CN215084925U - Cyclopentadienyl rare earth compound purification device - Google Patents
Cyclopentadienyl rare earth compound purification device Download PDFInfo
- Publication number
- CN215084925U CN215084925U CN202121576527.0U CN202121576527U CN215084925U CN 215084925 U CN215084925 U CN 215084925U CN 202121576527 U CN202121576527 U CN 202121576527U CN 215084925 U CN215084925 U CN 215084925U
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- Prior art keywords
- fixedly connected
- rare earth
- earth compound
- barrel
- furnace body
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- 229910052761 rare earth metal Inorganic materials 0.000 title claims abstract description 47
- -1 Cyclopentadienyl rare earth Chemical class 0.000 title claims abstract description 42
- ZSWFCLXCOIISFI-UHFFFAOYSA-N endo-cyclopentadiene Natural products C1C=CC=C1 ZSWFCLXCOIISFI-UHFFFAOYSA-N 0.000 title claims abstract description 38
- 238000003883 substance clean up Methods 0.000 title claims abstract description 19
- 239000000463 material Substances 0.000 claims abstract description 21
- 238000009434 installation Methods 0.000 claims abstract description 17
- 230000006698 induction Effects 0.000 claims abstract description 14
- 238000000926 separation method Methods 0.000 claims description 26
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 25
- 238000005406 washing Methods 0.000 claims description 22
- 239000007921 spray Substances 0.000 claims description 11
- 238000011010 flushing procedure Methods 0.000 claims description 5
- 150000002910 rare earth metals Chemical class 0.000 description 5
- 238000003756 stirring Methods 0.000 description 5
- 238000007599 discharging Methods 0.000 description 4
- 239000012535 impurity Substances 0.000 description 4
- 238000003723 Smelting Methods 0.000 description 3
- 238000000746 purification Methods 0.000 description 3
- 230000007547 defect Effects 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 238000000034 method Methods 0.000 description 2
- 238000005192 partition Methods 0.000 description 2
- 238000011403 purification operation Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 239000010865 sewage Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 230000007306 turnover Effects 0.000 description 2
- 229910000831 Steel Inorganic materials 0.000 description 1
- 229910052729 chemical element Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229910052747 lanthanoid Inorganic materials 0.000 description 1
- 150000002602 lanthanoids Chemical class 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 229910052706 scandium Inorganic materials 0.000 description 1
- SIXSYDAISGFNSX-UHFFFAOYSA-N scandium atom Chemical compound [Sc] SIXSYDAISGFNSX-UHFFFAOYSA-N 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
- 229910052727 yttrium Inorganic materials 0.000 description 1
- VWQVUPCCIRVNHF-UHFFFAOYSA-N yttrium atom Chemical compound [Y] VWQVUPCCIRVNHF-UHFFFAOYSA-N 0.000 description 1
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a cyclopentadienyl rare earth compound purification device, comprising a base plate, fixed surface is connected with the installation pole on the bottom plate, installation pole top fixedly connected with furnace body, and fixed mounting has the branch bank in the furnace body, and branch bank central point puts the department and rotates and be connected with the back shaft, and back shaft outer wall fixed mounting has the feeder hopper, and the feeder hopper has three angle bars including the rotatory feed opening down of a plurality of slopes, and it has a plurality of discharge gates to separate to open on the bank, and installation pole one side fixedly connected with induction heater, and induction heater is located the bottom of furnace body. The utility model discloses a set up the rotatory feed opening down of a plurality of slopes on the feeder hopper that rotates the installation for when adding the material toward the feeder hopper, the material can disperse, thereby produces the component, drives the feeder hopper and begins to rotate, makes the material unloading even in the furnace body.
Description
Technical Field
The utility model relates to a cyclopentadienyl rare earth compound technical field especially relates to cyclopentadienyl rare earth compound purification device.
Background
Rare earth is a total name of 17 chemical elements including scandium, yttrium and lanthanide elements in the third subgroup of the periodic table of elements, generally exists in the form of oxides, belongs to non-renewable resources, is not rare in nature, but becomes a useful material, has complex and tedious procedures and high cost, and is named as 'rare earth', the 17 elements can be generally divided into light rare earth and heavy rare earth, wherein the heavy rare earth is more valuable, and the rare earth compound also needs to be highly purified to be applied to human life production.
