CN209162252U - A kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio - Google Patents

A kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio Download PDF

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Publication number
CN209162252U
CN209162252U CN201821767860.8U CN201821767860U CN209162252U CN 209162252 U CN209162252 U CN 209162252U CN 201821767860 U CN201821767860 U CN 201821767860U CN 209162252 U CN209162252 U CN 209162252U
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crucible
silicon
silicon ingot
conversion ratio
heat
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汪伟华
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Zhejiang Yi Yang Solar Power Science And Technology Ltd
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Zhejiang Yi Yang Solar Power Science And Technology Ltd
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Abstract

The utility model relates to a kind of polycrystal silicon ingot pouring devices of efficient photoelectricity treater conversion ratio, belong to photovoltaic technology field, it solves the problems, such as that polycrystal silicon ingot crystal dislocation density is big in the prior art.The polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio includes furnace body, heat-insulation cage equipped with liftable movement in furnace body, crucible, crucible guard boards, graphite bottom plate, graphite cover board, top heater and side heater are equipped in heat-insulation cage, graphite bottom plate is placed on heat exchange platform, crucible is placed on graphite bottom plate, heat exchange platform is equipped with auxiliary cooling device, and cooling temperature is adjusted in the auxiliary cooling device.The polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio crucible bottom in casting is laid with high temperature resistant silicon particle, on the one hand play the role of forming the preferable forming core of crystal phase structure, on the other hand since silicon particle is coated with high-temperature-resistant layer, can preventing silicon particle, all melting causes texture chaotic again, can play the role of fixing forming core well.

Description

A kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio
Technical field
The utility model belongs to photovoltaic technology field, is related to a kind of pouring device of polycrystal silicon ingot, especially a kind of fritting The device of method casting polycrystal silicon ingot.
Background technique
Solar power generation is the important means of human use's solar energy, and solar battery is then the master for realizing photoelectric conversion Device is wanted, the photoelectric conversion efficiency of solar battery determines the utilization conversion ratio of solar energy source.In recent years, world's solar-electricity The speed of the yield in pond and installed capacity every year all 30% is fast-developing.Currently, the accumulative installed capacity in the whole world is 25.4GW, in advance It counts the installed capacity of the year two thousand twenty whole world and is up to 278GW.
Currently, the type of solar battery is increasing, wherein crystal silicon solar energy battery especially polycrystalline silicon solar Battery will occupy leading position within following one period with lower cost and higher transfer efficiency.But relative to Traditional energy, the cost is relatively high for polycrystalline silicon solar power generation, and market rate is relatively low.From current global situation and entire row From the point of view of the development of industry, improving the transfer efficiency of polysilicon solar cell, reducing the cost of electricity-generating of photovoltaic module is photovoltaic industry Inexorable trend.As how lower cost prepares hot spot of the efficient solar battery as industry research.Except battery Outside technological factor, the excessively high dislocation density of conventional polysilicon silicon wafer is one of the principal element for limiting polycrystal silicon cell transfer efficiency. On the one hand dislocation producing cause in conventional polysilicon silicon wafer is that carbon content is excessively high in silicon ingot, carbon atom is small compared with silicon atom radius, meeting Cause biggish distortion of lattice, generates a large amount of dislocations;It on the other hand is the limitation of traditional directional freeze method, at the beginning of crystal growth Phase, there are biggish dislocation density in crystal, later period dislocation multiplication causes whole spindle position dislocation density excessively high, directly affects the sun The incident photon-to-electron conversion efficiency of energy battery.
For the bad situation of crystal growth primary growth, seed crystal high-efficiency polycrystalline silicon technology can be used, that is, used millimeter Grade silicon material carries out epitaxial growth as nucleating center, and the silicon liquid of melting is guided to carry out when solidifying by nucleating center of high quality silicon material Columnar growth.And in crystal growing process, temperature gradient when directional solidification is also the important ring for determining crystal quality, existing The problem of the type of cooling maximum used in technology is non-uniform temperature at Solid-Liquid Separation, and generating transverse temperature difference leads to crystal The orientation of growth is poor, big so as to cause the dislocation density of polycrystal silicon ingot, affects the incident photon-to-electron conversion efficiency of solar battery.
Utility model content
The purpose of this utility model is the presence of the above problem in view of the prior art, proposes a kind of small more of dislocation density Crystal silicon ingot pouring device.
