CN208894219U - A kind of reduction reaction kettle with agitating function - Google Patents

A kind of reduction reaction kettle with agitating function Download PDF

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Publication number
CN208894219U
CN208894219U CN201821553464.5U CN201821553464U CN208894219U CN 208894219 U CN208894219 U CN 208894219U CN 201821553464 U CN201821553464 U CN 201821553464U CN 208894219 U CN208894219 U CN 208894219U
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Prior art keywords
autoclave body
reduction reaction
blower
motor
reaction kettle
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CN201821553464.5U
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Chinese (zh)
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周友法
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Shandong Chengwu Zhongyuan Chemical Co Ltd
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Shandong Chengwu Zhongyuan Chemical Co Ltd
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Abstract

The utility model discloses a kind of reduction reaction kettle with agitating function, including autoclave body, the middle position of the autoclave body bottom is equipped with outlet valve, the four corners of the autoclave body bottom are all equipped with support rod, bottom on the outside of the inside of the autoclave body is arranged with heating muff, the heating muff is internally provided with multiple groups electric heating wire, liquid injection pipe is provided at the top of the autoclave body side, and liquid feed valve is installed on the outside of liquid injection pipe, the autoclave body is provided with connecting tube far from blower, the input terminal of the blower is equipped at the top of liquid injection pipe side.Utility model device passes through the mutual cooperation of stirring motor, rotation axis, rotor plate and anchor formula stirring rod, material is mixed, and pass through the mutual cooperation of servo motor, gear, rack gear, motor bin, litter, sliding block and connecting plate, up and down adjustment is carried out to the position of stirring, accelerate the reaction rate of device, the reaction time is saved, so that the mixed effect of device is more abundant.