At present, most of the existing cyclopentadienyl rare earth compound purification devices have the following defects: when a compound raw material needs to be smelted, the raw material is not completely smelted due to the uneven distribution in the furnace body, so that the purity of the cyclopentadienyl rare earth compound is not enough to meet the use requirement, and in conclusion, most of the existing cyclopentadienyl rare earth compound purifying devices cannot well meet the actual requirement.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects existing in the prior art and providing a cyclopentadienyl rare earth compound purifying device.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
the cyclopentadienyl rare earth compound purification device comprises a bottom plate, wherein an installation rod is fixedly connected to the upper surface of the bottom plate, a furnace body is fixedly connected to the top of the installation rod, a separation disc is fixedly installed in the furnace body, a support shaft is rotatably connected to the central position of the separation disc, a feed hopper is fixedly installed on the outer wall of the support shaft, the feed hopper comprises a plurality of discharge openings which obliquely rotate downwards, triangular bars are fixedly installed on the outer wall of the bottom of the feed hopper, a plurality of discharge openings are formed in the separation disc, an induction heater is fixedly connected to one side of the installation rod, the induction heater is positioned at the bottom of the furnace body, one side of the mounting rod is fixedly connected with a separation barrel and a washing barrel, the material guide pipe is fixedly connected between the furnace body and the separation barrel, the shell is fixedly connected to the upper surface of the bottom plate, a distiller is arranged in an inner cavity of the shell, and the distiller is located below the washing barrel and is communicated with the washing barrel through a pipeline.
Furthermore, the separating barrel is located above the washing barrel, the separating barrel is communicated with the washing barrel through a pipeline, a filter screen is fixedly connected to the inner wall of the circumference of the separating barrel, and the washing barrel is located below the filter screen.
Furthermore, the upper surface of the bottom plate is fixedly connected with a water tank, the upper surface of the water tank is fixedly connected with a water pump, a water outlet of the water pump is movably connected with a flow guide pipe, one end of the flow guide pipe is fixedly connected with a spray head, and the spray head is positioned inside the washing barrel.
Furthermore, a vacuum air pump is fixedly connected to one side of the bottom plate, one end of the output end of the vacuum air pump is movably connected with an air pipe, one end of the air pipe is movably connected with the distiller, and a discharge pipe is fixedly connected to one side of the distiller.
Furthermore, one end of the material guide pipe is provided with a heat insulation ring.
Furthermore, a plurality of handles are arranged on the furnace body, and a rotary drum is connected to the supporting shaft in a threaded manner.
Furthermore, one side of the washing barrel is fixedly connected with a drain pipe.
The utility model has the advantages that:
1. through set up the feed opening of a plurality of inclined rotation down on the feeder hopper of rotation installation for when adding the material toward the feeder hopper in, the material can disperse, thereby produces the component, drives the feeder hopper and begins the rotation, makes the material unloading even in the furnace body.
2. Through three angle bars on the feeder hopper and the setting of partition plate upper discharge gate, can drive three angle bars when the feeder hopper rotates and rotate, and then make three angle bars can scrape the material on the partition plate discharge gate department and fall down to accomplish the unloading, make the unloading process separate controllable, avoided the accumulational phenomenon of material.
3. Through the cooperation setting of induction heater, filter screen, shower nozzle, vacuum aspiration pump and distiller, carry out multiple physical operation and chemical operation such as high temperature melting, physics filter, erode cleanness and chemical distillation to rare earth compound, promoted integrated device's purification precision and purification efficiency to device overall structure is simple, the easy operation, the purification precision is high, and inside spare part easily dismantles, is of value to the maintenance operation in later stage.
Drawings
FIG. 1 is a schematic perspective view of a cyclopentadienyl rare earth compound purification device according to the present invention;
FIG. 2 is a schematic view of a partial cross-sectional structure of a cyclopentadienyl rare earth compound purification device according to the present invention;
FIG. 3 is a schematic view of a partial three-dimensional structure of a cyclopentadienyl rare earth compound purification device provided by the present invention;
FIG. 4 is a schematic view of a partial three-dimensional structure of a cyclopentadienyl rare earth compound purification device provided by the present invention;
fig. 5 is a schematic view of a partial cross-sectional structure of a cyclopentadienyl rare earth compound purification device provided by the present invention.