The purpose of this utility model can be realized by the following technical scheme: a kind of polycrystal silicon ingot of efficient photoelectricity treater conversion ratio Pouring device, including furnace body, the heat-insulation cage equipped with liftable movement in the furnace body, be equipped in the heat-insulation cage crucible, Crucible guard boards, graphite bottom plate, graphite cover board, top heater and side heater, the graphite bottom plate are placed on heat exchange On platform, the crucible is placed on graphite bottom plate, which is characterized in that the crucible bottom is laid with one layer of silicon particle, described Silicon particle layer formed have countless holes supporting structure, the silicon particle be surface coating silicon nitride layer high temperature resistant Silicon particle, the crucible bottom and side are coated with silicon nitride coating.
Original silicon fusing point in silicon particle is 1420 ± 2 °, and traditional half process of smelting uses merely silicon particle to lay crucible bottom Portion, once seed crystal has melted, cannot play seed crystal forming core work because affected by many factors in ingot casting stove heating, fusion process With.And when silicon particle surface is covered with silicon nitride powder, it will play the role of protecting silicon particle, so as not to fusing, thus It is effectively maintained seed crystal.Silicon nitride chemical formula Si3N4, white powder crystal, 1900 DEG C of fusing point, silicon nitride pole high temperature resistant, by It will not be melt into melt body after heat, can just be decomposed until 1900 DEG C.Therefore without repeatedly souning out solid liquid interface in silicon material melting process, Certain time between 1420~1900 DEG C only need to be kept, melting to wear without having to worry about silicon particle influences its function as forming core. The setting of silicon nitride layer on crucible internal walls, the impurity that crucible internal walls can be effectively prevented enters in crystal, and prevents polycrystal silicon ingot Viscous pot phenomenon occurs, to improve the quality of polycrystal silicon ingot and reduce the operation difficulty of casting ingot process.
In the polycrystal silicon ingot pouring device of above-mentioned efficient photoelectricity treater conversion ratio, the heat exchange platform is equipped with auxiliary Cooling temperature is adjusted in cooling device, the auxiliary cooling device.
During long brilliant, for the variation for realizing longitudinal temperature gradient, after heat-insulation cage rises, due to bottom silicon ingot no longer into Row heating, therefore bottom silicon ingot and peripheral temperature reduce, since the temperature of silicon ingot two sides is nature decline, bottom temp is also certainly So decline, in the initial stage, silicon ingot side and distance from bottom solid liquid interface are equidistant, therefore the interface of solid-liquid intersection is in cross Temperature is identical on direction, and long crystalline substance process is smooth, but with the rising of silicon ingot solid liquid interface, bottom heat exchange and side heat exchange Efficiency will be significantly different, because more and more remoter with solid liquid interface at the heat exchange of bottom, and the side of solid liquid interface and sidewall of crucible Distance is constant always, and the side of solid liquid interface and middle portion temperature imbalance lead to transverse temperature difference occur in order to prevent, influences long crystalline substance Direction needs the raising with solid liquid interface, steps up the heat exchanger effectiveness of silicon ingot bottom, equal to reach solid liquid interface temperature Weighing apparatus, there is no the purposes of transverse temperature difference.Using auxiliary cooling device, cooling efficiency is adjusted, is continuously improved during long brilliant The heat exchanger effectiveness of bottom, so that bottom is consistent with the temperature gradient of side.
In the polycrystal silicon ingot pouring device of above-mentioned efficient photoelectricity treater conversion ratio, the auxiliary cooling device includes setting In the cooling line of heat exchange mesa base, the external argon gas of the cooling line, the inlet end of the cooling line is equipped with Frequency-changeable compressor.Using frequency-changeable compressor according to different temperatures demand, gas flow is improved, to change cooling velocity, is guaranteed The transverse temperature difference that solid-liquid is practised physiognomy is as small as possible.
This polycrystal silicon ingot casting device further includes argon inlet pipe, and the argon inlet pipe passes through furnace body, heat-insulation cage, and Connect with the cooling line on heat exchange platform, the external escape pipe in the outlet side of the cooling line, the escape pipe around It is protruded into crucible above to heat-insulation cage and across top heater and graphite cover board, the air-flow that the escape pipe sprays is directed at earthenware Melt above crucible.
