CN209123387U - A kind of long-chain biatomic acid crystalline solid high-efficiency collecting device - Google Patents
A kind of long-chain biatomic acid crystalline solid high-efficiency collecting device Download PDFInfo
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- CN209123387U CN209123387U CN201821702802.7U CN201821702802U CN209123387U CN 209123387 U CN209123387 U CN 209123387U CN 201821702802 U CN201821702802 U CN 201821702802U CN 209123387 U CN209123387 U CN 209123387U
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- coolant
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- intake pipe
- crystallizing tank
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Abstract
The utility model discloses a kind of long-chain biatomic acid crystalline solid high-efficiency collecting devices, including crystallizing tank and crystal collecting tank, coolant seal cover is provided on the outside of the crystallizing tank, one upper side of the coolant seal cover is provided with the first coolant outlet hose, coolant intake pipe is provided with below the other side of the coolant seal cover, first coolant intake pipe is embedded to be cased with the second coolant intake pipe, second coolant intake pipe is fixed on underlying cooler pan, it is connected between the cooler pan by cooling water pipe, the second coolant outlet hose is provided on the cooler pan being located above, the upper end of the crystallizing tank is fixed with mounting bracket, motor is installed in the mounting bracket, the upper side of the crystallizing tank is provided with feed inlet, the lower section discharge port of the crystallizing tank passes through communicating pipe and the fixed company of crystal collecting tank It connects.The utility model, by the way that from the inside and outside cooling down of crystallizing tank, the fast crystallization that cools down is precipitated fastly, collects efficient.
Description
Technical field
The utility model belongs to long-chain biatomic acid preparation technical field, and in particular to a kind of long-chain biatomic acid crystalline solid is efficient
Collection device.
Background technique
Long-chain biatomic acid is also long carbochain biatomic acid, refers to that the normal carbon chain aromatic series containing 10 or more carbon atoms is full
And dicarboxylic acids, it is important fine-chemical intermediate, it can be a series of with synthetic perfume, extraordinary nylon, polyamide hot etc.
The speciality chemical of high added value.
Long-chain biatomic acid needs the decrease temperature crystalline in crystallizing tank tank to be made, and existing crystallizing tank temperature reduces slowly, causes to tie
Brilliant speed of separating out is slow, proposes that a kind of long-chain biatomic acid crystalline solid high-efficiency collecting device is necessary to solve the above problems thus.
Utility model content
The purpose of this utility model is to provide a kind of long-chain biatomic acid crystalline solid high-efficiency collecting devices, to solve above-mentioned back
The problem of being proposed in scape technology.
To achieve the above object, the utility model provides the following technical solutions: a kind of long-chain biatomic acid crystalline solid is efficiently received
Acquisition means, including crystallizing tank and crystal collecting tank are provided with coolant seal cover, the coolant seal cover on the outside of the crystallizing tank
A upper side be provided with the first coolant outlet hose, cooling water input is provided with below the other side of the coolant seal cover
Pipe, first coolant intake pipe is embedded to be cased with the second coolant intake pipe, and second coolant intake pipe is fixed on position
Cooler pan in lower section is connected between the cooler pan by cooling water pipe, and the is provided on the cooler pan being located above
Two coolant outlet hoses, the upper end of the crystallizing tank are fixed with mounting bracket, and motor, the electricity are equipped in the mounting bracket
The output shaft of machine is fixedly connected by shaft coupling with agitating shaft, and the upper side of the crystallizing tank is provided with feed inlet, the knot
The lower section discharge port of brilliant tank with valvular communicating pipe with crystal collecting tank by being fixedly connected, the inside of the crystal collecting tank
Inclined filter screen is installed, the side of the crystal collecting tank is provided with blow tank, the bottom setting of the crystal collecting tank
There is outlet tube, the crystallizing tank is fixed on pedestal by support frame.
Further, the middle part of the cooler pan is hollow structure, and the agitating shaft passes through the middle part of cooler pan, described cold
But disk is fixed on the inside of crystallizing tank by fixed arm.
Further, the radius of first coolant intake pipe is greater than the radius of the second coolant intake pipe, and described the
Two coolant intake pipes are fixed on the inside of the first coolant intake pipe.