FIG. 1, bottom plate; 101. a divider disk; 102. a discharge port; 103. a support shaft; 104. a rotating drum; 105. a feed hopper; 106. triangular bars; 107. a handle; 2. mounting a rod; 3. a furnace body; 4. a steel pipe; 5. a heat insulating ring; 6. an induction heater; 7. a separation barrel; 8. filtering with a screen; 9. washing the barrel; 10. a water tank; 11. a water pump; 12. a spray head; 13. a housing; 15. a distiller; 16. a discharge pipe; 17. a vacuum pump; 18. a gas delivery pipe.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-5, a cyclopentadienyl rare earth compound purification device comprises a bottom plate 1, wherein an installation rod 2 is fixedly connected to the upper surface of the bottom plate 1, a furnace body 3 is fixedly connected to the top of the installation rod 2, a separation disc 101 is fixedly installed in the furnace body 3, a support shaft 103 is rotatably connected to the central position of the separation disc 101, a feed hopper 105 is fixedly installed on the outer wall of the support shaft 103, the feed hopper 105 comprises a plurality of obliquely-rotating downward-facing feed openings, a triangular strip 106 is fixedly installed on the outer wall of the bottom of the feed hopper 105, a plurality of discharge openings 102 are formed in the separation disc 101, the triangular strip 106 is in contact with the upper surface of the separation disc 101, the plurality of obliquely-rotating downward-facing feed openings are arranged on the rotatably-installed feed hopper 105, so that when materials are added into the feed hopper 105, the materials can be dispersed, thereby generating component force to drive the feed hopper 105 to start rotating, so that the materials are uniformly fed into the furnace body, a plurality of handles 107 are arranged on the furnace body 3, the feed hopper 105 may also be manually rotated by a handle 107;
the induction heating device comprises an installation rod 2, an induction heater 6 is fixedly connected to one side of the installation rod 2, the induction heater 6 is JX-35KW in model number, the induction heater 6 is located at the bottom of a furnace body 3, a device for heating rare earth compounds is convenient to install, the rare earth compounds are melted at high temperature, a separation barrel 7 and a flushing barrel 9 are fixedly connected to one side of the installation rod 2, a material guide pipe 4 is fixedly connected between the furnace body 3 and the separation barrel 7, a shell 13 is fixedly connected to the upper surface of a bottom plate 1, a distiller 15 is arranged at an inner cavity of the shell 13, and the distiller 15 is located below the flushing barrel 9 and communicated with the flushing barrel through a pipeline.
Wherein, separation bucket 7 is located the top of washing bucket 9, through the pipeline intercommunication between separation bucket 7 and the washing bucket 9, and separation bucket 7 circumference inner wall fixedly connected with filter screen 8, and washing bucket 9 is located the below of filter screen 8, and filter screen 8 carries out preliminary treatment to cyclopentadienyl rare earth compound, filters the impurity in the cyclopentadienyl rare earth compound on filter screen 8 surface.
Wherein, one side of the furnace body 3, the separation barrel 7, the washing barrel 9 and the distiller 15 is provided with a rotating plate, one side of the rotating plate is fixedly connected with a rotating shaft, one end of the rotating shaft is fixedly connected with a toggle block, the upper surface of the bottom plate 1 is fixedly connected with a water tank 10, the upper surface of the water tank 10 is fixedly connected with a water pump 11, the water outlet of the water pump 11 is movably connected with a flow guide pipe, one end of the flow guide pipe is fixedly connected with a spray head 12, the spray head 12 is positioned in the washing barrel 9, one side of the washing barrel 9 is fixedly connected with a drain pipe, the water pump 11 pumps water from the water tank 10 and sprays on the surface of the cyclopentadienyl rare earth compound through the spray head 12 to wash the impurities on the surface of the cyclopentadienyl rare earth compound, finally, the sewage is discharged through the drain pipe, one side of the bottom plate 1 is fixedly connected with a vacuum air pump 17, the model of the vacuum air pump 17 is WLW-300, one end of the output end of the vacuum air pump 17 is movably connected with an air pipe 18, and gas-supply pipe 18 one end and distiller 15 form swing joint, and distiller 15 one side fixedly connected with discharging pipe 16, start vacuum air pump 17, vacuum air pump 17 exhausts the inside air of distiller 15 totally, builds vacuum environment, and the welding of distiller 15 one side has discharging pipe 16, and cyclopentadienyl rare earth compound passes through discharging pipe 16 and discharges distiller 15, accomplishes the purification operation.
Wherein, one end of the material guiding pipe 4 is provided with a heat insulation ring 5, and a rotating cylinder 104 is connected with the supporting shaft 103 through screw threads.
