CN210813986U - High-efficient molecular distillation device - Google Patents
High-efficient molecular distillation device Download PDFInfo
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- CN210813986U CN210813986U CN201921632632.4U CN201921632632U CN210813986U CN 210813986 U CN210813986 U CN 210813986U CN 201921632632 U CN201921632632 U CN 201921632632U CN 210813986 U CN210813986 U CN 210813986U
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- molecular distillation
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Abstract
The utility model discloses a high-efficient molecular distillation device, which comprises a tank body, the internal inner chamber that is equipped with of jar, be equipped with the guiding gutter on the lateral wall of inner chamber, be equipped with the export of light component on the lateral wall of inner chamber, and the guiding gutter is connected with the export of light component, the upper end of the jar body is equipped with condensation mechanism, the lower extreme of the jar body is equipped with heat conduction mechanism, be equipped with the export of heavy component on the diapire of inner chamber, fixedly connected with fixed plate on the jar body, fixedly connected with connecting rod on the jar body, the other end fixed connection of connecting rod is at the lower surface of fixed plate, fixedly connected with vacuum pump on the fixed plate, the output of vacuum pump runs through the jar body. The utility model can scrape the feed liquid into a thin liquid film, so that the distillation is more sufficient, and the utilization rate of the raw material is improved; when the temperature of the control device is constant, the device can be operated continuously, has higher extraction efficiency and is suitable for industrial production.
Description
Technical Field
The utility model relates to a pharmacy technical field especially relates to a high-efficient molecular distillation device.
Background
Cholesterol is a multifunctional cosmetic auxiliary agent with biological activity, is a natural steroid resource of steroid medicines, and is widely applied to the aspects of cosmetics, emulsifiers, medicines, electronic liquid crystals and the like. Therefore, the process of extracting cholesterol is receiving much attention from researchers. Lanolin is a lipid rich in cholesterol, and the cholesterol can be extracted by solvent extraction of lanolin, but the room method has high difficulty in industrial operation and high production cost, and is not suitable for industrial production. The complexation method is a development trend of research on extracting cholesterol from lanolin in the technical field of pharmacy, and the method needs molecular distillation on raw materials, collects fraction rich in cholesterol, and further processes the fraction into a finished product, wherein a molecular distillation device is involved in the process.
The existing molecular distillation device mostly adopts gravity to change materials on an evaporation surface into a liquid film to fall, then the liquid film is heated, the evaporated materials can be condensed on a condensation surface in the opposite direction, the liquid film formed by the device is thick, the distillation is insufficient, and the efficiency is low.
SUMMERY OF THE UTILITY MODEL
The utility model aims at solving the defects existing in the prior art and providing a high-efficiency molecular distillation device.
In order to achieve the above purpose, the utility model adopts the following technical scheme:
the utility model provides a high-efficient molecular distillation device, which comprises a tank body, the internal inner chamber that is equipped with of jar, be equipped with the guiding gutter on the lateral wall of inner chamber, be equipped with the export of light component on the lateral wall of inner chamber, and the guiding gutter is connected with the export of light component, the upper end of the jar body is equipped with condensation mechanism, the lower extreme of the jar body is equipped with heat conduction mechanism, be equipped with the export of heavy component on the diapire of inner chamber, fixedly connected with fixed plate on the jar body, fixedly connected with connecting rod on the jar body, the other end fixed connection of connecting rod is at the lower surface of fixed plate, fixedly connected with vacuum pump on the fixed plate, the output of vacuum pump.
Preferably, the condensing mechanism comprises a condensing layer arranged at the upper end of the tank body, and a condensed water inlet and a condensed water outlet are arranged on the condensing layer.
Preferably, the heat conducting mechanism comprises a heat conducting layer arranged at the lower end of the tank body, and a heat conducting oil inlet and a heat conducting oil outlet are formed in the heat conducting layer.
Preferably, rabbling mechanism includes the motor of fixed connection on the fixed plate, the output of motor runs through fixed plate and jar body internal extension and fixedly connected with stirring leaf, stirring leaf and jar body rotate to be connected.
Preferably, the side edges of the stirring blades cling to the side walls of the inner cavity.
Preferably, a heat insulation material is filled between the heat conduction layer and the condensation layer in the tank body.