Description

A kind of reduction reaction kettle with agitating function
Technical field
It is specially a kind of with agitating function the utility model relates to Para Amino Benzamide production equipment technology Reduction reaction kettle.
Background technique
Para Amino Benzamide is a kind of organic compound, is the higher a kind of colorant of fastness in ice dyeing fuel, to ammonia The technique of yl-benzamide reduction is and the important link in production, reaction kettle are the capital equipments for carrying out reduction reaction operation, It is all lower in preparation, its product purity, yield for existing reduction reaction kettle, is unfavorable for the protection of environment, and agitating device is One important component of reduction reaction kettle, is mainly responsible for and is stirred material, mix material sufficiently in reduction reaction kettle Reaction is closed, improves reaction rate, the mixing position in existing reduction reaction kettle is relatively fixed, and mixed effect is poor, reaction rate It is relatively slow, a large amount of operating time is wasted, and device, in charging, the inner sidewall of powder autoclave body easy to attach can cause raw material Certain waste, and the pernicious gas that some devices generate during reduction reaction, can damage working environment, influence The health of operator.
Utility model content
The purpose of this utility model is to provide a kind of reduction reaction kettle with agitating function, to solve above-mentioned background skill The problem of being proposed in art.
To achieve the above object, the utility model provides the following technical solutions: a kind of reduction reaction with agitating function Kettle, including autoclave body, the middle position of the autoclave body bottom are equipped with outlet valve, and the four corners of the autoclave body bottom are all equipped with Support rod, the bottom on the outside of the inside of the autoclave body are arranged with heating muff, and the heating muff is internally provided with multiple groups electricity Heater strip is provided with liquid injection pipe at the top of the autoclave body side, and is equipped with liquid feed valve on the outside of liquid injection pipe, and the autoclave body is separate Blower is installed at the top of liquid injection pipe side, the input terminal of the blower is provided with connecting tube, the blower by connecting tube with The inside of autoclave body is interconnected, and middle position of the autoclave body close to blower side is equipped with cartridge filter, and the output of blower End is interconnected with cartridge filter, and the middle position on the outside of the cartridge filter is provided with filtering mounting groove, and filters mounting groove It is internally provided with screen pack, mounting plate, the middle position of the autoclave body over top are installed at the top of the screen pack Place is provided with multiple groups motor bin, and the bottom of motor bin is provided with multiple groups buffer spring, the motor bin by buffer spring with The top of autoclave body is connected with each other, and the inside of the motor bin is equipped with stirring motor, and the output end of the stirring motor is equipped with The rotation axis inside autoclave body is extended to, three groups of rotor plates are provided on the side wall of the rotation axis, are set on the outside of the rotor plate It is equipped with scraper plate compatible with autoclave body inner sidewall, the bottom of the rotation axis is equipped with anchor formula stirring rod, at the top of the autoclave body Side is provided with feed inlet, and the side far from feed inlet is equipped with L-type support plate, the L-type support plate one at the top of the autoclave body Servo motor is installed, and the output end of servo motor runs through the inside of L-type support plate at the top of end, the servo motor it is defeated Outlet is equipped with gear, and the motor bin is equipped with rack gear close to the side of L-type support plate, and rack and pinion is intermeshed, The motor bin is equipped with connecting plate far from the side of rack gear, and the connecting plate is equipped with sliding block far from the side of motor bin, institute It states and litter is installed between the top cushion spring of autoclave body and feed inlet, and litter is slidably connected with sliding block, described autoclave body one end The side at top is equipped with control panel.
Preferably, the bottom of the support rod is equipped with support foot.
Preferably, the side at the top of described autoclave body one end is provided with observation window.
Preferably, sealing cover is provided at the top of the feed inlet.
Preferably, the bottom end inside the filtering mounting groove is provided with card slot, the bottom of the screen pack be provided with The compatible buckle of card slot.
Preferably, the autoclave body is made of aluminum material.
Compared with prior art, the utility model has the beneficial effects that there is the reduction reaction kettle of agitating function to pass through for this The mutual cooperation of stirring motor, rotation axis, rotor plate and anchor formula stirring rod, is mixed material, and passes through servo electricity The mutual cooperation of machine, gear, rack gear, motor bin, litter, sliding block and connecting plate carries out up and down adjustment to the position of stirring, accelerates The reaction rate of device saves the reaction time, so that the mixed effect of device is more abundant, and device is in reaction, by right Autoclave body is internally heated, and further speeds up its reaction rate, and while agitating, and scraper plate is driven to adhere to autoclave body inner sidewall Powder scraped off, avoid it is viscous glutinous for a long time subsequent operation is impacted, while convenient for being cleaned after operation to autoclave body, And device passes through the mutual cooperation of blower, screen pack and cartridge filter, can purify the gas generated after reaction, be discharged, By the mutual cooperation of buckle, card slot and mounting plate, convenient for replacing to screen pack, enhanced convenience is operated.
Detailed description of the invention
Fig. 1 is the main view of the utility model;
Fig. 2 is the structural schematic diagram of the utility model;
Fig. 3 is the cartridge filter schematic diagram of internal structure of the utility model.
In figure: 1, outlet valve;2, support rod;3, autoclave body;4, cartridge filter;5, mounting groove is filtered;6, blower;7, connecting tube; 8, L-type support plate;9, servo motor;10, gear;11, rack gear;12, motor bin;13, litter;14, connecting plate;15, sliding block; 16, buffer spring;17, feed inlet;18, liquid injection pipe;19, liquid feed valve;20, control panel;21, heating muff;22, scraper plate;23, Stirring motor;24, rotation axis;25, rotor plate;26, anchor formula stirring rod;27, screen pack;28, mounting plate.
Specific embodiment
