CN209270874U - A kind of novel batch-type molecule fractionating device - Google Patents
A kind of novel batch-type molecule fractionating device Download PDFInfo
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- CN209270874U CN209270874U CN201821938444.XU CN201821938444U CN209270874U CN 209270874 U CN209270874 U CN 209270874U CN 201821938444 U CN201821938444 U CN 201821938444U CN 209270874 U CN209270874 U CN 209270874U
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- tower reactor
- drainage conduit
- storage tank
- material kettle
- heat
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Abstract
The utility model discloses a kind of novel batch-type molecule fractionating devices, including the first tower reactor, second tower reactor, condenser, material kettle, heat-conducting oil heating seat, feed pipe, first storage tank, second storage tank, oil guide pipe, collect pendular ring, reflux splitter, return pipe, first drainage conduit, second drainage conduit and thermally conductive font, first tower reactor and the second tower reactor bottom are mounted on material kettle, the material kettle lower surface of first tower reactor bottom has wrapped heat-conducting oil heating seat, and material kettle side is equipped with feed pipe, the material kettle lower surface of second tower reactor bottom is fixed with thermally conductive font, and thermally conductive font is connected to heat-conducting oil heating seat by oil guide pipe, this fractionating device carries out fractionation work using two tower reactors, using a fraction products as secondary fractionation raw material, increase fraction products purity, improve product quality, simultaneously the first tower reactor with Second tower reactor shares a heat source and condenser, reduces the investment of heat resource equipment.
Description
Technical field
The utility model relates to fractionating technology field, specially a kind of novel batch-type molecule fractionating device.
Background technique
Step is important to the fractionation of natural perfume material in the process of natural perfume material, this process can obtain naturally
The isolated molecule of fragrance, improves the quality of natural perfume material, and being fractionated used device now is fractionating column, if expecting high-precision
Fractionation, the height of fractionating column and the investment of device must increase, therefore improve a large amount of cost.For this purpose, it is proposed that a kind of
Novel batch-type molecule fractionating device.
Summary of the invention
The purpose of this utility model is to provide a kind of novel batch-type molecule fractionating devices, to solve above-mentioned background technique
The problem of middle proposition.
To achieve the above object, the utility model provides the following technical solutions: a kind of novel batch-type molecule fractionating device,
Including the first tower reactor, the second tower reactor, condenser, material kettle, heat-conducting oil heating seat, feed pipe, the first storage tank, the second storage tank,
Oil guide pipe, collection pendular ring, reflux splitter, return pipe, the first drainage conduit, the second drainage conduit and thermally conductive font, first tower reactor
It is mounted on material kettle with the second tower reactor bottom, the material kettle lower surface of first tower reactor bottom has wrapped heat-conducting oil heating
Seat, and material kettle side is equipped with feed pipe, the material kettle lower surface of second tower reactor bottom is fixed with thermally conductive font, and conduction oil
Seat is connected to heat-conducting oil heating seat by oil guide pipe, is mounted on several collection pendular rings inside first tower reactor and the second tower reactor,
It is equipped with condenser at the top of first tower reactor, and is connect with condenser at the top of the first tower reactor and the second tower reactor, first tower
It is equipped with the first storage tank and the second storage tank between kettle and the second tower reactor, collection pendular ring corresponding position is located on the outside of first tower reactor
It is respectively connected with the first drainage conduit, and the first drainage conduit is connect with the first storage tank, collection pendular ring pair is located on the outside of second tower reactor
Position is answered to be respectively connected with the second drainage conduit, and the second drainage conduit is connected to the second storage tank, first drainage conduit and second row
Expects pipe is communicated with return pipe, and return pipe is connect with the material kettle of the second tower reactor bottom, and reflux point is equipped in the middle part of the return pipe
Orchestration.
Preferably, first storage tank and the second storage tank are respectively connected with vacuum tube, and vacuum tube top and condenser
Connection.
Preferably, filler is mounted on inside first tower reactor and the second tower reactor.
Preferably, return valve is mounted on the outside of first drainage conduit, the second drainage conduit, return pipe and vacuum tube.
Preferably, first tower reactor is adjacent with the second tower reactor position.