The effect of argon inlet pipe is to provide cooling for cooling line, simultaneously as argon gas is laggard by cooling line Sufficient heat exchange is gone, therefore the argon gas sprayed from escape pipe is high temperature argon, so that argon gas is directly injected into the silicon of melting The temperature decrease that not will lead to silicon liquid on liquid is conducive to maintain the temperature gradient of silicon liquid unaffected, in addition, the mesh of injection argon gas Be the impurity that suspends in silicon liquid is carried out it is evenly dispersed so that the silicon ingot ingredient after solidify is uniform, crystal phase structure after long crystalline substance Stablize, dislocation density is small, effectively promotes polycrystal silicon ingot quality.
Alternatively, in the polycrystal silicon ingot pouring device of above-mentioned efficient photoelectricity treater conversion ratio, the auxiliary Cooling device includes the cooling water channel being set in heat exchange platform, and the cooling water channel is circular layout in heat exchange platform bottom Portion, the cooling water channel are equipped with flow control valve.Argon inlet pipe passes through furnace body, heat-insulation cage, top heater and graphite Cover board is directly protruding into crucible.
In the polycrystal silicon ingot pouring device of above-mentioned efficient photoelectricity treater conversion ratio, the furnace body is equipped with vacuum orifice, The crucible guard boards are equipped with exhaust outlet.
The another object of the utility model is to provide a kind of polycrystal silicon ingot casting method that crystal dislocation density is small: including Following steps: 1), charging before, high temperature resistant silicon particle be uniformly layered on to the crucible bottom of spraying silicon nitride;
2) it, charges;Silicon material is loaded in crucible, and then furnace body is vacuumized;
3), heat: open top part heater and side heater adjust heat-insulation cage height during melting silicon materials, allow Thermal field forms biggish temperature gradient, upper heat and lower cold, to guarantee that silicon material orients fusing from top to bottom;During melting silicon materials Crucible bottom remains i.e. 1420 DEG C of < of supercooling, and high temperature resistant silicon particle is made to be attached to crucible bottom always;
4) after, silicon material has all melted, crucible bottom high temperature resistant silicon particle retains 0.1~1.5cm thickness, covers entire crucible Bottom surface and highly uniform;Argon inlet pipe is opened, argon gas enters cooling pipe by argon inlet pipe, on the one hand flat to heat exchange Platform is cooled down, it is on the other hand heated after melt upper surface of the argon gas into crucible spray gas, then slowly promoted every Hot cage reduces the temperature of silicon melt, forms certain degree of supercooling, and silicon melt starts on the basis of the silicon particle of endless running down It is long brilliant to start forming core;
5), into after growing brilliant process, high temperature resistant silicon particle plays the role of good forming core, and melted silicon erects on the basis of forming core It is straight long brilliant, until heat-insulation cage is promoted to all silicon melts and crystallizes completion;
6), after the completion of whole melt crystallizations, annealed and cooling obtains polycrystal silicon ingot.
Silicon particle place mat in crucible bottom be it is disorderly arranged, particle layer forms a supporting structure, which has Countless holes, in the melting silicon materials stage, the silicon melt that melting silicon materials are formed will be filled in hole, in the initial forming core stage, Under supercooled state, multiple equally distributed forming core sources are formed in silicon particle level, so that it is good to obtain polycrystal silicon ingot Initial forming core, and then grow the crystal with advantage crystal orientation.Specifically, control temperature makes in silicon melt and unfused silicon The silicon melt that material is formed by the silicon melt of solid liquid interface and is filled in hole first reaches supercooled state, and preferential forming core crystallizes, Subsequent silicon melt circle is mobile away from the direction of crucible bottom, silicon melt crystallization and freezing.The initial forming core of polycrystal silicon ingot obtains Good control, to grow beneficial to the prevailing crystal of crystal orientation, therefore can prevent a large amount of proliferation of dislocation, obtain height Quality polycrystal silicon ingot.
In above-mentioned step 4), with the promotion of heat-insulation cage, compressor horsepower gradually mentions the frequency-changeable compressor Height, so that argon gas flows fast flow velocity and is gradually increased, cooling line heat exchanger effectiveness is gradually increased.