Further, the side of the crystal collecting tank is provided with electric control valve, and the electric control valve is set to filter screen
Bottom righthand side, be located on the crystal collecting tank on the outside of electric control valve and be fixed with blow tank.
Further, no less than four cooling water pipes, band on the feed inlet are symmetrically arranged between the cooler pan
There is sealing cover, is provided with inspection hole on the crystallizing tank.
Further, cooling cavity, the first cooling water input are provided between the crystallizing tank and coolant seal cover
Pipe is connected to cooling cavity with the first coolant outlet hose.
The technical effect and advantage of the utility model: the long-chain biatomic acid crystalline solid high-efficiency collecting device, by crystallizing
Coolant seal cover is arranged in the external of tank, injects cooling water from the output of the first coolant outlet hose by the first coolant intake pipe and is
Crystallizing tank cools down from outside, and three layers of cooler pan are arranged inside crystallizing tank, and cooling water pipe are arranged between cooler pan, by the
Two coolant intake pipes injection cooling water is from the second coolant outlet hose, from crystallizing tank internal cooling, and the driving for passing through motor
Agitating shaft stirring, accelerates cooling, so that the cooling velocity of crystallizing tank is fast, crystallization speed of separating out is fast, is filtered by crystal collecting tank
It collects, to make to collect more efficient.
Detailed description of the invention
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the cooler pan and cooling water pipe attachment structure schematic diagram of the utility model;
Fig. 3 is the coolant seal cover structure schematic diagram of the utility model;
Fig. 4 is the crystallization collecting tank structural schematic diagram of the utility model.
In figure: 1 motor, 2 mounting brackets, 3 second coolant outlet hoses, 4 first coolant outlet hoses, 5 crystallizing tanks, 6 cold
But seal closure, 7 support frames, 8 pedestals, 9 outlet tubes, 10 filter screens, 11 agitating shafts, 12 crystal collecting tanks, 13 electric control valves, 14
One coolant intake pipe, 15 second coolant intake pipes, 16 fixed arms, 17 cooling water pipes, 18 cooler pans, 19 feed inlets, 20
Axis device, 21 blow tanks, 22 communicating pipes.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work
Every other embodiment obtained, fall within the protection scope of the utility model.
The utility model provides a kind of long-chain biatomic acid crystalline solid high-efficiency collecting device as shown in Figs 1-4, including knot
Brilliant tank 5 and crystal collecting tank 12, the outside of the crystallizing tank 5 are provided with coolant seal cover 6, the side of the coolant seal cover 6
Top is provided with the first coolant outlet hose 4, is provided with coolant intake pipe 14 below the other side of the coolant seal cover 6,
First coolant intake pipe 14 is embedded to be cased with the second coolant intake pipe 15, and second coolant intake pipe 15 is fixed on
Underlying cooler pan 18 is connected between the cooler pan 18, the cooler pan 18 being located above by cooling water pipe 17
On be provided with the second coolant outlet hose 3, the upper end of the crystallizing tank 5 is fixed with mounting bracket 2, pacifies in the mounting bracket 2
Equipped with motor 1, the output shaft of the motor 1 is fixedly connected by shaft coupling 20 with agitating shaft 11, the upper end side of the crystallizing tank 5
Face is provided with feed inlet 19, and the lower section discharge port of the crystallizing tank 5 passed through with valvular communicating pipe 22 and crystal collecting tank 12
It is fixedly connected, the inside of the crystal collecting tank 12 is equipped with inclined filter screen 10, and the side of the crystal collecting tank 12 is set
It is equipped with blow tank 21, the bottom of the crystal collecting tank 12 is provided with outlet tube 9, and the crystallizing tank 5 is fixed on by support frame 7
On pedestal 8.
Specifically, the middle part of the cooler pan 18 is hollow structure, the agitating shaft 11 passes through the middle part of cooler pan 18, leads to
It crosses the agitation solution of agitating shaft 11 to make, solution and the contact of cooler pan 18 and cooling water pipe 17 are abundant, cool down quicker, described
Cooler pan 18 is fixed on the inside of crystallizing tank 5 by fixed arm 16.