Compared with prior art, the utility model has the beneficial effects that
1, the liquid fractionation that collection pendular ring is collected in the first tower reactor of the utility model is separated by the first drainage conduit exports, the first storing
Tank collects the product of the first tower reactor fractionation, and the liquid fractionation that collection pendular ring is collected in the second tower reactor is separated by the second drainage conduit to be exported, the
Two storage tanks collect the product of the second tower reactor fractionation, and the phegma of the first tower reactor is imported by return pipe in the material kettle of the second tower reactor
Secondary fractionation is carried out, this fractionating device carries out fractionation work using two tower reactors, former using a fraction products as secondary fractionation
Material increases fraction products purity, improves product quality.
2, the first tower reactor of the utility model and the second tower reactor share a heat source and condenser, and the first tower reactor and second
Tower reactor position is close to the investment for reducing heat resource equipment reduces the loss of the energy.
Detailed description of the invention
Fig. 1 is the utility model overall structure diagram.
In figure: 1, the first tower reactor;2, the second tower reactor;3, condenser;4, material kettle;5, heat-conducting oil heating seat;6, feed pipe;7,
First storage tank;8, the second storage tank;9, oil guide pipe;10, collect pendular ring;11, filler;12, reflux splitter;13, return pipe;
14, the first drainage conduit;15, vacuum tube;16, return valve;17, the second drainage conduit;18, thermally conductive font.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
Referring to Fig. 1, the utility model provides a kind of technical solution: a kind of novel batch-type molecule fractionating device, including
First tower reactor 1, the second tower reactor 2, condenser 3, material kettle 4, heat-conducting oil heating seat 5, feed pipe 6, the first storage tank 7, the second storing
Tank 8, oil guide pipe 9, collection pendular ring 10, reflux splitter 12, return pipe 13, the first drainage conduit 14, the second drainage conduit 17 and conduction oil
Seat 18, the first tower reactor 1 and 2 bottom of the second tower reactor are mounted on material kettle 4, and 4 lower surface of material kettle of 1 bottom of the first tower reactor wraps
There is heat-conducting oil heating seat 5,5 heating efficiency of heat-conducting oil heating seat is high, and 4 side of material kettle is equipped with feed pipe 6, passes through feed pipe 6
Raw material is added in material kettle 4, and 4 lower surface of material kettle of 2 bottom of the second tower reactor is fixed with thermally conductive font 18, and thermally conductive font 18 with it is thermally conductive
Oily heated seats 5 are connected to by oil guide pipe 9, and the first tower reactor 1 and the second tower reactor 2 share a heat source, save equipment investment, the first tower
Be mounted on several collection pendular rings 10 inside kettle 1 and the second tower reactor 2, be equipped with condenser 3 at the top of the first tower reactor 1, and the first tower reactor 1 with
Second tower reactor, 2 top is connect with condenser 3, and the first storage tank 7 and the second storage are equipped between the first tower reactor 1 and the second tower reactor 2
Batch can 8 is located at collection 10 corresponding position of pendular ring on the outside of first tower reactor 1 and is respectively connected with the first drainage conduit 14, collects pendular ring in the first tower reactor 1
10 liquid fractionations collected are separated by the first drainage conduit 14 to be exported, and the first drainage conduit 14 is connect with the first storage tank 7, the first storing
Tank 7 collects the product of the first tower reactor 1 fractionation, and collection 10 corresponding position of pendular ring is located on the outside of the second tower reactor 2 and is respectively connected with the second discharge
Pipe 17, the liquid fractionation that collection pendular ring 10 is collected in the second tower reactor 2 is separated by the second drainage conduit 17 to be exported, and the second drainage conduit 17 and the
The connection of two storage tanks 8, the second storage tank 8 collect the product of the second tower reactor 2 fractionation, and the first drainage conduit 14 and the second drainage conduit 17 connect
It is connected with return pipe 13, and return pipe 13 is connect with the material kettle 4 of 2 bottom of the second tower reactor, the phegma of the first tower reactor 1 passes through return pipe
13 import the secondary fractionation of progress in the material kettle 4 of the second tower reactor 2, are equipped with reflux splitter 12 in the middle part of return pipe 13.
First storage tank 7 and the second storage tank 8 are respectively connected with vacuum tube 15, and 15 top of vacuum tube is connect with condenser 3,
Control works in a low voltage state, guarantees the raising of working efficiency.
It is mounted on filler 11 inside first tower reactor 1 and the second tower reactor 2, the contact area of gas-liquid two-phase is increased, more connects
Close vapor liquid equilibrium, improves separative efficiency.
It is mounted on return valve 16 on the outside of first drainage conduit 14, the second drainage conduit 17, return pipe 13 and vacuum tube 15, is guaranteed
Each pipe path controllability.