The utility model has the advantages that:
through the stirring leaf that hugs closely jar body lateral wall, can scrape into thin one deck liquid film with the feed liquid, and the blade slope of stirring leaf sets up, can produce oblique ascending power to the feed liquid during the stirring, slows down the speed that the liquid film slided down, and the feed liquid can be fully with jar body contact, has prolonged the feed liquid and has stopped the internal time in jar, makes the distillation of feed liquid more abundant, has improved the utilization ratio of raw materials.
Through setting up condensation mechanism, guiding gutter, light component export cooperation use, meet cold liquefaction when steam constantly rises and contact the inner chamber roof to along jar body downflow to the guiding gutter in, converge light component export outflow again and collect, can collect different fractions through control temperature, control when the uniform temperature, the device can constantly distill and draw, has higher extraction efficiency, and this device simple structure, and convenient the manufacturing is applicable to industrial production.
Drawings
FIG. 1 is a schematic structural diagram of a high efficiency molecular distillation apparatus provided by the present invention;
fig. 2 is a side view of the stirring vane.
In the figure: 1 tank body, 2 diversion trenches, 3 light component outlets, 4 inner cavities, 5 heat conduction layers, 6 heat conduction oil inlets, 7 heavy component outlets, 8 stirring blades, 9 heat conduction oil outlets, 10 condensed water inlets, 11 feed inlets, 12 condensation layers, 13 condensed water outlets, 14 fixing plates, 15 motors, 16 vacuum pumps and 17 connecting rods.
Detailed Description
The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments.
Referring to fig. 1-2, a high-efficiency molecular distillation apparatus comprises a tank body 1, an inner chamber 4 is arranged in the tank body 1, a diversion trench 2 is arranged on the side wall of the inner chamber 4, a light component outlet 3 is arranged on the side wall of the inner chamber 4, the diversion trench 2 is connected with the light component outlet 3, a condensing mechanism is arranged at the upper end of the tank body 1, a heat conducting mechanism is arranged at the lower end of the tank body 1, a heavy component outlet 7 is arranged on the bottom wall of the inner chamber 4, a fixing plate 14 is fixedly connected to the tank body 1, a connecting rod 17 is fixedly connected to the tank body 1, the other end of the connecting rod 17 is fixedly connected to the lower surface of the fixing plate 14, a vacuum pump 16 is fixedly connected to the fixing plate 14, the output end of the vacuum pump 16 penetrates through the tank body 1 and extends into the inner chamber 4, a stirring mechanism is arranged on the fixing plate, the vacuum pump 16 is responsible for evacuating the interior of the tank 1 to a vacuum environment.
In the utility model, the condensing mechanism comprises a condensing layer 12 arranged at the upper end of a tank body 1, the condensing layer 12 is provided with a condensed water inlet 10 and a condensed water outlet 13, the heat conducting mechanism comprises a heat conducting layer 5 arranged at the lower end of the tank body 1, the heat conducting layer 5 is provided with a heat conducting oil inlet 6 and a heat conducting oil outlet 9, a heat insulating material is filled between the heat conducting layer 5 and the condensing layer 12 in the tank body 1, no direct heat transfer exists between the two structures, the energy loss caused by heat exchange is avoided, the stirring mechanism comprises a motor 15 fixedly connected on a fixed plate 14, the output end of the motor 15 penetrates through the fixed plate 14 and the tank body 1 to extend inwards and is fixedly connected with a stirring blade 8, the stirring blade 8 is rotatably connected with the tank body 1, the side edge of the stirring blade 8 is tightly attached to the side wall of an inner cavity 4, the feed liquid can be scraped into, the speed of the liquid film sliding is slowed down, the feed liquid can be fully contacted with the side wall of the inner cavity 4, the time of the feed liquid staying in the tank body 1 is prolonged, the distillation of the feed liquid is more sufficient, and the utilization rate of raw materials is improved.