Specifically, the radius of first coolant intake pipe 14 is greater than the radius of the second coolant intake pipe 15, it is described
Second coolant intake pipe 15 is fixed on the inside of the first coolant intake pipe 14.By being connected for the first coolant intake pipe 14
After cooling water, cooling water is synchronous to be input to 18 He of cooler pan by the second coolant intake pipe 15 and the first coolant intake pipe 14
In coolant seal cover 6, water supply enhanced convenience.
Specifically, the side of the crystal collecting tank 12 is provided with electric control valve 13, the electric control valve 13 was set to
The bottom righthand side of strainer 10, the outside that electric control valve 13 is located on the crystal collecting tank 12 are fixed with blow tank 21.Pass through opening
Electric control valve, crystallization are discharged in specified device from blow tank 21.
Specifically, being symmetrically arranged with no less than four cooling water pipes 17 between the cooler pan 18, increase solution contact
Face accelerates cooling, has sealing cover on the feed inlet 19, avoids dust from entering, be provided with inspection hole on the crystallizing tank 5.Side
Just the case where observation crystallization.
Specifically, cooling cavity is provided between the crystallizing tank 5 and coolant seal cover 6, the first cooling water input
Pipe 14 is connected to cooling cavity with the first coolant outlet hose 4.From the fast cooling of the external large area of crystallizing tank 5.
Working principle:
By connecting the first coolant intake pipe 14, cooling water is synchronous cooling by the second coolant intake pipe 15 and first
Water inlet pipe 14 is input in the cooler pan 18 and coolant seal cover 6 of bottom, passes through cooling water pipe 17 between bottom coohng disk 18
Cooling water is diffused into the cooler pan on top and is finally discharged from the second coolant outlet hose 3, is solution from the inside of crystallizing tank 5
Cooling down, it is solution cooling from the outside of crystallizing tank 5 that the cooling water in coolant seal cover 6 is discharged from the first coolant outlet hose 4,
And drive the stirring of agitating shaft 11 to increase contact surface by motor 1 and accelerate cooling, fit on cooling is fast in crystallizing tank 5, crystal
It is precipitated quickly, crystal is observed by the inspection hole on crystallizing tank 5 and is precipitated, the valve on communicating pipe 22 is opened after precipitation,
Crystallization solution enters in crystal collecting tank 12 from communicating pipe 22, is filtered by filter screen 10, and solution is discharged from outlet tube 9, and
Crystal is stored in crystal collecting tank 12, electric control valve 13 is opened, crystal is discharged by blow tank 21.
Finally, it should be noted that the above descriptions are merely preferred embodiments of the present invention, it is not limited to this
Utility model, although the utility model is described in detail with reference to the foregoing embodiments, for those skilled in the art
For, it is still possible to modify the technical solutions described in the foregoing embodiments, or to part of technical characteristic
It is equivalently replaced, within the spirit and principle of the utility model, any modification, equivalent replacement, improvement and so on,
It should be included within the scope of protection of this utility model.
Claims (6)
1. a kind of long-chain biatomic acid crystalline solid high-efficiency collecting device, including crystallizing tank (5) and crystal collecting tank (12), feature exists
In: it is provided with coolant seal cover (6) on the outside of the crystallizing tank (5), a upper side of the coolant seal cover (6) is provided with
One coolant outlet hose (4) is provided with coolant intake pipe (14) below the other side of the coolant seal cover (6), and described the
One coolant intake pipe (14) is embedded to be cased with the second coolant intake pipe (15), and second coolant intake pipe (15) is fixed on
Underlying cooler pan (18) is connected between the cooler pan (18) by cooling water pipe (17), and what is be located above is described cold
But it is provided with the second coolant outlet hose (3) on disk (18), the upper end of the crystallizing tank (5) is fixed with mounting bracket (2), described
It is equipped in mounting bracket (2) motor (1), the output shaft of the motor (1) is fixed by shaft coupling (20) and agitating shaft (11)
Connection, the upper side of the crystallizing tank (5) are provided with feed inlet (19), and the lower section discharge port of the crystallizing tank (5) passes through band
Valvular communicating pipe (22) is fixedly connected with crystal collecting tank (12), and the inside of the crystal collecting tank (12) is equipped with inclination
Filter screen (10), the side of the crystal collecting tank (12) is provided with blow tank (21), the bottom of the crystal collecting tank (12)
Portion is provided with outlet tube (9), and the crystallizing tank (5) is fixed on pedestal (8) by support frame (7).