First tower reactor 1 is adjacent with 2 position of the second tower reactor, reduces the loss of heat conduction, energy saving.
It should be noted that, in this document, relational terms such as first and second and the like are used merely to a reality
Body or operation are distinguished with another entity or operation, are deposited without necessarily requiring or implying between these entities or operation
In any actual relationship or order or sequence.Moreover, the terms "include", "comprise" or its any other variant are intended to
Non-exclusive inclusion, so that the process, method, article or equipment including a series of elements is not only wanted including those
Element, but also including other elements that are not explicitly listed, or further include for this process, method, article or equipment
Intrinsic element.
While there has been shown and described that the embodiments of the present invention, for the ordinary skill in the art,
It is understood that these embodiments can be carried out with a variety of variations in the case where not departing from the principles of the present invention and spirit, repaired
Change, replacement and variant, the scope of the utility model is defined by the appended claims and the equivalents thereof.
Claims (5)
1. a kind of novel batch-type molecule fractionating device, including the first tower reactor (1), the second tower reactor (2), condenser (3), material kettle
(4), heat-conducting oil heating seat (5), feed pipe (6), the first storage tank (7), the second storage tank (8), oil guide pipe (9), collection pendular ring
(10), reflux splitter (12), return pipe (13), the first drainage conduit (14), the second drainage conduit (17) and thermally conductive font (18),
Be characterized in that: first tower reactor (1) and the second tower reactor (2) bottom are mounted on material kettle (4), the first tower reactor (1) bottom
Material kettle (4) lower surface wrapped heat-conducting oil heating seat (5), and material kettle (4) side is equipped with feed pipe (6), described
Material kettle (4) lower surface of two tower reactors (2) bottom is fixed with thermally conductive font (18), and thermally conductive font (18) and heat-conducting oil heating seat
(5) it is connected to by oil guide pipe (9), is mounted on several collection pendular rings (10) inside first tower reactor (1) and the second tower reactor (2),
Be equipped with condenser (3) at the top of first tower reactor (1), and at the top of the first tower reactor (1) and the second tower reactor (2) with condenser (3)
Connection, equipped with the first storage tank (7) and the second storage tank (8) between first tower reactor (1) and the second tower reactor (2), described the
Be located at collection pendular ring (10) corresponding position on the outside of one tower reactor (1) to be respectively connected with the first drainage conduit (14), and the first drainage conduit (14) with
First storage tank (7) connection, the second tower reactor (2) outside are located at collection pendular ring (10) corresponding position and are respectively connected with the second drainage conduit
(17), and the second drainage conduit (17) is connected to the second storage tank (8), and first drainage conduit (14) and the second drainage conduit (17) are even
It is connected with return pipe (13), and return pipe (13) is connect with the material kettle (4) of the second tower reactor (2) bottom, in the middle part of the return pipe (13)
Reflux splitter (12) are installed.
2. a kind of novel batch-type molecule fractionating device according to claim 1, it is characterised in that: first storage tank
(7) it is respectively connected with vacuum tube (15) with the second storage tank (8), and is connect at the top of vacuum tube (15) with condenser (3).
3. a kind of novel batch-type molecule fractionating device according to claim 1, it is characterised in that: first tower reactor
(1) and inside the second tower reactor (2) filler (11) are mounted on.
4. a kind of novel batch-type molecule fractionating device according to claim 1, it is characterised in that: first drainage conduit
(14), return valve (16) are mounted on the outside of the second drainage conduit (17), return pipe (13) and vacuum tube (15).
5. a kind of novel batch-type molecule fractionating device according to claim 1, it is characterised in that: first tower reactor
(1) adjacent with the second tower reactor (2) position.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201821938444.XU CN209270874U (en) | 2018-11-23 | 2018-11-23 | A kind of novel batch-type molecule fractionating device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201821938444.XU CN209270874U (en) | 2018-11-23 | 2018-11-23 | A kind of novel batch-type molecule fractionating device |
Publications (1)
Publication Number | Publication Date |
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CN209270874U true CN209270874U (en) | 2019-08-20 |
Family
ID=67602224
Family Applications (1)
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CN201821938444.XU Active CN209270874U (en) | 2018-11-23 | 2018-11-23 | A kind of novel batch-type molecule fractionating device |
Country Status (1)
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CN (1) | CN209270874U (en) |
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2018
- 2018-11-23 CN CN201821938444.XU patent/CN209270874U/en active Active
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