The following will be combined with the drawings in the embodiments of the present invention, carries out the technical scheme in the embodiment of the utility model Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiments of the present invention, those of ordinary skill in the art are without making creative work Every other embodiment obtained, fall within the protection scope of the utility model.
Fig. 1-3 is please referred to, a kind of embodiment provided by the utility model: a kind of reduction reaction kettle with agitating function, Including autoclave body 3, the middle position of 3 bottom of autoclave body is equipped with outlet valve 1, and the four corners of 3 bottom of autoclave body are all equipped with support rod 2, the bottom on the outside of the inside of autoclave body 3 is arranged with heating muff 21, and the multiple groups electric heating wire that is internally provided with of heating muff 21 (should The use model 0Cr21Al6Nb of electric heating wire), liquid injection pipe 18 is provided at the top of 3 side of autoclave body, and liquid injection pipe 18 is outer Side is equipped with liquid feed valve 19, and autoclave body 3 is far from the use model for being equipped with the blower 6(blower at the top of 18 side of liquid injection pipe GY4-73), the input terminal of blower 6 is provided with connecting tube 7, and blower 6 is interconnected by the inside of connecting tube 7 and autoclave body 3, autoclave body 3 middle position close to 6 side of blower is equipped with cartridge filter 4, and the output end of blower 6 and cartridge filter 4 are interconnected, filtering The middle position in 4 outside of cylinder is provided with filtering mounting groove 5, and filters mounting groove 5 and be internally provided with screen pack 27, to also The gas of original reaction carries out purification run, and the top of screen pack 27 is equipped with mounting plate 28, the interposition of 3 over top of autoclave body The place of setting is provided with multiple groups motor bin 12, and the bottom of motor bin 12 is provided with multiple groups buffer spring 16, and motor bin 12 passes through buffering The top of spring 16 and autoclave body 3 is connected with each other, and the inside of motor bin 12 is equipped with the use type of the stirring motor 23(stirring motor Number be Y90S-2), the output end of stirring motor 23 is equipped with the rotation axis 24 extended to inside autoclave body 3, the side wall of rotation axis 24 On be provided with three groups of rotor plates 25, the outside of rotor plate 25 is provided with scraper plate 22 compatible with 3 inner sidewall of autoclave body, to autoclave body 3 The powder of inner sidewall attachment is scraped off, and the bottom of rotation axis 24 is equipped with anchor formula stirring rod 26, the side setting at 3 top of autoclave body There is feed inlet 17,3 top of autoclave body is equipped with L-type support plate 8, the top peace of 8 one end of L-type support plate far from the side of feed inlet 17 Use model 57HB76-401A equipped with the servo motor 9(servo motor), and the output end of servo motor 9 runs through L-type branch The inside of fagging 8, the output end of servo motor 9 are equipped with gear 10, and motor bin 12 is equipped with close to the side of L-type support plate 8 Rack gear 11, and rack gear 11 and gear 10 are intermeshed, motor bin 12 is equipped with connecting plate 14, connecting plate far from the side of rack gear 11 14 sides far from motor bin 12 are equipped with sliding block 15, cooperate with litter 13, are supported, keep away to the side of motor bin 12 Exempt from motor bin 12 and positional shift occurs, litter 13, and litter are installed between the top cushion spring 16 and feed inlet 17 of autoclave body 3 13 are slidably connected with sliding block 15, and the side at the top of 3 one end of autoclave body is equipped with the use model of the control panel 20(control panel JG-128C), control panel 20 is electrically connected with blower 6, servo motor 9, electric heating wire and stirring motor 23 respectively by conducting wire, Blower 6, servo motor 9, control panel 20, electric heating wire and stirring motor 23 in device are the prior art, composed structure It is identical with connection type with existing apparatus.
In this embodiment, the bottom of support rod 2 is equipped with support foot, increasing friction force, anti-locking apparatus sliding, autoclave body 3 Side at the top of one end is provided with observation window, observes device inside reduction reaction, the top of feed inlet 17 is provided with close Capping improves device obturation effect, filters the bottom end inside mounting groove 5 and is provided with card slot, the bottom of screen pack 27 is provided with Buckle compatible with card slot, is replaced convenient for screen pack 27, and autoclave body 3 is made of aluminum material, is conducive in heating muff 21 Electric heating wire device is internally heated.
Working principle: the device electrical component is all powered by external power supply, is powered on, open sealing cover, through into Material mouth 17 injects raw material to the inside of autoclave body 3, opens liquid feed valve 19, is urged by liquid injection pipe 18 to the injection reaction of the inside of autoclave body 3 Then agent opens control panel 20, open stirring motor 23 by control panel 20, drive rotation axis 24,25 and of rotor plate Anchor formula stirring rod 26 is stirred mixed solution, accelerates reduction reaction rate, and by opening servo motor 9, band moving gear 10 carry out positive and negative rotation, and gear 10 is moved up and down with carry-over bar 11, enterprising in litter 13 by sliding block 15 while mobile Row sliding, and then drive motor bin 12 move up and down, while moving up and down by buffer spring 16 charge cabin 12 into Row buffering, and device is while agitating, scraper plate 22 is driven by the rotation of rotor plate 25, to the powder of 3 inner sidewall of autoclave body attachment End is scraped off, and the bottom end fallen into inside autoclave body 3 again is reacted, and opens electric heating wire to autoclave body by control panel 20 3 are internally heated operation, further speed up the reduction reaction rate of device, after reaction, stand to reaction solution Cooling, the liquid after the reduction of outlet valve 1 takes out, and device can be by buckling and card slot is mutually clamped, to screen pack 27 realize replacement.
It is obvious to a person skilled in the art that the present invention is not limited to the details of the above exemplary embodiments, and And without departing substantially from the spirit or essential attributes of the utility model, it can realize that this is practical new in other specific forms Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this is practical new The range of type is indicated by the appended claims rather than the foregoing description, it is intended that containing for the equivalent requirements of the claims will be fallen in All changes in justice and range are embraced therein.It should not treat any reference in the claims as limiting Related claim.