Compared with prior art, the polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio crucible bottom in casting is laid with On the one hand high temperature resistant silicon particle plays the role of forming the preferable forming core of crystal phase structure, on the other hand since silicon particle is coated with resistance to Heat zone, can preventing silicon particle, all melting causes texture chaotic again, can play the role of fixing forming core well, separately It is outer to pass through setting auxiliary cooling device, the heat exchanger effectiveness of adjustable bottom heat exchange platform, so that silicon ingot bottom and side Portion's temperature gradient is uniform, eliminates the transverse temperature difference of solid liquid interface, so that long chip reduces dislocation density, protecting to stabilization Temperature of thermal field gradient stabilization is demonstrate,proved, in the case that primary crystalline quality is high, crystal growth is good after polycrystal silicon ingot directional solidification, crystal Dislocation density is low, applied to can effectively improve incident photon-to-electron conversion efficiency on solar battery.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio;
Fig. 2 is the structural schematic diagram of heat exchange platform in the polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio.
In figure, 1, furnace body;11, vacuum orifice;2, heat-insulation cage;3, crucible;4, crucible guard boards;41, exhaust outlet;5, graphite bottom Plate;51, graphite cover board;6, top heater;61, side heater;7, heat exchange platform;71, cooling line;8, argon inlet Pipe;81, escape pipe;9, silicon particle.
Specific embodiment
It is specific embodiment of the utility model and in conjunction with attached drawing below, the technical solution of the utility model is made further Description, but the utility model is not limited to these examples.
As shown in Figs. 1-2, the polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio, including furnace body 1, the furnace body 1 The interior heat-insulation cage 2 equipped with liftable movement, the heat-insulation cage 2 is interior to be equipped with crucible 3, crucible guard boards 4, graphite bottom plate 5, graphite cover Plate 51, top heater 6 and side heater 61, the graphite bottom plate 5 are placed on heat exchange platform 7, the crucible 3 It is placed on graphite bottom plate 5,3 bottom of crucible is laid with one layer of silicon particle 9, and 9 layers of silicon particle form with countless holes Supporting structure, the silicon particle 9 are the high temperature resistant silicon particle 9 of surface coating silicon nitride layer.Original silicon fusing point in silicon particle 9 It is 1420 ± 2 DEG C, traditional half process of smelting uses merely silicon particle 9 to lay 3 bottom of crucible, in ingot casting stove heating, fusion process Because affected by many factors, once seed crystal has melted, seed crystal forming core cannot be played the role of.And when 9 surface of silicon particle is covered with nitrogen When SiClx powder, it will play the role of protecting silicon particle 9, so as not to fusing, to be effectively maintained seed crystal.Silicon nitride Formula Si3N4, white powder crystal, 1900 DEG C of fusing point, silicon nitride pole high temperature resistant will not be melt into melt body after heated, until 1900 It DEG C can just decompose.Therefore it need to only be kept between 1420~1900 DEG C in silicon material melting process without repeatedly souning out solid liquid interface Certain time, melting to wear without having to worry about silicon particle 9 influences its function as forming core.3 bottom of crucible and side spray It is coated with silicon nitride coating.The setting of silicon nitride layer on 3 inner wall of crucible, the impurity that 3 inner wall of crucible can be effectively prevented enter crystal In, and prevent polycrystal silicon ingot from viscous pot phenomenon occurs, to improve the quality of polycrystal silicon ingot and reduce the operation difficulty of casting ingot process. The furnace body 1 is equipped with vacuum orifice 11, and for vacuumizing to furnace body 1, the crucible guard boards 4 are equipped with exhaust outlet 41, For being recycled to injection to the argon gas in crucible 3.
In the polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio, the heat exchange platform 7 is equipped with supplement heat rejecter Cooling temperature is adjusted in device, the auxiliary cooling device.The auxiliary cooling device includes being set to heat exchange platform 7 The inlet end of the cooling line 71 of bottom, the external argon gas of cooling line 71, the cooling line 71 is equipped with frequency conversion pressure Contracting machine.The argon inlet pipe 8 passes through furnace body 1, heat-insulation cage 2, and connect with the cooling line 71 on heat exchange platform 7, institute The external escape pipe 81 in the outlet side for the cooling line 71 stated, the escape pipe 81 add around to 2 top of heat-insulation cage and across top Hot device 6 and graphite cover board 51 protrude into crucible 3, the melt for 3 top of air-flow alignment crucible that the escape pipe 81 sprays.