When the utility model is used, the vacuum pump 16 is utilized to pump the inner cavity 4 into a vacuum environment, the condensate with lower temperature is respectively injected into the condensate inlet 10, the heat conducting oil is injected into the heat conducting oil inlet 6, the circulation of the condensate and the heat conducting oil is ensured, the motor 15 is started to drive the stirring blade 8 to rotate, then the feed liquid is injected into the inner cavity 4 through the feed inlet 11, the feed liquid is changed into a thin liquid film along the inner wall of the inner cavity 4 under the action of the stirring blade 8 in the process of flowing downwards along the inner wall of the inner cavity 4, the inner wall of the inner cavity 4 flows along the inner wall, because the side edge of the stirring blade 8 is tightly attached to the inner wall of the inner cavity 4, and the blade of the stirring blade 8 is obliquely arranged, in the stirring process, the feed liquid continuously bears upward force, the feed liquid flows downwards at an extremely slow speed, the temperature of the inner bottom wall of the inner cavity 4 is, the molecules with larger mean free path move until contacting the inner top wall of the inner cavity 4, the temperature of the inner top wall of the inner cavity 4 is lower under the action of condensate, the steam molecules are liquefied and flow into the diversion trench 2 along the inner wall of the inner cavity 4 and finally flow into the light component outlet 3 for collection, and the molecules with smaller mean free path finally flow out through the heavy component outlet 7 of the inner bottom wall of the inner cavity 4.
The above, only be the concrete implementation of the preferred embodiment of the present invention, but the protection scope of the present invention is not limited thereto, and any person skilled in the art is in the technical scope of the present invention, according to the technical solution of the present invention and the utility model, the concept of which is equivalent to replace or change, should be covered within the protection scope of the present invention.
Claims (6)
1. The high-efficiency molecular distillation device comprises a tank body (1) and is characterized in that an inner cavity (4) is arranged in the tank body (1), a diversion trench (2) is arranged on the side wall of the inner cavity (4), a light component outlet (3) is arranged on the side wall of the inner cavity (4), the diversion trench (2) is connected with the light component outlet (3), a condensation mechanism is arranged at the upper end of the tank body (1), a heat conduction mechanism is arranged at the lower end of the tank body (1), a heavy component outlet (7) is arranged on the bottom wall of the inner cavity (4), a fixed plate (14) is fixedly connected onto the tank body (1), a connecting rod (17) is fixedly connected onto the tank body (1), the other end of the connecting rod (17) is fixedly connected onto the lower surface of the fixed plate (14), a vacuum pump (16) is fixedly connected onto the fixed plate (14), and the output end of the vacuum pump (16) penetrates through the tank, and a stirring mechanism is arranged on the fixing plate (14).
2. A high efficiency molecular distillation apparatus according to claim 1, wherein the condensation mechanism comprises a condensation layer (12) disposed at the upper end of the tank (1), and the condensation layer (12) is provided with a condensed water inlet (10) and a condensed water outlet (13).
3. A high efficiency molecular distillation apparatus according to claim 1, wherein the heat conducting mechanism comprises a heat conducting layer (5) disposed at the lower end of the tank (1), and the heat conducting layer (5) is provided with a heat conducting oil inlet (6) and a heat conducting oil outlet (9).
4. A high efficiency molecular distillation apparatus as claimed in claim 1, wherein the stirring mechanism comprises a motor (15) fixedly connected to the fixing plate (14), the output end of the motor (15) penetrates through the fixing plate (14) and extends inwards from the tank (1) and is fixedly connected with a stirring blade (8), and the stirring blade (8) is rotatably connected with the tank (1).
5. A high efficiency molecular distillation apparatus according to claim 4, wherein the side edges of the stirring vanes (8) are closely attached to the side walls of the inner chamber (4).
6. A high efficiency molecular distillation apparatus according to claim 3, wherein the heat conducting layer (5) and the condensing layer (12) are filled with heat insulating material in the tank (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921632632.4U CN210813986U (en) | 2019-09-28 | 2019-09-28 | High-efficient molecular distillation device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201921632632.4U CN210813986U (en) | 2019-09-28 | 2019-09-28 | High-efficient molecular distillation device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN210813986U true CN210813986U (en) | 2020-06-23 |
Family
ID=71250646
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201921632632.4U Active CN210813986U (en) | 2019-09-28 | 2019-09-28 | High-efficient molecular distillation device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN210813986U (en) |
-
2019
- 2019-09-28 CN CN201921632632.4U patent/CN210813986U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A high-efficiency molecular distillation device Effective date of registration: 20220829 Granted publication date: 20200623 Pledgee: Wenxian Rural Credit Cooperative Association Renmin Road Credit Cooperative Pledgor: Henan Liwei Biological Pharmaceutical Co.,Ltd. Registration number: Y2022980013755 |
|
| PE01 | Entry into force of the registration of the contract for pledge of patent right |