Claims (6)

1. a kind of reduction reaction kettle with agitating function, including autoclave body (3), it is characterised in that: in autoclave body (3) bottom Between be equipped with outlet valve (1) at position, the four corners of autoclave body (3) bottom are all equipped with support rod (2), the autoclave body (3) Inside on the outside of bottom be arranged with heating muff (21), the heating muff (21) is internally provided with multiple groups electric heating wire, It is provided with liquid injection pipe (18) at the top of autoclave body (3) side, and liquid feed valve (19) is installed on the outside of liquid injection pipe (18), it is described For autoclave body (3) far from being equipped with blower (6) at the top of liquid injection pipe (18) side, the input terminal of the blower (6) is provided with connecting tube (7), the blower (6) is interconnected by the inside of connecting tube (7) and autoclave body (3), and the autoclave body (3) is close to blower (6) one The middle position of side is equipped with cartridge filter (4), and the output end of blower (6) and cartridge filter (4) are interconnected, the cartridge filter (4) middle position on the outside of is provided with filtering mounting groove (5), and filters mounting groove (5) and be internally provided with screen pack (27), it is equipped with mounting plate (28) at the top of the screen pack (27), the middle position of autoclave body (3) over top is set It is equipped with multiple groups motor bin (12), and the bottom of motor bin (12) is provided with multiple groups buffer spring (16), the motor bin (12) is logical The top for crossing buffer spring (16) and autoclave body (3) is connected with each other, and the inside of the motor bin (12) is equipped with stirring motor (23), The output end of the stirring motor (23), which is equipped with, extends to the internal rotation axis (24) of autoclave body (3), the rotation axis (24) It is provided with three groups of rotor plates (25) on side wall, is provided on the outside of the rotor plate (25) compatible with autoclave body (3) inner sidewall The bottom of scraper plate (22), the rotation axis (24) is equipped with anchor formula stirring rod (26), and the side at the top of the autoclave body (3) is provided with Feed inlet (17), autoclave body (3) top are equipped with L-type support plate (8) far from the side of feed inlet (17), the L-type support It is equipped with servo motor (9) at the top of plate (8) one end, and the output end of servo motor (9) runs through the inside of L-type support plate (8), The output end of the servo motor (9) is equipped with gear (10), and the motor bin (12) is pacified close to the side of L-type support plate (8) Equipped with rack gear (11), and rack gear (11) and gear (10) are intermeshed, and the motor bin (12) is pacified far from the side of rack gear (11) Equipped with connecting plate (14), the connecting plate (14) is equipped with sliding block (15) far from the side of motor bin (12), the autoclave body (3) It is equipped between top cushion spring (16) and feed inlet (17) litter (13), and litter (13) is slidably connected with sliding block (15), Side at the top of described autoclave body (3) one end is equipped with control panel (20).
2. a kind of reduction reaction kettle with agitating function according to claim 1, it is characterised in that: the support rod (2) bottom is equipped with support foot.
3. a kind of reduction reaction kettle with agitating function according to claim 1, it is characterised in that: the autoclave body (3) Side at the top of one end is provided with observation window.
4. a kind of reduction reaction kettle with agitating function according to claim 1, it is characterised in that: the feed inlet (17) sealing cover is provided at the top of.
5. a kind of reduction reaction kettle with agitating function according to claim 1, it is characterised in that: the filtering installation The internal bottom end of slot (5) is provided with card slot, and the bottom of the screen pack (27) is provided with buckle compatible with card slot.
6. a kind of reduction reaction kettle with agitating function according to claim 1, it is characterised in that: the autoclave body (3) It is made of aluminum material.
CN201821553464.5U 2018-09-22 2018-09-22 A kind of reduction reaction kettle with agitating function Active CN208894219U (en)

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Application Number Priority Date Filing Date Title
CN201821553464.5U CN208894219U (en) 2018-09-22 2018-09-22 A kind of reduction reaction kettle with agitating function

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Application Number Priority Date Filing Date Title
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110771677A (en) * 2019-12-08 2020-02-11 常德云港生物科技有限公司 Chicken gallbladder thawing and filtering device for pretreatment of chicken gallbladder processing by biological enzyme
CN112619586A (en) * 2021-03-10 2021-04-09 山东亚邦化工科技有限公司 Gas phase reaction bed for hydrocyanic acid production

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110771677A (en) * 2019-12-08 2020-02-11 常德云港生物科技有限公司 Chicken gallbladder thawing and filtering device for pretreatment of chicken gallbladder processing by biological enzyme
CN112619586A (en) * 2021-03-10 2021-04-09 山东亚邦化工科技有限公司 Gas phase reaction bed for hydrocyanic acid production

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