During long brilliant, for the variation for realizing longitudinal temperature gradient, after heat-insulation cage 2 rises, no longer due to bottom silicon ingot It is heated, therefore bottom silicon ingot and peripheral temperature reduce, since the temperature of silicon ingot two sides is nature decline, bottom temp is also Naturally decline, in the initial stage, silicon ingot side and distance from bottom solid liquid interface are equidistant, therefore the interface of solid-liquid intersection exists Temperature is identical in transverse direction, and long crystalline substance process is smooth, but as the rising of silicon ingot solid liquid interface, bottom heat exchange and side heat are handed over Changing efficiency will be significantly different, because more and more remoter with solid liquid interface at the heat exchange of bottom, and the side of solid liquid interface and 3 wall of crucible Distance it is constant always, the side of solid liquid interface and middle portion temperature imbalance lead to transverse temperature difference occur in order to prevent, influence to grow Chip is to needing the raising with solid liquid interface, step up the heat exchanger effectiveness of silicon ingot bottom, to reach solid liquid interface temperature Equilibrium, there is no the purposes of transverse temperature difference.Using auxiliary cooling device, cooling efficiency is adjusted, is constantly mentioned during long brilliant The heat exchanger effectiveness of high bottom, so that bottom is consistent with the temperature gradient of side.Using frequency-changeable compressor according to different temperatures need It asks, improves gas flow, to change cooling velocity, the transverse temperature difference for guaranteeing that solid-liquid is practised physiognomy is as small as possible.Argon inlet pipe 8 Effect is to provide cooling for cooling line 71, simultaneously as argon gas has carried out sufficient heat exchange after cooling line 71, Therefore the argon gas sprayed from escape pipe 81 is high temperature argon, so that argon gas, which is directly injected into the silicon liquid of melting, not will lead to silicon liquid Temperature decrease, be conducive to maintain silicon liquid temperature gradient it is unaffected, in addition, injection argon gas purpose be in silicon liquid hang Floating impurity progress is evenly dispersed, so that the silicon ingot ingredient after solidifying is uniform, crystal phase structure is stablized after long crystalline substance, and dislocation density is small, Effectively promote polycrystal silicon ingot quality.
The casting method of the polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio: include the following steps:
1) before, charging, high temperature resistant silicon particle 9 is uniformly layered on to 3 bottom of crucible of spraying silicon nitride, thickness 0.5~ 2cm;
2) it, charges;Silicon material is loaded in crucible 3, and then furnace body 1 is vacuumized;
3), heat: it is high to adjust heat-insulation cage 2 during melting silicon materials for open top part heater 6 and side heater 61 Degree, allows thermal field to form biggish temperature gradient, upper heat and lower cold, to guarantee that silicon material orients fusing from top to bottom;In melting silicon materials 3 bottom of crucible remains i.e. 1420 DEG C of < of supercooling in the process, and high temperature resistant silicon particle 9 is made to be attached to 3 bottom of crucible always;
4) after, silicon material has all melted, 3 bottom high temperature resistant silicon particle 9 of crucible retains 0.1~1.5cm thickness, covers entire earthenware 3 bottom surface of crucible and highly uniform;Argon inlet pipe 8 is opened, argon gas enters cooling pipe by argon inlet pipe 8, on the one hand to heat Switching plane 7 is cooled down, and gas is sprayed in melt upper surface of the argon gas after another aspect is heated into crucible 3, then slowly It is slow to promote heat-insulation cage 2, reduce the temperature of silicon melt, it is 10k/min that temperature, which reduces amplitude, forms certain degree of supercooling, and silicon is molten Body starts to start forming core long crystalline substance on the basis of the silicon particle 9 of endless running down;
5), into after growing crystalline substance, high temperature resistant silicon particle 9 plays the role of good forming core, and melted silicon is vertical on the basis of forming core It is long brilliant, until heat-insulation cage 2 is promoted to all silicon melts and crystallizes completion;
6), after the completion of whole melt crystallizations, annealed and cooling obtains polycrystal silicon ingot.
9 place mat of silicon particle is disorderly arranged, particle layer one supporting structure of formation, supporting structure tool in 3 bottom of crucible There is countless holes, in the melting silicon materials stage, the silicon melt that melting silicon materials are formed will be filled in hole, in initial forming core rank Section, under supercooled state, forms multiple equally distributed forming core sources in 9 level of silicon particle, so that it is good to obtain polycrystal silicon ingot Good initial forming core, and then grow the crystal with advantage crystal orientation.Specifically, control temperature make in silicon melt with it is unfused The silicon material silicon melt that is formed by the silicon melt of solid liquid interface and is filled in hole first reach supercooled state, preferential forming core knot Crystalline substance, subsequent silicon melt circle is mobile away from the direction of 3 bottom of crucible, silicon melt crystallization and freezing.The initial forming core of polycrystal silicon ingot It is well controlled, to grow beneficial to the prevailing crystal of crystal orientation, therefore a large amount of proliferation of dislocation can be prevented, obtained To high quality polycrystal silicon ingot.