The working principle is as follows: when the device is used, an operator slowly pours the cyclopentadienyl rare earth compound into the interior of the smelting furnace 3 through the feeding hole, the material is dispersed in the feeding hopper 105 to drive the feeding hopper 105 to rotate, so that the material is uniformly fed in the furnace body, the induction heater 6 is started, the induction heater 6 heats the smelting furnace 3 to melt the cyclopentadienyl rare earth compound at high temperature, the stirring block at the bottom of the smelting furnace 3 is stirred to turn over the rotating plate, so that the channel of the material guide pipe 4 is exposed, the high-temperature molten cyclopentadienyl rare earth compound enters the interior of the separation barrel 7 through the material guide pipe 4, impurities in the cyclopentadienyl rare earth compound are filtered on the surface of the filter screen 8, the operator stirs the stirring block at the bottom of the separation barrel 7 to turn over the rotating plate, the cyclopentadienyl rare earth compound flows into the interior of the washing barrel 9, at the moment, the water pump 11 is started, the water pump 11 pumps water from the water tank 10 and sprays the water on the surface of the cyclopentadienyl rare earth compound through the spray nozzle 12, erode the impurity on cyclopentadienyl rare earth compound surface, last sewage is discharged through the drain pipe, the operation personnel stir the stirring piece of washtub 9 bottoms and overturn the rotor plate, cyclopentadienyl rare earth compound falls into the inside of distiller 15, start vacuum air pump 17, vacuum air pump 17 discharges the inside air of distiller 15 completely, build vacuum environment, distiller 15 carries out last step distillation operation to cyclopentadienyl rare earth compound, cyclopentadienyl rare earth compound passes through discharging pipe 16 discharge distiller 15 at last, accomplish the purification operation.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
In the description of this patent, it is to be understood that the terms "center," "upper," "lower," "front," "rear," "left," "right," "vertical," "horizontal," "top," "bottom," "inner," "outer," and the like are used in the orientations and positional relationships indicated in the drawings for the convenience of describing the patent and for the simplicity of description, and are not intended to indicate or imply that the referenced devices or elements must have a particular orientation, be constructed and operated in a particular orientation, and are not to be considered limiting of the patent.
Claims (7)
1. Cyclopentadienyl rare earth compound purification device, comprising a bottom plate (1) and is characterized in that the upper surface of the bottom plate (1) is fixedly connected with an installation rod (2), the top of the installation rod (2) is fixedly connected with a furnace body (3), a separation disc (101) is fixedly installed in the furnace body (3), the central position of the separation disc (101) is rotatably connected with a support shaft (103), the outer wall of the support shaft (103) is fixedly installed with a feed hopper (105), the feed hopper (105) comprises a plurality of inclined rotating downward feed openings, the outer wall of the bottom of the feed hopper (105) is fixedly installed with a triangular bar (106), the separation disc (101) is provided with a plurality of discharge openings (102), one side of the installation rod (2) is fixedly connected with an induction heater (6), the induction heater (6) is positioned at the bottom of the furnace body (3), one side of the installation rod (2) is fixedly connected with a separation barrel (7) and a washing barrel (9), the material guide pipe (4) is fixedly connected between the furnace body (3) and the separation barrel (7), the shell (13) is fixedly connected to the upper surface of the bottom plate (1), a distiller (15) is arranged in an inner cavity of the shell (13), and the distiller (15) is located below the flushing barrel (9) and is communicated with the flushing barrel through a pipeline.
2. The cyclopentadienyl rare earth compound purification device according to claim 1, wherein the separation barrel (7) is located above the washing barrel (9), the separation barrel (7) is communicated with the washing barrel (9) through a pipeline, a filter screen (8) is fixedly connected to the inner circumferential wall of the separation barrel (7), and the washing barrel (9) is located below the filter screen (8).
3. The cyclopentadienyl rare earth compound purification device according to claim 1, wherein a water tank (10) is fixedly connected to the upper surface of the bottom plate (1), a water pump (11) is fixedly connected to the upper surface of the water tank (10), a flow guide pipe is movably connected to a water outlet of the water pump (11), a spray head (12) is fixedly connected to one end of the flow guide pipe, and the spray head (12) is located inside the washing barrel (9).
4. The cyclopentadienyl rare earth compound purification device according to claim 3, wherein a vacuum air pump (17) is fixedly connected to one side of the bottom plate (1), one end of the output end of the vacuum air pump (17) is movably connected with an air pipe (18), one end of the air pipe (18) is movably connected with the distiller (15), and a discharge pipe (16) is fixedly connected to one side of the distiller (15).
5. Cyclopentadienyl rare earth compound purification device according to claim 1, characterized in that one end of said guide tube (4) is provided with an insulating ring (5).
6. Cyclopentadienyl rare earth compound purification device according to claim 1, characterized in that said furnace body (3) is provided with a plurality of handles (107), on the supporting shaft (103) there is a revolving drum (104) in threaded connection.
7. Cyclopentadienyl rare earth compound purification device according to claim 3, characterized in that a drain pipe is fixedly connected to one side of the washing tub (9).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121576527.0U CN215084925U (en) | 2021-07-12 | 2021-07-12 | Cyclopentadienyl rare earth compound purification device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202121576527.0U CN215084925U (en) | 2021-07-12 | 2021-07-12 | Cyclopentadienyl rare earth compound purification device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN215084925U true CN215084925U (en) | 2021-12-10 |
Family
ID=79320289
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202121576527.0U Expired - Fee Related CN215084925U (en) | 2021-07-12 | 2021-07-12 | Cyclopentadienyl rare earth compound purification device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN215084925U (en) |
-
2021
- 2021-07-12 CN CN202121576527.0U patent/CN215084925U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20211210 |