2. a kind of long-chain biatomic acid crystalline solid high-efficiency collecting device according to claim 1, it is characterised in that: the cooling
The middle part of disk (18) is hollow structure, and the agitating shaft (11) passes through the middle part of cooler pan (18), and the cooler pan (18) passes through
Fixed arm (16) is fixed on the inside of crystallizing tank (5).
3. a kind of long-chain biatomic acid crystalline solid high-efficiency collecting device according to claim 1, it is characterised in that: described first
The radius of coolant intake pipe (14) is greater than the radius of the second coolant intake pipe (15), second coolant intake pipe (15)
It is fixed on the inside of the first coolant intake pipe (14).
4. a kind of long-chain biatomic acid crystalline solid high-efficiency collecting device according to claim 1, it is characterised in that: the crystal
The side of collecting tank (12) is provided with electric control valve (13), and the electric control valve (13) is set to the bottom righthand side of filter screen (10),
It is located on the outside of electric control valve (13) on the crystal collecting tank (12) and is fixed with blow tank (21).
5. a kind of long-chain biatomic acid crystalline solid high-efficiency collecting device according to claim 1, it is characterised in that: the cooling
It is symmetrically arranged with no less than four cooling water pipes (17) between disk (18), sealing cover is had on the feed inlet (19), it is described
Crystallizing tank is provided with inspection hole on (5).
6. a kind of long-chain biatomic acid crystalline solid high-efficiency collecting device according to claim 1, it is characterised in that: the crystallization
Cooling cavity is provided between tank (5) and coolant seal cover (6), first coolant intake pipe (14) and the first cooling water are defeated
Outlet pipe (4) is connected to cooling cavity.
Priority Applications (1)
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CN201821702802.7U CN209123387U (en) | 2018-10-20 | 2018-10-20 | A kind of long-chain biatomic acid crystalline solid high-efficiency collecting device |
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CN201821702802.7U CN209123387U (en) | 2018-10-20 | 2018-10-20 | A kind of long-chain biatomic acid crystalline solid high-efficiency collecting device |
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110898456A (en) * | 2019-12-16 | 2020-03-24 | 潍坊联兴新材料科技股份有限公司 | Equipment for low-temperature crystallization of magnesium sulfate by using desulfurization circulating liquid |
CN113173861A (en) * | 2021-06-11 | 2021-07-27 | 长春市吉达自动化***有限公司 | Automatic system and method for lysine production crystallization extraction |
CN114853596A (en) * | 2021-02-04 | 2022-08-05 | 青岛智库生物技术有限公司 | Long-chain dicarboxylic acid refining method and device |
CN115634467A (en) * | 2022-10-28 | 2023-01-24 | 江西领能锂业有限公司 | Cooling equipment and process for industrial brine solution crystallization |
-
2018
- 2018-10-20 CN CN201821702802.7U patent/CN209123387U/en active Active
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110898456A (en) * | 2019-12-16 | 2020-03-24 | 潍坊联兴新材料科技股份有限公司 | Equipment for low-temperature crystallization of magnesium sulfate by using desulfurization circulating liquid |
CN114853596A (en) * | 2021-02-04 | 2022-08-05 | 青岛智库生物技术有限公司 | Long-chain dicarboxylic acid refining method and device |
CN113173861A (en) * | 2021-06-11 | 2021-07-27 | 长春市吉达自动化***有限公司 | Automatic system and method for lysine production crystallization extraction |
CN113173861B (en) * | 2021-06-11 | 2021-09-14 | 长春市吉达自动化***有限公司 | Automatic system and method for lysine production crystallization extraction |
CN115634467A (en) * | 2022-10-28 | 2023-01-24 | 江西领能锂业有限公司 | Cooling equipment and process for industrial brine solution crystallization |
CN115634467B (en) * | 2022-10-28 | 2023-08-04 | 江西领能锂业有限公司 | Cooling equipment and process for industrial brine solution crystallization |
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