation kettle body (1) is close to below position and is provided with row material pipe (105), first pivot (3) run through baffle (2) and with rotate seat (102) sliding connection.
3. The reaction kettle for preparing nano-materials according to claim 1, characterized in that: an air extraction box (202) is fixedly mounted on the upper surface of the partition plate (2), and an air extraction pipe (203) and an exhaust pipe (204) are respectively arranged on the outer side of the air extraction box (202).
4. The reaction kettle for preparing nano-materials according to claim 1, characterized in that: the upper end of the transmission rod (4) is fixedly connected with a square frame (405), the outer side of the square frame (405) is fixedly connected with an L-shaped rod (406), and one end of the L-shaped rod (406) is fixedly connected with a piston (407) which is located in an inner cavity of the air extraction box (202).
5. The reaction kettle for preparing nano-materials according to claim 3, characterized in that: the outer side of the reaction kettle body (1) is provided with a purification box (6), the inside of the purification box (6) is provided with a cooling box (601), and the exhaust pipe (204) penetrates through the cooling box (601).
6. The reaction kettle for preparing nano-materials according to claim 5, wherein: a filter screen (602) is arranged in the purification box (6), and an exhaust port (603) is formed in the outer side of the purification box (6).
CN202122866800.XU 2021-11-22 2021-11-22 Reaction kettle for preparing nano material Expired - Fee Related CN216224397U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202122866800.XU CN216224397U (en) 2021-11-22 2021-11-22 Reaction kettle for preparing nano material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202122866800.XU CN216224397U (en) 2021-11-22 2021-11-22 Reaction kettle for preparing nano material

Publications (1)

Publication Number Publication Date
CN216224397U true CN216224397U (en) 2022-04-08

Family

ID=80955611

Family Applications (1)

Application Number Title Priority Date Filing Date
CN202122866800.XU Expired - Fee Related CN216224397U (en) 2021-11-22 2021-11-22 Reaction kettle for preparing nano material

Country Status (1)

Country Link
CN (1) CN216224397U (en)

Similar Documents

Publication Publication Date Title
CN216224397U (en) Reaction kettle for preparing nano material
CN218944618U (en) Chemical waste gas treatment device
CN113355829B (en) Dip dyeing device for core spun yarn production
CN113069816B (en) Circulating cylinder type filter press for preparing hydrated silicon dioxide
CN216456977U (en) Vacuum distillation device for production of organophosphorus ligand
CN215136905U (en) Separation and purification device for bulk drug synthesis
CN215288203U (en) Waste water recovery device used in green building construction
CN212712817U (en) Ethanol extraction waste liquid ethanol recovery unit
CN216898191U (en) Drying device is used in fertilizer production
CN218422794U (en) Causticization reaction tank capable of automatically exhausting
CN112619200A (en) Natural products polysaccharide draws concentrated all-in-one
CN216303321U (en) Industrial wastewater stirring and filtering device
CN214159270U (en) Sodium bicarbonate aqueous solution liquid preparation device
CN216260804U (en) Uniform clutch reaction tank for producing polyaluminium chloride
CN217313427U (en) 6-chloro-2-methyl-2H-indazole-5-amine condensation reaction dehydration device
CN218307965U (en) Automatic production equipment for polyferric chloride
CN217856108U (en) Convenient high-efficient preparation mixes device of iron nickel sulfide
CN220425278U (en) High-temperature high-pressure preparation device for titanium diboride
CN108117414A (en) A kind of high energy-saving organic fertilizer production equipment of production efficiency
CN218248587U (en) High vacuum concentration device of chiral ligand medicine
CN217490555U (en) Mixing device for scandium oxide production
CN117757593A (en) Stirring type vertical fermentation tank
CN220153141U (en) Powder metallurgy drying device
CN218357386U (en) A liquid medicine concentrator for animal remedy processing
CN212915622U (en) A novel reation kettle for detergent production

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20220408