In above-mentioned step 4), with the promotion of heat-insulation cage 2, compressor horsepower gradually mentions the frequency-changeable compressor Height, so that argon gas flows fast flow velocity and is gradually increased, 71 heat exchanger effectiveness of cooling line is gradually increased.
The polycrystal silicon ingot pouring device of this efficient photoelectricity treater conversion ratio is handed over by setting auxiliary cooling device, adjustable bottom heat The heat exchanger effectiveness of platform 7 is changed, so that silicon ingot bottom and side temperature gradient are uniform, eliminates the laterally temperature of solid liquid interface Difference, in addition, 3 bottom of crucible is laid with high temperature resistant silicon particle 9, on the one hand rises so that long chip reduces dislocation density to stabilization Silicon particle 9 can be prevented all on the other hand since silicon particle 9 is coated with high-temperature-resistant layer to the preferable forming core effect of crystal phase is formed Melting causes texture chaotic again, can play the role of fixing forming core well, is guaranteeing temperature of thermal field gradient stabilization, just In the case that beginning crystal quality is high, crystal growth is good after polycrystal silicon ingot directional solidification, and crystal dislocation density is low, is applied to the sun Incident photon-to-electron conversion efficiency can be effectively improved on battery.
The specific embodiments described herein are merely examples of the spirit of the present invention.The utility model institute Belonging to those skilled in the art can make various modifications or additions to the described embodiments or using similar Mode substitute, but without departing from the spirit of the present application or beyond the scope of the appended claims.

Claims (6)

1. a kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio, including furnace body, the interior liftable that is equipped with of the furnace body is transported Dynamic heat-insulation cage, the heat-insulation cage is interior to be equipped with crucible, crucible guard boards, graphite bottom plate, graphite cover board, top heater and side Heater, the graphite bottom plate are placed on heat exchange platform, and the crucible is placed on graphite bottom plate, and feature exists In the crucible bottom is laid with one layer of silicon particle, and silicon particle layer forms the supporting structure with countless holes, and the silicon is broken Material is the high temperature resistant silicon particle of surface coating silicon nitride layer, and the crucible bottom and side are coated with silicon nitride coating.
2. a kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio according to claim 1, it is characterised in that: described Heat exchange platform be equipped with auxiliary cooling device, cooling temperature is adjusted in the auxiliary cooling device.
3. a kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio according to claim 2, it is characterised in that: described Auxiliary cooling device include the cooling line for being set to heat exchange mesa base, the external argon gas of the cooling line is described Cooling line inlet end be equipped with frequency-changeable compressor.
4. a kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio according to claim 3, it is characterised in that: this is more Crystal silicon ingot casting device further includes argon inlet pipe, the argon inlet pipe pass through furnace body, heat-insulation cage, and with heat exchange platform On cooling line connection, the external escape pipe in the outlet side of the cooling line, the escape pipe is around to above heat-insulation cage And protruded into crucible across top heater and graphite cover board, it is molten above the air-flow alignment crucible that the escape pipe sprays Liquid.
5. a kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio according to claim 2, it is characterised in that: described Auxiliary cooling device include the cooling water channel being set in heat exchange platform, the cooling water channel is circular layout in heat exchange Mesa base, the cooling water channel are equipped with flow control valve, and argon inlet pipe passes through furnace body, heat-insulation cage, top heater It is directly protruding into crucible with graphite cover board.
6. a kind of polycrystal silicon ingot of efficient photoelectricity treater conversion ratio described in any claim is cast dress in -5 according to claim 1 It sets, it is characterised in that: the furnace body is equipped with vacuum orifice, and the crucible guard boards are equipped with exhaust outlet.
CN201821767860.8U 2018-10-30 2018-10-30 A kind of polycrystal silicon ingot pouring device of efficient photoelectricity treater conversion ratio Expired - Fee Related CN209162252U (en)

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